Company Name: Road Binders Ltd
Licence No: P0084-01
Year: 2015, Visit No: 1
Report No: 015-166
Cuil Greine House
Ballincollig Commercial Park
Link Road
Ballincollig
Cork
T: 021 4810016
M: 086 3819387
[email protected]
www.glenenv.ie
se
.
_____________________________________________________________
f c Fo
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ot
he
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Stack Emissions Monitoring Report
for
Road Binders Ltd
nt
o
Mallow, Co. Cork
Co
n
se
EPA IPPC Licence REF: P0084-01
_______________________________________________________________
Report No: 015-166
Monitoring Date:
16th December 2015
Test report shall not be reproduced except in full, without written approval of the laboratory.
Page 1 of 12
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Licence No: P0084-01
Year: 2015, Visit No: 1
Report No: 015-166
Report Summary:
QGE15-067-03
Operator Licence No:
P0084-01
Operator Name:
Road Binders Ltd
Installation:
Mallow, Co. Cork
Contact Name:
Paul Byrne
Phone No:
0 66 9763588
Monitoring dates:
16th December 2015
Monitoring Organisation:
Glenside Environmental, Cuil Greine House
Link Road, Ballincollig, Cork
Phone No:
(021) 4810016
Email:
[email protected]
se
.
Job Quotation No:
4th January 2016
ot
he
ru
Report Date:
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Report written by:
MCERTS reg No:
Competency:
Function:
Co
n
Report approved by:
se
nt
o
Endorsements:
Ewa Piatek
MM07 799
Level 2
Team Leader
TE1, TE2, TE3, TE4
Ewa Piatek
MCERTS reg No:
MM07 799
Competency:
Level 2
Function:
Team Leader
Endorsements:
TE1, TE2, TE3, TE4
Signed by: Quality Manager
Page 2 of 12
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Report No: 015-166
TABLE OF CONTENTS
PAGE
1.
INTRODUCTION........................................................................................................................ 4
2.
OBJECTIVES .............................................................................................................................. 4
2.1.
2.2.
3.
SUBSTANCES TO BE MONITORED AT EACH EMISSION POINT ..................................................... 4
SPECIAL REQUIREMENTS ........................................................................................................ 4
MATERIALS AND METHODS ................................................................................................ 4
3.1.
FLUE GAS ANALYSIS (CO – IS EN 15058:2006, CO2 – ISO12039:2001, NOX – IS EN
14792:2006, O2 – IS EN 14789:2005, SO2 – METHOD TGN M21) .................................................... 4
3.2.
VOLUMETRIC FLOW RATE – ISO 16911-1:2013 ..................................................................... 4
MONITORING RESULTS ......................................................................................................... 5
he
ru
se
.
MONITORING RESULTS ........................................................................................................... 5
REFERENCE CONDITIONS ........................................................................................................ 5
VOLUMETRIC FLOW RATE ...................................................................................................... 6
BOILER A1 RESULTS IN E-PRTR FORMAT ............................................................................... 6
METHODS AND ACCREDITATION STATUS................................................................................ 7
ot
4.1.
4.2.
4.3.
4.4.
4.5.
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4.
OPERATING INFORMATION................................................................................................. 8
6.
MONITORING DEVIATION .................................................................................................... 8
7.
ANNEX 1 .................................................................................................................................... 10
8.
se
ANNEX 2 .................................................................................................................................... 11
8.1.
8.2.
9.
PERSONNEL ........................................................................................................................... 10
EQUIPMENT USED .................................................................................................................. 10
Co
n
7.1.
7.2.
nt
o
5.
DIAGRAMS OF THE STACKS – A1 ........................................................................................... 11
SAMPLING MEASUREMENTS .................................................................................................. 11
ANNEX 3 .................................................................................................................................... 12
9.1.
RESULTS AND UNCERTAINTY CALCULATIONS FOR STACK A1-1 – TOTAL OF 13 PAGES ......... 12
Page 3 of 12
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Report No: 015-166
1. Introduction
Glenside Environmental was commissioned by Southern Scientific Services ltd to perform air emission
monitoring at Road Binders Ltd - Mallow, Co. Cork. This report presents details of this monitoring
programme.
2. Objectives
2.1.
Substances to be monitored at each emission point
Sample Locations
Parameter
O2
CO
A1
NOx as NO2
SO2
Special Requirements
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2.2.
ot
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.
CO2
The boiler normally operate intermittently to maintain the prescribed storage temperature requirement
of the product. In order to facilitate monitoring for a minimum of thirty minutes the boilers were turned
off in advance of scheduled monitoring and the product was allowed to cool. The boilers then operated
for an extended time to bring the product back up to temperature and this facilitated a 15 minute
monitoring period.
Co
n
se
nt
o
3. Materials and Methods
This section provides brief details of the methodologies employed to perform the air emission
monitoring.
3.1.
Flue Gas analysis (CO – IS EN 15058:2006, CO2 – ISO12039:2001, NOx – IS EN 14792:2006,
O2 – IS EN 14789:2005, SO2 – Method TGN M21)
Flue gas concentrations were monitored using a Horiba PG-250 flue gas analyser. The PG-250 is a
portable stack gas analyzer that can simultaneously measure up to five separate gas components:
NOx, CO, CO2, SO2 and O2. The PG-250 uses non-dispersive IR detection for CO, SO2, and CO2;
chemiluminescence (cross-flow modulation) for NOx; and a paramagnetic cell for O2 measurements.
3.2.
Volumetric Flow Rate – ISO 16911-1:2013
The volumetric airflow rate was determined from stack velocity measurements calculated
in accordance with ISO 16911-1:2013. Airflow rate and temperature profiles were performed at precalculated intervals across the stack in order to determine the average velocity profile across the stack
diameters.
Page 4 of 12
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Report No: 015-166
4. Monitoring Results
Tables 4.1 and 4.2 presents the results of the air emission monitoring sampling program carried out at the emission stacks listed below.
4.1.
Monitoring Results
Uncertainty
Date of
Monitoring
Start –End Time of
Monitoring
ru
Results reported are corrected to reference conditions as per IPPC Licence requirements.
--
0.28 %
16/12/2015
10:00-10:15
0.000
kg/hr
0.12
kg/hr
2.19 mg/m3
16/12/2015
10:00-10:15
10.25 mg/m3
16/12/2015
10:00-10:15
n/a
2.95 mg/m3
16/12/2015
10:00-10:15
12.69 %
n/a
0.56 %
16/12/2015
10:00-10:15
93.53 %
n/a
n/a
16/12/2015
10:00-10:15
Substances
ELV
mg/m3
CEMS
Results
LOD
Results
Results
A1
O2
n/a
n/a
0.1 %
3.81 %
A1
CO
80
n/a
0.4 mg/m3
<0.4 mg/m3
A1
Nitrogen Oxides as
NO2
350
n/a
0.2 mg/m3
A1
SO2
850
n/a
0.3
mg/m3
144.13
mg/m3
<0.3
mg/m3
A1
CO2
n/a
n/a
0.1 %
A1
Boiler Efficiency
n/a
n/a
n/a
Co
ns
en
to
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.
Emission
Point
Results for NOx, CO, CO2, O2 and SO2 are within INAB accreditation range.
4.2.
Reference Conditions
Emission Point
Reference Temperature
Reference Pressure
Reference Moisture
Reference Oxygen
A1
273 K
101.3 kPa
Dry
3%
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Report No: 015-166
Emission Point
Actual Moist Flow
Rate
Moist Flow Rate at
STP
Flow Rate at STP,
Ref O2
Emission Limit Value
Units
A1
1556.22
857.05
818.46
n/a
m3/h
Boiler A1 results in E-PRTR format
ru
se
.
Release to air
Quantity
he
Pollutant
Pollutant NO.
Name
M/C/E
8
11
2
NOx as NO2
SOx as SO2
CO
M
M
M
3
CO2
M
to
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ot
Method
Code
IS EN 14792:2006
TGN M21
IS EN 15058:2006
ISO 12039:2001
Description
Paramagnetic
NDIR
NDIR
NDIR
Total kg/yr
Accidental (kg/yr)
206.41
0.00
0.00
-
356896.37
-
ns
en
4.4.
Volumetric Flow Rate
Co
4.3.
Page 6 of 12
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Report No: 015-166
4.5.
Methods and Accreditation Status
Determinant
Reference Method
Accreditation
Status
Analytical Method
Description
Subcontracted
Laboratory
Laboratory
Accreditation
Status
A1
CO by Horiba
IS EN 15058:2006
INAB
NDIR
n/a
n/a
A1
CO2 by Horiba
ISO 12039:2001
INAB
NDIR
n/a
n/a
A1
Flow, Temperature, Pressure
ISO 16911-1:2013
INAB
n/a
n/a
n/a
A1
Nox by Horiba
IS EN 14792:2006
INAB
Chemiluminescence
n/a
n/a
A1
O2 by Horiba
IS EN 14789:2005
INAB
Paramagnetic
n/a
n/a
A1
SO2 by Horiba
TGN M21
INAB
NDIR
n/a
n/a
to
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.
Sampling
Point:
Co
ns
en
Substances were monitored as per monitoring objectives.
Substances were monitored in accordance with the requirements stated in AG2 (Air Emissions Monitoring Guidance Note#2)
Page 7 of 12
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Report No: 015-166
5. Operating Information
Emission
Point
A1
Process
Status
Load
/Feedstock
Process Details
Fuel
/Feedstock
Abatement
System
Status of
Abatement
System
Operation as
normal
Boiler operate
intermittently to
maintain the
prescribed storage
temperature
requirement of the
product. The average
running time is
approximately 1750
hours per year.
Marked Gas Oil
None
None
se
.
6. Monitoring Deviation
A1
ot
he
ru
Requirements of IS EN 15259 for sampling
points
Yes, measuring plane is located as far downstream
and upstream from any disturbances.
Yes, measuring plane of duct is located in a section
of duct with five hydraulic diameters of straight duct
upstream of the sampling plane.
Yes, measuring plane is located in a section of duct
with five hydraulic diameters from top of stack.
Co
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Measuring plane is located as far downstream and
upstream from any disturbances, which could
change direction of flow (bends, fans, partially
closed dumpers).
Measuring Plane is located in a section of duct with
at least five hydraulic diameters of straight duct
upstream of the sampling plane.
Measuring Plane is located in a section of duct with
at least two hydraulic diameters of straight duct
downstream of the sampling plane (five hydraulic
diameters from top of the stack).
Measuring Plane is located in a section of duct with
constant shape and cross-sectional area.
Measurement section is clearly identified and
labelled.
Yes, measuring plane is located in a section of duct
with constant shape and cross-sectional area.
Yes, measuring section is clearly identified and
labelled.
Requirements of IS EN 15259 for platform,
working space and ports size.
A1
Appropriate working area.
Yes, platform has appropriate size.
Safe access to monitoring point.
Yes, access is safe.
Sufficient ports number
Small stacks(<0.7) – 1 port
0.7-1.5m – 2 ports
>1.5m – 4 ports
1 port available.
Appropriate port size.
Yes, 50 mm.
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Report No: 015-166
Requirements of ISO 16911-1:2013 for flow,
temperature and pressure profile of the stack
Required number of points were sampled as per
ISO 16911-1 requirements.
A1
Yes, 4 point sampled.
No negative flow.
Yes, no negative flow found in the stack flue gasses.
All points sampled swirl check was below 15°
Yes, al point sampled swirl check result were below
15°
Differential pressure higher than 5Pa measured with
pitot tube.
The ratio of highest to lowest local gas velocity is
outside (higher than 3:1) of requirements
Yes, differential pressure result was higher than 5 P.
Yes, Ratio of highest to lowest gas velocity was
within requirements.
Requirements of IS EN 14792 for NOx
NOx overall uncertainty calculated is within
requirement of <10% at the daily ELV expressed on
dry basis before correction to O2 reference
concentration.
NOx calibration drift is lower than 2% of the span
value.
A1
Uncertainty within requirements.
Drift below 2%.
ru
se
.
.
A1
ot
he
Requirements of IS EN 15058 for CO
f c Fo
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CO overall uncertainty calculated is within
requirement of <6% at the daily ELV expressed on
dry basis before correction to O2 reference
concentration.
CO calibration drift is lower than 2% of the span
value.
Requirements of IS EN 14789 for O2
Drift below 2%.
A1
Uncertainty within requirements.
Co
n
se
nt
o
O2 overall uncertainty calculated is within
requirement of <6% of value expressed on dry
basis.
O2 calibration drift is lower than 2% of the span
value.( Section 8.4.2.3)
Uncertainty within requirements.
Page 9 of 12
Drift below 2%.
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Report No: 015-166
7. Annex 1
Personnel
Scientist/Technician
Name
Team
Leader
Technician
Ewa Piatek
Patrick Power
Qualification
Technical
Endorsements
MCERTS
Number
Level 2
TE1, TE2, TE3, TE4
MM07 799
Trainee
-
MM12 1183
Equipment used
Equipment
GEN Equipment No
Distance Meter
EQ089
Measuring Tape
EQ090
he
ru
7.2.
Position
se
.
7.1.
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KIMO Pitot Tube
KIMO Flow Meter
Horiba PG-250
EQ079
EQ066
EQ068
Co
n
se
nt
o
Chiller Unit
EQ080
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Report No: 015-166
8. Annex 2
Diagrams of the stacks – A1
8.2.
Sampling measurements
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.
8.1.
Determinant
A1
Units
1
-
4
-
5.38
m/s
101.155
kPa
Average Temperature
222
°C
Stack Diameter
0.32
m
T Reference
273
Deg K
P Reference
101.3
kPa
Isokinetic condition
n/a
%
Oxygen
3.81
%
CO2
12.69
%
Water vapour
n/a
%
Nozzle Size
n/a
mm
Number of Ports Sampled
Average Pressure
se
Co
n
Average Velocity v'a
nt
o
Number of Points Sampled
Velocity, temperature and pressure measurements are within INAB accreditation range.
Page 11 of 12
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Report No: 015-166
9. Annex 3
Results and uncertainty calculations for Stack A1-1 – Total of 13 pages
Co
n
se
nt
o
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.
9.1.
Page 12 of 12
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Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
Road Binders Ltd
P0084-01
Visit No: 1
Doc No
Rev Date:
Issued by:
GEN2-002rev17
9/18/2015
QM
Flow Calculations
for
12/16/2015
015-166
A1 Boiler
Equipment Used:
Millenium 5
console:
EQ069
Probe:
EQ071
KIMO - Flow Test: EQ079
Pitot Tube:
EQ081
Kimo Pitot Tube :
EQ080
Rule:
Laser Distance
Meater:
EQ083
EQ089
Circular no central
point (tangential)
0.3
0.3
0.3
0.3 m
Stack
Diameter Measurements
Diameter Average:
Stack Area
Sampling Line
Sampling Points
0.08 m2
1
1
Port Depth (m):
Port 1:
Wall thicknes (m):
0
0.1
Pitot Tube Checks:
Deformities, Burrs, Damage
Line 2
0.00
0.00
0.00
0.00
0.00
0.00
Note: At least once per line.
Pa
Pa
Pa
Pa
Pa
Pa
of
mmH2O
55.00
55.00
55.00
55.00
55.00
55
en
t
Pa
6
6
6
6
6
5.6
1.08
ns
mmH2O
Unc of static pressure calculations
St Dev:
0.00
0.00
0.00
0.00
Unc
1.52
1.52
Note: Sampling point should be located either >3% of th
Co
Static Pressure:
Reading 1
Reading 2
Reading 3
Reading 4
Reading 5
Average:
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
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re o
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ny
ot
he
ru
se
.
Points Calculations
Comments
KIMO Pitot EQ080
None
Inernal Leakage Check
Pressuriezed pressure:
500 Pa
Note: blow through the pitot impact opening until at least 7.6 cm (3.0 in.) H20
Page1of13
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Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
Time of leak check:
15 s
Leak Check Result:
Pass
Road Binders Ltd
P0084-01
Visit No: 1
°
GEN2-002rev17
9/18/2015
QM
Flow Calculations
for
12/16/2015
015-166
A1 Boiler
velocity head registers on the manometer; then, close off the impact opening.
The pressure shall remain stable for at least 15 seconds; (2) do the same for
the static pressure side, except using suction to obtain the minimum
of 7.6 cm (3.0 in.) H20.
S-tupe pitot tube shall be positioned perpendicular to the direction of the
flow. The static pressure is than measured using both taps. The difference in
the measured static pressure should be < 10Pa
Check on stagnation and reference
pressure taps:
<10Pa
Swirl Check:
Point 1
Doc No
Rev Date:
Issued by:
Within requirements <15°
0.00 Yes
If Swirl Check is outside requiremnts the correction has
to be applied.
Absolute pressure of the stack gas:
The absolute pressure in the duct is given by the measurement of the atmospheric pressure on the site
and the static pressure measured in the duct.
𝑃𝑃𝑆𝑆𝑆𝑆𝑆𝑆𝑆𝑆𝑆𝑆𝑆𝑆
𝑃𝑃𝑠𝑠 = 𝑃𝑃𝑏𝑏 +
13.6
Barometric
(Atmospheric
Pressure)Pb
Pstatic
758.3123612 mmHg
5.610461387 mmH2O
Conversion form
mmH2O to mmHg
Note: 1mb = 0.75 mmHg (Since1 atmosphere=1013.25 mb = 760 mmHg)
760 mmHg =
101325 Pa
13.6
101100 Pa
10.00
C°
%𝐶𝐶𝐶𝐶𝐶
%𝑂𝑂𝑂
%𝐶𝐶𝐶𝐶 + %𝑁𝑁𝑁
+ 32
+ 28
100
100
100
28.85
he
0.040
28.85
18
of
Md=
%
%
%
%
Bwo
Md
Molecular weight of
CO
ppm
15 Ms=
28.41
en
t
0.06
20.90
0.0015
79.04
𝑀𝑀𝑠𝑠 = 𝑀𝑀𝑑𝑑 1 − 𝐵𝐵𝑤𝑤𝑤𝑤 + 18(𝐵𝐵𝑤𝑤𝑤𝑤 )
ns
CO2
O2
CO
N2
Pitot Cooficiency
Calibration Date:
EQ080 KIMO
m/sec
Molecular weight of stack gas (wet):
Co
𝑀𝑀𝑑𝑑 = 44
Absolute Pressure
of stack
ot
758.7248951 mmHg
101155 Pa
Molecular Weigh of Dry Gas Stream:
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
Ps =
ru
se
.
Atmospheric Press
Atmospheric Temperature:
7/29/2015
Cp
EQ081 Mill 5
m/sec
Cp
3.02
5.2
10.38
15.6
20.43
25.8
Pitot Cooficiency used for
calculations:
0.806
0.806
0.83
0.838
0.829
0.832
0.8060
Page2of13
EPA Export 17-04-2016:00:48:47
Pitot Tube Checks:
√ΔPs mmH2O
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707
0.707106781
m/s
5.4
5.3
5.2
5.6
3.0
3.0
3.0
3.0
3.0
3.0
3.0
3.0
3.0
3.0
3.0
3.0
3.0
3.0
3.0
3.0
5.38
Temperature
222
222
222
222
222
222
222
222
222
222
222
222
222
222
222
222
222
222
222
222
222
Max flow:
Min. Flow:
Pressure of Stack
kPa
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
101.155
Differencial Pressure
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
4.90
Pa
Uncertainty Calculations
Dynamic
Temperat
Pressure Velocity
ure
Pressure
4.90
4.90
4.90
4.90
3.020139
3.020139
222
222
222
101.155
101.155
101.155
.
Velocity
4.90
3.020139
222
101.155
5.30
3.02
3.491111
222
101.155
Comments
KIMO Pitot EQ080
None
Uncertainty Calc
0.00 Std Dev
0.00
1.52 UΔp
0.16 Uvi
0.01
0.00 Std Dev
0.00
1.52 UΔp
0.41
0.06
0.00 Std Dev
0.00
1.52 UΔp
0.41
0.06
0.00 Std Dev
0.00
1.52 UΔp
0.41
0.06
4.43
2.214
#####
0.118
2√ΔP
√ΔP
U2Δp
U2Δp/4Δp
4.43
2.214
2.32
0.118
2√ΔP
√ΔP
U2Δp
U2Δp/4Δp
4.43
2.214
2.32
0.118
2√ΔP
√ΔP
U2Δp
U2Δp/4Δp
4.43
2.214
2.32
0.118
2√ΔP
√ΔP
U2Δp
U2Δp/4Δp
0.473 ∑U2Δp/4Δp
78.42 (∑√Δp)2
en
t
of
Deformities, Burrs, Damage
A1 Boiler
12:00
Velocity by Mill 5
1.8 :1
for
se
ΔPs Pa
ΔPs mmH2O
0.5
Point 1
4.90
Point 2
4.90
0.5
Point 3
4.90
0.5
Point 4
4.90
0.5
Point 5
4.90
0.5
0.5
Point 6
4.90
Point 7
4.90
0.5
Point 8
4.90
0.5
Point 9
4.90
0.5
Point 10
4.90
0.5
0.5
Point 11
4.90
Point 12
4.90
0.5
Point 13
4.90
0.5
0.5
Point 14
4.90
Point 15
4.90
0.5
Point 16
4.90
0.5
Point 17
4.90
0.5
Point 18
4.90
0.5
0.5
Point 19
4.90
Point 20
4.90
0.5
Total Average:
0.5
Higes to Lowest flow ratio:
Requirement is Duct Flow ratio of max. to min. <3:1
Flow Calculations
12/16/2015
015-166
ru
Time End:
GEN2-002rev17
9/18/2015
QM
he
11:56
Doc No
Rev Date:
Issued by:
ot
Time Start:
Road Binders Ltd
P0084-01
Visit No: 1
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
Co
ns
Inernal Leakage Check
Pressuriezed pressure:
Time of leak check:
500 Pa
15 sec
Leak Check Result:
Pass
Check on stagnation and reference
pressure taps:
<10Pa
Note: blow through the pitot impact opening until at least 7.6 cm (3.0 in.) H20
velocity head registers on the manometer; then, close off the impact opening.
The pressure shall remain stable for at least 15 seconds; (2) do the same for
the static pressure side, except using suction to obtain the minimum
of 7.6 cm (3.0 in.) H20.
S-tupe pitot tube shall be positioned perpendicular to the direction of the
flow. The static pressure is than measured using both taps. The difference in
the measured static pressure should be < 10Pa
Page3of13
EPA Export 17-04-2016:00:48:47
Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
Road Binders Ltd
P0084-01
Visit No: 1
Doc No
Rev Date:
Issued by:
GEN2-002rev17
9/18/2015
QM
Flow Calculations
for
12/16/2015
015-166
A1 Boiler
Results:
Circular Stack
Stak Diameter:
A default wall effect adjustments factors may be used
without without taking wall effect measurements.
WAF Wall effect correction factor:
0.32 m
Average flow:
Wall effect correction factor:
Average Flow corrected for wall effect:
Average Temperature:
Average Pressure:
Average Moisture:
Average Oxygen:
5.38
1
5.38
495.00
101.155
Reeference Conditions:
Reference Temperature:
Reference Pressure:
m/s
Smooth walled ducts
m/s
K
kPa
%
3.81 %
Rough Walled ducts
0.99 bricks, mortar
Note: The correction of average velocity for wall
effect is not required for measurements to support
isokinetic sampling.
273.15 K
101.325 kPa
Reference Moisture:
0%
Reference Oxygen:
3%
Mass Emissions Calculations:
Volumetric Flow Rate
0.43 m3/s
he
ru
se
857.05 m3/h
818.33 m3/h
818.33 m3/h
ot
Volumertic Flow Rate corrected to STP
Volumertic Flow Rate corrected to STP and O2 ref
Volumertic Flow Rate corrected to STP O2 ref and Moisture
.
1556.22 m3/h
Uncertainty Calculations:
Input Quantities:
Expanded uncerta expressed with a level of confidence of 95
Expanded uncerta expressed with a level of confidence of 95
0.0074
0.25
0.51
9.41
%
Pa
±%
±%
±%
of
K
1
Pa
300
% dry
6
% dry
6
%
20
kg/m3
Pa
m/s
K
0.02
u(K)
Pa
Pa
Pa
2
% of the range between 2 calibration
% of the range
kg/mol
Max permissible error
Accuracy
Max permissible error estimated at
Volume fraction on d
Volume fraction on d
Volume fraction on dry gas
en
t
2%
20 Pa
ns
Unit
m
Co
0.32
1
495
10115.5
20.90
0.06
4
0.70
101155
3.491111122
1.01
0.01
1000
1
2
0.1
0.06
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
Volumetric Flow Rate
Diameter of Stack
Number of points measured:
Temperature:
Atmospheric Pressure:
Oxygen content:
CO2 content:
H2O content
Density of Gas
Absolute pressure
average Velocity
Pitot Tube characteristic
Standard unc on the coefficient ot the
Range:
0
Resolution
Calibration Uncertainty
Drift
Lack of fit
Mollar Mass Wet (M
0.284456
unc H2O
0.4 %
unc O2
0.61 %
unc CO2
0.00 %
unc Molar Weight
0.00006 Kg/mol
unc Temp
2.48 K
Abs press unc
174.38 Pa
unc Patm
173.30 Pa
std unc associated with the density u(ρ)
0.995
20.1 % wet
0.1 % wet
±
coverage factor
kg/m3
m/s
±m/s
±%
Page4of13
EPA Export 17-04-2016:00:48:47
Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
Road Binders Ltd
P0084-01
Visit No: 1
12/16/2015
015-166
CO
ppm
SOx
ppm
Doc No
Rev Date:
Issued by:
GEN2-002rev17
9/18/2015
QM
Flue Gasses Records and Calculations
for
A1 Boiler
1. Calibration:
Zero Cylinder
Calibration Values:
Horiba Range:
0
0-500
Zero:
Span:
2 times repeatability:
Zero:
0
0-500
0-500
Directly to analyzer:
0.3
0.2
407.7
401
0.2
0.2
0.1
-0.02
0.6
0.3
Through the sampling line:
0.2
-0.02
387.60
<200
381.33
<200
NO 400 ppm
Nitrogen
400.3 ppm
3.7 ppm
2128269
7/30/2013
7/30/2016
NO2 - 100 ppm
Nitrogen
80.2 ppm
2%
323876
4/7/2013
1/21/2016
CO - 400 ppm
Nitrogen
401.4 ppm
3.7 ppm
92314
11/7/2013
11/7/2016
10/23/2018
0
SO2 requirement: When applying the zero and
span gases, measure the T90response time,
and then wait at least three times the T90value
before taking the readings for zero and span;
0-25
0.2
402.6
0.2
15
0.2
21
0.2
0.3
0.04
0.3
0.02
0.2
0.2
-0.02
0.2
-0.67
0.1
-0.48
383.52
Exp date:
20.86
0
0-20
<200
Date of
calibration
92361
14.99
0
Cylinder No
14.24
<200
Zero deviation lower than 2 times the
repeatability at zero.
NO 400 ppm
Nitrogen
408
4 ppm
216866
10/24/2014
CO2 - 15%
Nitrogen
14.99%
0.12%
PR297816
9/7/2013
9/7/2016
O2 - 21%
Nitrogen
20.86%
0.11%
92361
9/7/2013
9/7/2016
Nitrogen
403.7 ppm
0.50%
324415
6/24/2013
6/24/2016
SO2 -400 ppm
Nitrogen
19.82
<200
A5477
Differences between the readings
obtained during the adjustments of the
analyser and during the check shall be
145.00 lower than 2%
Time (s):
121.00
132.00
134.00
134.00
Co
ns
en
t
of
Zero:
Difference as %:
Response Time:
95% of Span Gas:
Time Required (s):
403.7
Uncertainty
.
401.4
Certified
Value
se
408
Span Cylinder
Calibration Values:
324415 PR297816
Balance
ru
92314
Components
he
216866
O2
%
ot
Calibration Gas
Cylinder Number:
CO2
%
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
NO
ppm
SO2 requirement: When applying the zero and
span gases, measure the T90response time,
and then wait at least three times the T90value
before taking the readings for zero and span;
Span:
Difference as %:
Zero:
Span:
Zero Drift:
Span Drift:
407.3
401.2
402.8
14.99
20.98
0.10
-0.05
-0.05
0.07
0.10
After measurement through the sampling line:
0.1
0.2
0.4
402.4
407.6
401.2
0.2
14.98
0.1
20.98
0.00
-0.07
0.00
0.00
-0.05
0.10
0.00
0.07
If the span or zero drift are bigger than 2%
of the span value it is necessery to correct
both for zero and span drift. If the drift
result is higher than 5% results shall be
rejected.
0.00
0.00
Page5of13
EPA Export 17-04-2016:00:48:47
Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
Equipment Used:
Horiba:
Chiller Unit:
Road Binders Ltd
P0084-01
Visit No: 1
12/16/2015
015-166
Doc No
Rev Date:
Issued by:
GEN2-002rev17
9/18/2015
QM
Flue Gasses Records and Calculations
for
A1 Boiler
EQ066
EQ068
2. Measurement:
Average:
12.68
12.69
12.68
12.69
12.69
12.71
12.69
12.68
12.69
12.68
12.68
12.69
12.68
12.69
12.69
3.83
3.81
3.81
3.8
3.8
3.77
3.81
3.83
3.81
3.81
3.83
3.81
3.81
3.8
3.8
0.00
12.69
3.81
se
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
.
O2
%
en
t
of
67
66
67
67
68
68
68
68
66
67
67
66
67
67
68
CO2
%
ns
10:00:00 AM
10:01:00
10:02:00
10:03:00
10:04:00
10:05:00
10:06:00
10:07:00
10:08:00
10:09:00
10:10:00
10:11:00
10:12:00
10:13:00
10:14:00
10:15:00
10:16:00
10:17:00
10:18:00
10:19:00
10:20:00
10:21:00
10:22:00
10:23:00
10:24:00
10:25:00
10:26:00
10:27:00
10:28:00
10:29:00
Average readings:
SOx
ppm
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Co
Readings:
CO
ppm
Gas temperature should be maintain below 4°C
ru
NOx
ppm
3 °C
he
0:01:00
MAK Conditioning Unit Temperature:
10:14:00 AM
ot
10:00:00 AM End Time:
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
Start Time:
67.13
0.00
Page6of13
EPA Export 17-04-2016:00:48:47
% Dry
Uncertainty %
mg/m3 Dry, STP
kg/hr
kg/yr
GEN2-002rev17
9/18/2015
QM
14.99
20.98
401.20
12:14:00 AM
0.00
0.20
0.20
1.00
1.00
0.00
0.00
-0.20
-0.20
0.00
0.00
0.00
402.40
12:14:00 AM
0.00
0.20
0.40
1.00
1.00
0.00
0.15
-0.20
-0.40
-0.20
-20.69
0.10
14.98
12:14:00 AM
0.00
0.20
0.20
1.01
1.01
0.00
0.07
-0.20
-0.20
0.00
-0.01
0.07
20.98
#########
0.00
0.10
0.10
1.00
1.00
0.00
0.00
-0.10
-0.10
0.00
0.00
0.00
0.00
0.00
12.69
3.81
-0.20
-0.20
12.78
3.74
ot
he
402.80
se
20.86
A1 Boiler
ru
14.99
for
.
Flue Gasses Records and Calculations
401.20
206.41
0.00
CO2
12.69
0.56
249215.48
203.94
356896.37
O2
3.81
0.28
Note: Boiler is running aproximatly 3 minutes per hour, intermittent operation is due to maintain the
prescribed storage temperaure requirement of the product.
of
%
m3/hr
hr/yr
m3/yr
273.15
101.325
3
0
K
kPa
%
%
ns
en
t
0
818.33
1750
1432079.5
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
495 K
101.155 kPa
3.808666667 %
Average Moisture:
Volumertic Flow Rate corrected to STP O2 ref and
Boiler running hours per year
Annual flow rate:
Reference Conditions:
Reference Temperature:
Reference Pressure:
Reference Oxygen:
Reference Moisture:
Results :
Units
NOX
CO
ppm Dry
67.13
0.00
Correction factor ppm
2.05
1.25
to mg/m3
mg/m3 Dry, STP
137.62
0.00
mg/m3 Dry, STP, ref
144.13
0.00
O2
350
80
ELV mg/m3
10.25
2.19
Uncertainty mg/m3
kg/hr
0.12
0.000
kg/yr
Doc No
Rev Date:
Issued by:
Co
Span Gas Value
408
Span reading before
measurement
407.30
Span reading after
measurement
407.60
Sampling time
12:14:00 AM
Zero expected result
0.00
Zero reading before
0.10
Zero reading after
0.10
Span adjustment
1.00
Span Check
1.00
Deviation
0.00
Drift/Min
-0.08
Zero adjustment
-0.10
Zero check
-0.10
Deviation (Zero Drift)
0.00
Drift/min
0.01
Span Drift
-0.07
Actual measured
Concentration
67.13
Corrected concentration
for drift
67.82
Stack Conditions:
Average Temperature:
Average Pressure:
Average Oxygen:
Company Name: Road Binders Ltd
Licence No:
P0084-01
Year: 2015
Visit No: 1
Sampling Date:
12/16/2015
Report No:
015-166
Drift Correction Calculations
401.4
403.7
SOx
0.00
2.86
0.00
0.00
850
2.95
0.00
0.00
Page7of13
EPA Export 17-04-2016:00:48:47
Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
A1 Boiler
A
B
C
FBr
Smoke
3,0
3,0
3,0
3,0
3,0
3,0
3,0
7,0
7,0
3,0
7,0
7,0
7,0
7,0
7,0
7,0
7,0
7,0
0,0
0,0
0.591
0,5970
0,6000
0,6395
0,6265
0,6375
0,6160
0,6970
0,6725
0,6300
0,6175
0,6200
0,6200
0,6190
0,6655
0,6655
0,6655
0,6655
0,0
0,0
0.0011
0,0013
0,0013
0,0016
0,0021
0,0018
0,0015
0,0027
0,0024
0,0018
0,0025
0,0025
0,0025
0,0025
0,0028
0,0028
0,0027
0,0027
0,0
0,0
9.66
8,00
7,68
6,15
5,24
4,85
6,63
2,21
3,58
6,45
8,14
9,23
10,43
11,63
7,88
9,71
11,55
13,40
0,0
0,0
0,2182
0,2182
0,2182
0,2302
0,2302
0,2302
0,2302
0,2505
0,2450
0,2332
0,2314
0,2314
0,2314
0,2314
0,2404
0,2404
0,2404
0,2404
0,0
0,0
no
no
no
no
no
no
no
no
no
no
no
no
no
no
no
no
no
no
no
no
.
93.47
O2ref
se
6.53
Fuel Specific Factors
USA
CO2max
spot
no.
Natur. Gas
11,7
propane
15,12
butane
14,1
fueloil #2
15,70
fueloil #3
16,3
fueloil #6
16,7
kerosene
15,12
anthr. Coal
19,90
bitum. Coal
18,50
distill.#1
15,40
wood 10%
20,0
wood 20%
20,0
wood 30%
20,0
wood 40%
20,0
bark 15%
20,0
bark 30%
20,0
bark 45%
20,0
bark 60%
20,0
test gas
0,0
userfuel 1:2
0,0
ru
A1 Boiler
Fuel Specific Factor as per Testo 350 Manual
he
283 K
495 K
Note:
ot
0.6395
0.0016
6.15
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
A
B
C
of
Combustion Efficiency
for
en
t
loss (%)
Flue Gasses Records and Calculations
Marked Gas Oil
3.81
Ambient Temperature-AT
Fuel Gas Temperature-F
Stack ID
GEN2-002rev17
9/18/2015
QM
ns
Fuel Specific Factors:
Doc No
Rev Date:
Issued by:
Co
Fuel Type:
Oxygen measured
Road Binders Ltd
P0084-01
Visit No: 1
12/16/2015
015-166
Page8of13
EPA Export 17-04-2016:00:48:47
Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
Road Binders Ltd
P0084-01
Visit No: 1
12/16/2015
015-166
GEN2-002rev17
9/18/2015
QM
Doc No
Rev Date:
Issued by:
for
Flue Gasses Records and Calculations
A1 Boiler
Uncertainty calculation for Gaseous Measurement Oxygen EN14789
Performance characteristic
Standard deviation of repeatability at zero
Uncertainty
ur0
<0.3 % volume
<2% of volume / 24hr
<2% volume/24hr
<1% range flow
< 1.5 % rang pressure
<0.3% volumtemp
CO2 range
NO range
NO2 range
<2% range Voltage
< 0.1%vol /10 volt
< 2% of value
Value of uncertainty quantity
range of variation from conditions at calibration
min
max
value at calib
5
15
10 l/h
99.00
101
100 kPa
280
285
285 K
8
15
0 % vol
100
150
0 mg/m3
5
7.5
0 mg/m3
105
115
110 V
for mean
% vol
Only use rep at span
for mean
0.00
Standard deviation of repeatability at span level
urs
Lack of fit
ufit
0.08
Drift
u0dr
0.06
volume or pressure flow dependence
uspres
0.00
atmospheric pressure dependence
ambient temperature dependence
CO2
NO
NO2
Combined interference (from mcerts)
dependence on voltage
losses in the line (leak)
uapres
utemp
uleak
0.04
-0.02
0.05
0.01
0.00
0.08
0.03
0.04
Uncertainty of calibration gas
ucalib
0.01
Measurement uncertainty
Combined uncertainty
% of value
Coverage factor k =
2
Expanded uncertainty expressed with a level of conf
Expanded uncertainty expressed with a level of conf
3.81
0.14
3.62
uvolt
.
stdev
% vol
+/% vol at zero leve +/% vol at span leve+/% of fs / 10l/h
+- 5 l/h
% of fs/kPa
+- 2kPa
% by volume /10K
+- 15K
% by volume per
15
% by volume per
300
% by volume per
30
% range
% by volume /10V
+- 5%
% of value
% of value
<0.2 % range
<0.4 % range
se
0
0.14
0.1
0.00
0
0.3
-0.07
0.07
0.02
0
0.56
0.1
2
0.5
stdev
ru
Repeatability at span level
Deviation from linearity
Zero drift (during measurement period
Span drift (during measurement perio
volume or pressure flow dependence
atmospheric pressure dependence
ambient temperature dependence
CO2 (% vol)
15
NO (mg/m3)
300
NO2 (mg/m3)
30
Combined interference
Dependence on voltage
Losses in the line (leak)
Uncertainty of calibration gas
% by volume
% by volume
Effect of drift
0.10 % vol
0.40 % full scale
he
0.05
seconds
seconds
minutes
Assuming 1 minute collected over 1 hour
ot
Repeatability at zero
specification
< 200 s
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
Performance character
Value
Response time
145.00
Logger sampling interval
60
Measurement period
30
Number of readings in measurement
30
20.86 %vol
25 %vol
of
Calibration gas
Full Scale
en
t
%vol
3.81 %vol
ns
Limit value
n/a
Measured concentratio
Jul-08
Co
V2.2
Use largest of sum of all positive or all negative influences
0.06 all +ves
Criteria
0 all -ves
sum <2% value
0.06 largest
0.076173
Value to use for intereference uncertainty
uint
0.06
%vol
%vol
%
7.24 % of value
0.28 % vol
Page9of13
EPA Export 17-04-2016:00:48:47
Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
Road Binders Ltd
P0084-01
Visit No: 1
12/16/2015
015-166
GEN2-002rev17
9/18/2015
QM
Doc No
Rev Date:
Issued by:
for
Flue Gasses Records and Calculations
A1 Boiler
Uncertainty calculation for Gaseous Measurement NOx EN14792
Jul-09
0
0.3
0.00
-0.07
0
0
0.3
0.0
0.2
% of value
mg/m3
mg/m3
%of full scale/kPa
%of value /kPa
% full scale/10K
mg/m3
mg/m3
<2 % range
<2% range / 24hr
<2% range/24hr
<2 % / kPa flow
<3% / kPa pressure
<3% range / temp
NH3 range
CO2 range
H2O (% vol)
4
dependence on voltage
losses in the line (leak)
Converter efficency
Uncertainty of calibration gas
0.0
0.1
0.10
95.86
2
mg/m3
% full scale/10V
% of value
%
% of value
H2O range
<2% range Voltage
< 0.1%vol /10 volt
>95%
< 2% of value
Performance characteristic
Standard deviation of repeatability at zero
Uncertainty
ur0
Value of uncertainty quantity
Effect of drift
-0.01 mg/m3
0.00 % full scale
ranges
min
95.00
101.30
289
0
0
max
105
101.3
289
0
15
value at calib
100
101.3
289
0
0
kPa
kPa
K
mg/m3
%vol
.
Repeatability at span level
Deviation from linearity(lack of fit)
Zero drift
Span drift
volume or pressure flow dependence
atmospheric pressure dependence
ambient temperature dependence
NH3 (mg/m3)
3
CO2 (% vol)
5
273.00
1.00
1.00
0.00
se
<1 % range
<2 % range
101.30
0.00
1.00
0.00
0.02
ru
% full scale
% full scale
Factors
Uncertainty in factor
Correction Factor
0.00
1.00
1.00
0.01
he
seconds
seconds
minutes
3.81
0.35
1.05
0.02
1.05 uf
ot
specification
180.000
measured
Uncert
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
NO
408 ppm
408 ppm
2.053
0
93
0
121
for mean
mg/m3
use rep at span
for mean
0.00
0 %vol
110 V
of
3
837.624 mg/m (NO2)
Correction for reference conditions
O2, %
Moisture, %
Pressure, Temperature, K
ref
3.00
0.00
101.30
273.00
en
t
Performance character
Value
Response time
121.00
Logger sampling interval
60
Measurement period
30
Number of readings in measurement
30
Repeatability at zero
0.05
-3
837.624 mg.m (NO2)
ns
3
Limit value
350.00 mg/m (corrected Cal gas conc
Measured concentration 67.1333333 ppm
Measured concentratio
137.82 mg/m3 (101.3kPa,Full Scale
3
Measured concentratio
144.31 mg/m (Corrected)
Gas
NO/NO2 ratio
100.00
Full Scale
Cal gas conc
Conversion
Co
v4.0
Standard deviation of repeatability at span level
urs
Lack of fit
ufit
0.24
Drift
u0dr
-0.01
volume or pressure flow dependence
uspres
0.00
atmopsheric pressure dependence
0.00
ambient temperature dependence
uapres
utemp
0.00
NH3
uinterf
0.00
Use largest of sum of all positive or all negative influences
CO2 (% vol)
uinterf
0.36
H2O (% vol)
Dependence on voltage
losses in the line (leak)
uinterf
0.00
0.72
0.08
0.36 all +ves
Criteria
0 all -ves
sum <4% range
0.36 largest
2.756495
Value to use for intereference uncertainty
uint
0.36
Uncertainty of calibration gas
ucalib
uceff
uvolt
uleak
converter efficiency
Uncertainty in factor
Measurement uncertainty
Combined uncertainty
Expanded uncertainty k =
1.59
3.29
3.28
uf
2
Uncertainty corrected to std conds
Expanded uncertainty expressed with a level of conf
Expanded uncertainty expressed with a level of conf
Expanded uncertainty expressed with a level of conf
3.76
7.51
mg/m 3
mg/m 3
10.25
mg/m3
2.93 % ELV
-3
10.25 mg.m
Should be < 10% at ELV at standard conditions
7.10 % value
Page10of13
EPA Export 17-04-2016:00:48:47
Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
Road Binders Ltd
P0084-01
Visit No: 1
12/16/2015
015-166
GEN2-002rev17
9/18/2015
QM
Doc No
Rev Date:
Issued by:
for
Flue Gasses Records and Calculations
A1 Boiler
Uncertainty calculation for Gaseous Measurement SO2 EA M21
3
1154.582 mg/m
% full scale
% full scale
<1 % range
<2 % range
% of value
mg/m3
mg/m3
% of full scale/3 kPa
% of full scale/2 kPa
% full scale/10K
mg/m3
<2 % range
<2% range / 24hr
<2% range/24hr
<2 % / 3 kPa flow
<3% / 2 kPa pressure
<3% range / temp
N2O range
ranges
min
95.00
100.76
287
0
CO2 range
0
15
0 %vol
CH4 range
H2O range
<2% range Voltage
< 0.1%vol /10 volt
< 2% of value
0
0
93
57
1
121
0 mg/m3
0 %vol
110 V
0
0.13
-0.05
0.10
0.02
0.8
0.01
0.2
0.2
mg/m3
CH4 (mg/m3)
40
H2O (% vol)
20
dependence on voltage
losses in the line (leak)
Uncertainty of calibration gas
0.7
0.2
0.1
1
1.07
mg/m3
mg/m3
% full scale/10V
% of value
% of value
max
105
100.92
288.5
40
value at calib
100
100.88
287.5
0
Standard deviation of repeatability at span level
Value of uncertainty quantity
urs
for mean
mg/m3
use rep at span
for mean
0.00
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
Uncertainty
ur0
of
Performance characteristic
Standard deviation of repeatability at zero
Lack of fit
ufit
0.00
Drift
u0dr
-0.03
volume or pressure flow dependence
uspres
0.22
atmopsheric pressure dependence
0.28
ambient temperature dependence
uapres
utemp
0.00
N2O (mg/m3)
uinterf
0.23
CO2 (% vol)
uinterf
0.12
0.93 all +ves
CH4 (mg/m3)
uinterf
uinterf
0.58
0 all -ves
H2O (% vol)
Dependence on voltage
losses in the line (leak)
0.01
1.00
0.00
uvolt
uleak
ucalib
Uncertainty of calibration gas
Uncertianty in factor
Measurement uncertainty
Combined uncertainty
Expanded uncertainty k =
kPa
kPa
K
mg/m3
ot
Repeatability at span level
Deviation from linearity(lack of fit)
Zero drift
Span drift
volume or pressure flow dependence
atmospheric pressure dependence
ambient temperature dependence
N2O (mg/m3)
20
CO2 (% vol)
15
.
Effect of drift
-0.05 mg/m3
0.00 % full scale
se
specification
180.000
seconds
seconds
minutes
3.00
3.81
0.35
1.05
0.02
1.05
Moisture, %
Pressure, Temperature, K
0.00
101.30
273.00
273.00
0.00
101.30
1.00
0.00
1.00
1.00
1.00
1.00
0.01
0.00
0.00
uf
0.02
ru
0.00 mg/m3
Full Scale
3
0.00 mg/m (Corrected)
Performance character
Value
Response time
134.00
Logger sampling interval
60
Measurement period
30
Number of readings in measurement
30
Repeatability at zero
0
Correction for reference conditions
O2, %
ref
measured
Uncert
Factors
Uncertainty in factor
Correction Factor
en
t
Measured concentratio
Measured concentratio
-3
1154.582 mg.m
he
3
850.00 mg/m (corrected Cal gas conc
ns
Limit value
Jul-08
Co
V2.2
Uncertainty corrected to std conds
Expanded uncertainty expressed with a level of conf
Expanded uncertainty expressed with a level of conf
Expanded uncertainty expressed with a level of conf
0.93 largest
Value to use for intereference uncertainty
uint
0.93
Criteria
sum <4% range
0
0.00
0.00
uf
2
Use largest of sum of all positive or all negative influences
1.41
2.82
mg/m 3
3
mg/m
2.95
mg/m3
0.35 % ELV
-3
2.95 mg.m
Should be < 10% at ELV at standard conditions
#DIV/0! % value
Page11of13
EPA Export 17-04-2016:00:48:47
Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
Road Binders Ltd
P0084-01
Visit No: 1
12/16/2015
015-166
GEN2-002rev17
9/18/2015
QM
Doc No
Rev Date:
Issued by:
for
Flue Gasses Records and Calculations
A1 Boiler
Uncertainty calculation for Gaseous Measurement CO
3
501.75 mg/m
% full scale
% full scale
<1 % range
<2 % range
<2 % range
<2% range / 24hr
<2% range/24hr
<2 % / 3 kPa flow
<3% / 2 kPa pressure
<3% range / temp
N2O range
ranges
min
95.00
100.76
287
0
CO2 range
0
15
0 %vol
CH4 range
H2O range
<2% range Voltage
< 0.1%vol /10 volt
< 2% of value
0
0
93
57
1
121
0 mg/m3
0 %vol
110 V
0.07
0.9
0.20
0.00
0.02
0.8
0.01
0.2
% of value
mg/m3
mg/m3
% of full scale/3 kPa
% of full scale/2 kPa
% full scale/10K
mg/m3
0.2
mg/m3
CH4 (mg/m3)
40
H2O (% vol)
20
dependence on voltage
losses in the line (leak)
Uncertainty of calibration gas
0.7
0.2
0.1
1
1.07
mg/m3
mg/m3
% full scale/10V
% of value
% of value
max
105
100.92
288.5
40
value at calib
100
100.88
287.5
0
Standard deviation of repeatability at span level
Value of uncertainty quantity
urs
for mean
mg/m3
use rep at span
for mean
0.06
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
Uncertainty
ur0
of
Performance characteristic
Standard deviation of repeatability at zero
Lack of fit
ufit
0.00
Drift
u0dr
0.12
volume or pressure flow dependence
uspres
0.10
atmopsheric pressure dependence
0.12
ambient temperature dependence
uapres
utemp
0.00
N2O (mg/m3)
uinterf
0.23
CO2 (% vol)
uinterf
0.12
0.93 all +ves
CH4 (mg/m3)
uinterf
uinterf
0.58
0 all -ves
H2O (% vol)
Dependence on voltage
losses in the line (leak)
0.01
0.43
0.00
uvolt
uleak
ucalib
Uncertainty of calibration gas
Uncertianty in factor
Measurement uncertainty
Combined uncertainty
Expanded uncertainty k =
kPa
kPa
K
mg/m3
ot
Repeatability at span level
Deviation from linearity(lack of fit)
Zero drift
Span drift
volume or pressure flow dependence
atmospheric pressure dependence
ambient temperature dependence
N2O (mg/m3)
20
CO2 (% vol)
15
.
Effect of drift
0.20 mg/m3
0.04 % full scale
se
specification
180.000
seconds
seconds
minutes
3.00
3.81
0.35
1.05
0.02
1.05
Moisture, %
Pressure, Temperature, K
0.00
101.30
273.00
273.00
0.00
101.30
1.00
0.00
1.00
1.00
1.00
1.00
0.01
0.00
0.00
uf
0.02
ru
0.00 mg/m3
Full Scale
3
0.00 mg/m (Corrected)
Performance character
Value
Response time
132.00
Logger sampling interval
60
Measurement period
30
Number of readings in measurement
30
Repeatability at zero
0
Correction for reference conditions
O2, %
ref
measured
Uncert
Factors
Uncertainty in factor
Correction Factor
en
t
Measured concentratio
Measured concentratio
-3
501.75 mg.m
he
3
80.00 mg/m (corrected Cal gas conc
ns
Limit value
Jul-08
Co
V2.0
Uncertainty corrected to std conds
Expanded uncertainty expressed with a level of conf
Expanded uncertainty expressed with a level of conf
Expanded uncertainty expressed with a level of conf
0.93 largest
Value to use for intereference uncertainty
uint
0.93
Criteria
sum <4% range
0
0.00
0.00
uf
2
Use largest of sum of all positive or all negative influences
1.04
2.09
mg/m 3
3
mg/m
2.19
mg/m3
2.73 % ELV
-3
2.19 mg.m
Should be < 10% at ELV at standard conditions
#DIV/0! % value
Page12of13
EPA Export 17-04-2016:00:48:47
Company Name:
Licence No:
Year: 2015
Sampling Date:
Report No:
Road Binders Ltd
P0084-01
Visit No: 1
12/16/2015
015-166
GEN2-002rev17
9/18/2015
QM
Doc No
Rev Date:
Issued by:
for
Flue Gasses Records and Calculations
A1 Boiler
Uncertainty calculation for Gaseous Measurement CO2
14.99 %vol
14.99 %vol
Performance character
Value
Response time
134.00
Logger sampling interval
60
Measurement period
30
Number of readings in measurement
30
specification
seconds
< 200 s
seconds
minutes
Assuming 1 minute collected over 1 hour
Repeatability at zero
% by volume
% by volume
Performance characteristic
Standard deviation of repeatability at zero
Uncertainty
ur0
.
range of variation from conditions at calibration
min
max
value at calib
5
15
10 l/h
99.00
101
100 kPa
280
285
285 K
8
15
0 % vol
100
150
0 mg/m3
5
7.5
0 mg/m3
105
115
110 V
se
<0.3 % volume
<2% of volume / 24hr
<2% volume/24hr
<1% range flow
< 1.5 % rang pressure
<0.3% volumtemp
CO2 range
NO range
NO2 range
<2% range Voltage
< 0.1%vol /10 volt
< 2% of value
ru
stdev
% vol
+/% vol at zero leve +/% vol at span leve+/% of fs / 10l/h
+- 5 l/h
% of fs/kPa
+- 2kPa
% by volume /10K
+- 15K
% by volume per
15
% by volume per
300
% by volume per
30
% range
% by volume /10V
+- 5%
% of value
% of value
<0.2 % range
<0.4 % range
he
0.01
0.38
0.00
0.07
0
0.3
-0.07
0.07
0.02
0
0.56
0.1
2
0.5
stdev
ot
Repeatability at span level
Deviation from linearity
Zero drift (during measurement period
Span drift (during measurement perio
volume or pressure flow dependence
atmospheric pressure dependence
ambient temperature dependence
CO2 (% vol)
15
NO (mg/m3)
300
NO2 (mg/m3)
30
Combined interference
Dependence on voltage
Losses in the line (leak)
Uncertainty of calibration gas
0
Effect of drift
0.06 % vol
0.38 % full scale
Value of uncertainty quantity
for mean
% vol
Only use rep at span
for mean
0.00
Standard deviation of repeatability at span level
urs
Lack of fit
ufit
0.22
Drift
u0dr
0.03
volume or pressure flow dependence
uspres
0.00
atmospheric pressure dependence
ambient temperature dependence
CO2
NO
NO2
Combined interference (from mcerts)
dependence on voltage
losses in the line (leak)
uapres
utemp
uleak
0.03
-0.02
0.05
0.01
0.00
0.05
0.03
0.15
Uncertainty of calibration gas
ucalib
0.04
Measurement uncertainty
Combined uncertainty
% of value
Coverage factor k =
2
Expanded uncertainty expressed with a level of conf
Expanded uncertainty expressed with a level of conf
12.69
0.28
2.20
uvolt
co For
py in
rig sp
ht ect
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
Calibration gas
Full Scale
of
%vol
12.69 %vol
en
t
Limit value
n/a
Measured concentratio
ns
Jul-08
Co
V2.2
Use largest of sum of all positive or all negative influences
0.06 all +ves
Criteria
0 all -ves
sum <2% value
0.06 largest
0.253747
Value to use for intereference uncertainty
uint
0.06
%vol
%vol
%
4.40 % of value
0.56 % vol
Page13of13
EPA Export 17-04-2016:00:48:47
EPA: Licensee Return LR019303 for Cold Chon (Galway) Limited (P0056-01)
Licences
My Notifications
Manage My Users
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Licensee Return LR019303 for Cold Chon (Galway) Limited (P0056-01)
Home >> All Licences >> Cold Chon (Galway) Limited (P0056-01) >> All Licensee Returns
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Enter a short subject heading below for your return to the EPA:
Approval of Southern Scientific and Glenside
Date Received:
10/11/2015
Enter the details of your return to the EPA below:
Dear Helen,
Last year we used Southern & Anua. Southern intend to subcontract stack air emissions monitoring to Glenside Environmental this year. As you
may be aware Anua, the company we used last year, no longer provides this service.
Attached is the ISO 17025 Cert.
to
f c Fo
op r i
yr ns
ig pe
ht ct
ow ion
ne pu
r r rp
eq os
ui es
re o
d nl
fo y.
ra
ny
ot
he
ru
se
.
Glenside Environmental are on the EPA's Accreditation for Air Emissions Monitoring Contractors for Monitoring of Stack Emissions at EPA
Licensed Sites.
http://www.epa.ie/air/airenforcement/guidanceinrelationtoqualityofairemissionsdata/accreditationforairemissionsmonitoringcontractors/#.VkGkT9gnyUl
The process will be the same as last year, only that the emissions will be done by Glenside instead of Anua.
To Confirm;
- The on-site monitoring, laboratory analysis and reporting will be fully sub-contracted to Anua who has the mandatory ISO 17025
accreditation.
- The report by Southern Scientific, will clearly state that all aspects of the work were carried out by an ISO 17025 accrediated organiation.
Trusting that this will be to the satisfaction of the agency.
Co
ns
en
Thanks & Regards,
Carl Mooney.
Select the type of return you are making to the EPA:
Requests for Approval (RFA) and Site Reports
Select the sub-type of return:
Amendments to Monitoring
Category:
Air
Decision:
File Attachments:
Glenside INAB Scope 2015 - 322T Ed 2.pdf
EDEN - EPA, Johnstown Castle, Co. Wexford - Phone: +353 (0)53 9160600 | [email protected]
https://licensing.edenireland.ie/licence/p0056-01/docsubmission/display/lr019303[10/11/2015 08:10:48]
EPA Export 17-04-2016:00:48:47
EPA Incidents: Licensing Notice Details
Home >> All Licences >> Cold Chon (Galway) Limited (P0056-01) >> All Actions & Notices >> Licence Return Approval Notice
Licensing Notice Details
Subject
Licence Return Approval Notice
Created Date
13/11/2015
Dear Carl,
The Agency has reviewed your submission LR019303, “Approval of Southern Scientific and Glenside” in relation to air emissions
monitoring and agrees to the following:
The on-site monitoring, laboratory analysis and reporting will be fully sub-contracted to Glenside who has the mandatory ISO
17025 accreditation.
The report by Southern Scientific, will clearly state that all aspects of the work were carried out by an ISO 17025 accredited
organisation
ru
se
.
The Agency may at any time, if it considers necessary, revisit and/or revoke this approval. to
f c Fo
op r i
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ot
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Yours sincerely,
Helen Boyce, Inspector
Office of Environmental Enforcement, EPA, Castlebar
Co
ns
en
Tel: 094 90 48448
https://licensing.edenireland.ie/licence/p0056-01/sha/0ee65b83-0b8a-e511-a5db-0050568a69e2/print[16/02/2016 08:10:05]
EPA Export 17-04-2016:00:48:47
APAC Consulting Ltd trading as
Glenside Environmental
Cuil Greine House, Link Road, Ballincollig, Co Cork.
Testing Laboratory
ot
he
ru
se
.
Registration number: 322T
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is accredited by the Irish National Accreditation Board (INAB) to undertake
testing as detailed in the Schedule bearing the Registration Number detailed
above, in compliance with the International Standard ISO/IEC 17025:2005 2nd Edition
“General Requirements for the Competence of Testing and Calibration Laboratories”
(This Certificate must be read in conjunction with the Annexed
Co
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se
nt
o
Schedule of Accreditation)
Date of award of accreditation: 25:02:2014
Date of last renewal of accreditation: 25:02:2014
Expiry date of this certificate of accreditation: 25:02:2019
This Accreditation shall remain in force until further notice subject to continuing compliance
with INAB accreditation criteria, ISO/IEC 17025 and any further requirements specified by the
Irish National Accreditation Board.
Manager:
Chairperson:
Dr Adrienne Duff
Mr Tom O’Neill
Issued on 25 February 2014
Organisations are subject to annual surveillance and are re-assessed every five years. The renewal date on this
Certificate confirms the latest date of renewal of accreditation. To confirm the validity of this Certificate, please
contact the Irish National Accreditation Board.
INAB is a signatory of the European co-operation for Accreditation (EA) Multilateral Agreement (MLA) and the
International Laboratory Accreditation Cooperation (ILAC) Mutual Recognition Arrangement, for Testing.
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Wilton Park House, Wilton Place, Dublin 2, Ireland
Tel +353 1 607 3003 Fax +353 1 607 3109
E-mail [email protected] Web www.inab.ie
Schedule of
Accreditation
(Annex to Accreditation Certificate)
Site Laboratory:
Category D
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APAC Consulting Ltd trading as Glenside Environmental
Stack Emission Testing Laboratory
as they apply)
Telephone:
Cuil Greine House, Link Road, Ballincollig, Co Cork.
nt
o
(Address of other locations
se
Postal Address:
25-February-2014
Co
n
Initial Registration Date :
+353 (21) 4810016
Fax:
E-mail:
[email protected]
Contact Name:
Patrick Power
Facilities:
Public testing service
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Wilton Park House, Wilton Place, Dublin 2, Ireland
Tel +353 1 607 3003 Fax +353 1 607 3109
E-mail [email protected] Web www.inab.ie
Schedule of
Accreditation
Site Laboratory:
Category D
THE IRISH NATIONAL ACCREDITATION BOARD (INAB) is the Irish body for the accreditation of
organisations including laboratories.
Laboratory accreditation is available to testing and calibration facilities operated by manufacturing
organisations, government departments, educational institutions and commercial testing/calibration
services. Indeed, any organisation involved in testing, measurement or calibration in any area of
technology can seek accreditation for the work it is undertaking.
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Each accredited laboratory has been assessed by skilled specialist assessors and found to meet criteria
which are in compliance with ISO/IEC 17025 or ISO/IEC 15189 (medical laboratories). Frequent audits,
together with periodic inter-laboratory test programmes, ensure that these standards of operation are
maintained.
Testing and Calibration Categories:
Permanent laboratory calibration and testing where the laboratory is erected on a fixed
location for a period expected to be greater than three years.
Category B:
Site calibration and testing that is performed by staff sent out on site by a permanent
laboratory that is accredited by the Irish National Accreditation Board.
Category C:
Site calibration and testing that is performed in a site/mobile laboratory or by staff sent
out by such a laboratory, the operation of which is the responsibility of a permanent
laboratory accredited by the Irish National Accreditation Board.
Category D:
Site calibration and testing that is performed on site by individuals and organisations that
do not have a permanent calibration/testing laboratory. Testing may be performed using
Co
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Category A:
(a)
portable test equipment
(b)
a site laboratory
(c)
a mobile laboratory or
(d)
equipment from a mobile or site laboratory
Standard Specification or Test Procedure Used:
The standard specification or test procedure that is accredited is the issue that is current on the date of the most
recent visit, unless otherwise stated.
Glossary of Terms
Facilities:
Public calibration/testing service:
Commercial operations which actively seek work from others.
Conditionally available for public
calibration/testing:
Established for another primary purpose but, more commonly than not,
is available for outside work.
Normally not available for public
calibration/testing:
Unavailable for public calibration/testing more often than not.
Laboratory users wishing to obtain assurance that calibration or test results are reliable and carried out to the Irish
National Accreditation Board criteria should insist on receiving an accredited calibration certificate or test report.
Users should contact the laboratory directly to ensure that this scope of accreditation is current. INAB will, on
request, verify the status and scope.
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Scope of
Accreditation
APAC Consulting Ltd trading as Glenside
Site Laboratory:
Category D
Environmental
Stack Emission Testing Laboratory
Sampling
Total Particulate Matter
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0.11 to 50mg/m³
ru
.71
he
Gases and Aerosols
Standard specifications
Equipment/techniques used
ot
770
Type of test/properties
measured
Range of measurement
se
.
INAB Classification number (P9)
Materials/products tested
(with subsequent analysis by
EN 13284-1:2002
Isokinetic sampling
GEN3-001/GEN3-020
ISO 17025 accredited
.71
Sampling
Total Particulate Matter
ISO 9096:2003 Isokinetic
50 to 1000 mg/m³
sampling method
nt
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laboratory)
GEN3-001/GEN3-020
Co
n
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(with subsequent analysis by
ISO 17025 accredited
laboratory)
.04
Sampling and on-site
analysis
Carbon Monoxide
0.4 to 500 mg.m
-3
EN 15058:2006 by (NDIR)
Infra red analyser with
continuous analysis
GEN3-018
.04
Industrial fumes and
Oxygen O2
EN 14789:2005
mixtures
Range 0.1 to 21 vol%
Paramagnetic cell
Sampling and analysis
.04
Industrial fumes and
mixtures
GEN3-018
Oxides of Nitrogen (NO)
0.2 to 536 mg.m
-3
EN 14792:2006
Chemi-luminescence with
Sampling and on site
continuous analysis
analysis
GEN3-018
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Scope of
Accreditation
Site Laboratory:
APAC Consulting Ltd trading as Glenside
Category D
Environmental
Stack Emission Testing Laboratory
.04
Industrial fumes and
Oxide of Sulphur (SOx)
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mixtures
ru
Gases and Aerosols
Standard specifications
Equipment/techniques used
he
770
Type of test/properties
measured
Range of measurement
se
.
INAB Classification number (P9)
Materials/products tested
(with subsequent analysis by
Sampling
EN 14791:2005 extraction
and sampling.
GEN3-0016
ISO 17025 accredited laboratory
0.02 to 2000 mg.m-3)
Water Vapour
mixtures
4 to 40%
.71
EN 14789:2005
se
Gravimetric
3
(29 to 250g/m )
GEN3-003
Industrial fumes and
Pressure: Range 30 to 110 kPa
EN ISO 16911-1:2013
mixtures
Temperature: Range 0 to
L Type and S Type pitot
Sampling and analysis
1200°C
tube
Velocity: Range 3 to 26 m/sec
GEN3-019
Hydrogen Chloride
EN 1911:2010 extraction and
(with subsequent analysis by
sampling.
ISO 17025 accredited
GEN3-011
Sampling and analysis
.04
nt
o
Industrial fumes and
Co
n
.04
Sampling
laboratory)
(0.05 to 5000 mg.m-3)
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Scope of
Accreditation
APAC Consulting Ltd trading as Glenside
Site Laboratory:
Category D
Environmental
Stack Emission Testing Laboratory
Type of test/properties
measured
Range of measurement
Standard specifications
Equipment/techniques used
ISO 12039:2001
Gases and Aerosols
.04
Industrial fumes and
Carbon Dioxide
mixtures
0.1 to 15%
he
ot
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Sampling and analysis
.04
ru
770
se
.
INAB Classification number (P9)
Materials/products tested
with continuous analysis
GEN3-018
Industrial fumes and
Sulpher Dioxide
TGN M21
mixtures
0.3 to 1150 mg.m-3
By (NDIR) Infra red analyser
nt
o
Sampling and analysis
with continuous analysis
se
GEN3-018
Co
n
.04
By (NDIR) Infra red analyser
Industrial fumes and
Total Gaseous Organic Carbon
IS EN 12619:2013-11-21
mixtures
1.6 to 642 mg.m-3
By flame ionisation
Sampling and analysis
detector.
GEN3-013
.71
Sampling
Dioxins and Furans
IS EN 1948:2006 Isokinetic
(with subsequent analysis by
sampling.
ISO 17025 accredited
GEN3-021
laboratory)
(0.005 to 0.3 ng l-TEQ.m-3)
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Scope of
Accreditation
APAC Consulting Ltd trading as Glenside
Site Laboratory:
Category D
Environmental
Stack Emission Testing Laboratory
Type of test/properties
measured
Range of measurement
Standard specifications
Equipment/techniques used
770
Gases and Aerosols
Metals
IS EN 14385:2004 Isokinetic
.71
Sampling
(with subsequent analysis by
sampling.
ru
se
.
INAB Classification number (P9)
Materials/products tested
GEN3-014
ot
he
ISO 17025 accredited
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laboratory)
(0.005 to 0.5 mg.m-3)
Sampling
Mercury
IS EN 13211:2011 Isokinetic
(with subsequent analysis by
sampling.
ISO 17025 accredited
GEN3-014
nt
o
.71
Co
n
se
laboratory)
(0.005 to 0.5 mg.m-3)
.71
Sampling
VOC’s Speciated (carbon
IS EN 13649:2002 extraction
and other suitable tubes)
and sampling.
(direct sampling of dry
GEN3-010
stacks only)
Mercaptans
Amines and Amides
Phenols
Cresols
Carboxylic Acids
Aldehydes
(with subsequent analysis
by ISO 17025 accredited
laboratory)
(0.09 to 2000 mg.m-3)
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Scope of
Accreditation
APAC Consulting Ltd trading as Glenside
Site Laboratory:
Category D
Environmental
Stack Emission Testing Laboratory
Standard specifications
Equipment/techniques used
IS EN 14791:2005 extraction
Gases and Aerosols
Ammonia (with subsequent
.71
Sampling
analysis by ISO 17025
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770
accredited laboratory)
se
.
Type of test/properties
measured
Range of measurement
ru
INAB Classification number (P9)
Materials/products tested
and sampling.
GEN3-004
-3
Co
n
se
nt
o
(0.25 to 2000 mg.m )
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