Applied Physics Research; Vol. 5, No. 4; 2013 ISSN 1916-9639 E-ISSN 1916-9647 Published by Canadian Center of Science and Education Process Anatomy for High Aspect Ratio Micro-Hole Drilling with Short Micro-Second Pulses Using a CW Single-Mode Fiber Jay Tu1, Ted Lehman1, Alexander G. Paleocrassas1, Wm. Ray Harp1, Satoru Noguchi2 & Etsuji Ohmura2 1 Department of Mechanical and Aerospace Engineering, North Carolina State University, EBIII, Raleigh, NC, USA 2 Division of Materials and Manufacturing Science, Graduate School of Engineering, Osaka University, 2-1 Yamada-oka, Suita, Osaka, Japan Correspondence: Jay Tu, Department of Mechanical and Aerospace Engineering, North Carolina State University, EBIII, Raleigh, NC 27695, USA. E-mail: [email protected] Received: May 14, 2013 doi:10.5539/apr.v5n4p1 Accepted: June 13, 2013 Online Published: July 1, 2013 URL: http://dx.doi.org/10.5539/apr.v5n4p1 Abstract The objective of this paper is to establish a detailed process anatomy of a micro-hole drilling process using a CW single-mode 300 W fiber laser with short micro-second pulses. For the drilling process with a one micro-second laser pulse, the process started with drastic evaporation and concluded with melt ejection approximately 150 micro-seconds later. It was concluded that two distinct hole drilling mechanisms occurred, one as adiabatic evaporation by the high power initial spike of the laser beam and one as melt ejection by the low power laser energy deposition. The drilling process time line was established based on the measurements by several in-process sensors, such as photodiodes, a high-speed camera, and a spectrometer. The theoretical modeling zoomed in the early stage of the process to investigate the hole formation which could not be observed experimentally. Both experimental and theoretical results were then compared to determine the laser-material interaction mechanisms among three media involved in the process: laser, material, and vapour/plasma. Finally, a series of temporal anatomy diagrams, denoted as process anatomy, were presented to describe the entire drilling process, including process temperature, laser energy deposition, hole formation, and material removal mechanisms. Keywords: micro-hole drilling, laser ablation, microsecond pulse, fiber laser, melt ejection 1. Introduction Laser drilling is an important industrial process to produce various sizes of holes for critical applications, such as cooling holes in turbine components. Typical laser pulse durations for laser drilling are in the nano-, pico- and femto-second ranges. Ultra-short-pulse lasers operate in the femto-second (10–15 sec) (fs) or pico-second (10–12 sec) (ps) ranges to produce peak power density in the range of 10–1,000 GW/cm2. The holes produced with ultra-short pulses usually exhibit a clean finish because melting is not significant. However, the Material Removal Rate (MRR) is usually very low, for example, in the range of 10–200 nm/pulse for steels with a Ti: Sapphire femto-second laser (Bauerle, 2000). Breitling et al. (2004) presented fundamental aspects in machining of metals with short and ultra-short laser pulses. Mao et al. (2007) presented detailed high speed photography images of laser ablation mechanisms using short and ultra-short laser pulses. The micro-hole drilling process using nanosecond (10–9 sec) (ns) pulses usually produces holes in metal with acceptable quality, but, in general, worse than those by ultra-short lasers because melting is more significant. The material removal rate is usually in the order of 1–10 μm/pulse. The power density of these lasers is in the range of GW/cm2. Laser drilling using long pulses in the range of several hundred microseconds (10–6 sec) to several milliseconds (10–3 sec) rely on mostly on melting to remove material because their power densities typically are below 107 W/cm2. The hole quality is usually low and the hole diameter is large due to significant melting. For example, in the experiments presented in Low and Li (2002) and Low et al. (2004), a Q-switiched 400W Nd:YAG laser was used to produce a pulse at 1.0 ms, with pulse energy up to 7 J and peak power over 7 kW. Using multiple pulses and with O2 as the assist gas, it could drill through a 2.5 mm stainless steel plate with a hole diameter approximately 600 μm. Similarly, Pandey et al. (2006), with a similar laser, conducted laser drilling with pulse durations ranging from 490 to 890 μs, pulse energy 0.5 J, and argon gas as the assist gas. Kayukov et al. (1998) 1 www.ccsenet.org/apr Applied Physics Research Vol. 5, No.4; 2013 applied a single pulse from an Nd:YAG laser for up to 40 J in energy and 20 ms in pulse duration, with 3–5 kW peak power, to drill blind holes in different metals. For chromium steel, they achieved 6.5 mm deep blind hole with a single pulse at 17.5 J with a power density below 106 W/cm2. The blind hole demonstrated a large opening similar to a nail head shape over 1 mm in diameter and an average waist diameter about 300 μm. In summary, the laser drilling process can be evaporation dominated or melting dominated depending on the pulse duration. In comparison, the body of work regarding short microsecond laser drilling/ablation is small. It is expected that the evaporation and melting both play an important role in the short microsecond drilling process. It is the objective of this paper to establish the drilling mechanisms and the temporal characteristics of the short microsecond drilling process, to be depicted in a series of diagrams, denoted as process anatomy. This paper is organized as follows. First, the time line of the short microsecond drilling process is established based on the measurements of several in-process sensors, including photo-diodes, a high speed camera, and a spectrometer. Theoretical modeling is then used to zoom in the early hole formation stage which cannot be observed experimentally. Both experimental and theoretical results are then compared to determine the laser-material interaction mechanisms. Finally, a series of temporal anatomy diagrams, denoted as process anatomy, are presented to describe the entire drilling process by a one micro-second laser pulse. The body of a manuscript opens with an introduction that presents the specific problem under study and describes the research strategy. 2. Review of Short Microsecond Pulse Drilling Garnov et al. (2004) performed laser ablation using pulse durations between 150 ns and 4.5 μs on samples of stainless steel, aluminum, alumina ceramics, and graphite with a Q-switched Nd:YAG laser that used an optical fiber as part of the resonator to produce the desired pulse length. They reported an MRR at 11 μm/pulse with a power density of 20 MW/cm2 and pulse duration of 4.5 μs for stainless steel. The advance of laser technology in the last decade has produced many high power lasers with very high beam quality. For example, Trippe et al. (2004) used a Q-switched Nd:YAG slab laser to produce pulses between 30 μs and 150 μs with power densities up to 220 MW/cm2. With a single pulse, they drilled holes in steel with diameters between 80 μm and 120 μm and depths from about 120 μm to 700 μm with argon gas. Their experimentally determined drilling speed was reported as 6 m/s. They also presented a dimensionless 2D model of free boundary problem and they computed the time for vaporization to be approximately 100 nanoseconds. Kreutz et al. (2007) applied this drilling technique to drill cooling holes in turbine components with multiple pulses (percussion drilling) combined with oxygen, helium, and argon assist gasses. Walther et al. (2008) combined the above Nd:YAG slab laser and the DPSS Nd:YAG laser to achieve very high aspect ratio percussion drilling (5 mm through holes with 170-180 μm waist diameter). Walther et al. (2008) utilized a flash lamp pumped Nd:YAG slab laser (FM015, LASAG) with a beam quality as M2 = 2 and it can produce pulses with durations from 100 to 500 μs and a laser energy of 0.64 J. This excellent beam quality allows a focus spot size 45 μm in diameter, producing a power density of 220 MW/cm2, as compared with M2 = 22-38, 600 μm spot size, and approximately 3 MW/cm2 for the laser used in Low and Li (2002) and Voisey et al. (2002). Walther et al. (2008) also utilized a diode-pumped solid state (DPSS) Nd:YAG laser (Powergator 1064, Lambda Physik) which has a beam quality of M2 = 1.7, with a spot size of 42 μm, 17 ns pulse, and 1.8 mJ pulse energy, producing a power density over 20 GW/cm2. Most interestingly, the development of high power, single-mode fiber laser has established a new level of beam quality. For example, Harp et al. (2008) conducted micro-hole drilling with a 300 W, CW, Yb-doped fiber laser (YLR-300, IPG), which has a near perfect beam quality M2=1.04 and the beam can be focused down to 10 μm with a 100 mm lens. It can also be modulated to produce pulses from 1 μs to any length of pulse duration. The modulated pulses all contain an initial spike at 1,500 W, followed by a constant power at 300 W, to reach a peak power density of 1.9 GW/cm2 and 380 MW/cm2 at the steady state. In comparison with ns-, ps-, and fs-lasers, the peak power of this modulated fiber laser pulse is low but its excellent beam quality allows for tight focusing to reach very high power density. The feasibility of laser drilling with such a CW laser via modulation control was demonstrated by Harp et al. (2008), in which pulses from 15–40 μs were used to produce holes with diameters from 40 to 100 μm and depths from 25 to 50 μm. This work indicated that, by using high beam quality lasers, micro-hole drilling with pulse durations in the short microsecond range (1–10 μs) has become feasible for applications which require moderate material removal depth per pulse, narrow opening (due to much smaller beam spot sizes), and moderate hole quality (due to moderate melt ejection). In this paper, we focus on a single pulse drilling process of blind holes on a stainless steel substrate with pulse 2 www.ccsennet.org/apr Applied Physics Researrch Vol. 5, No.4; 2013 durations oof 1–8 μs usinng a 300 W, C CW single-modde fiber laser. IIn this study, tthe micro-holee drilling techn nique investigateed in Harp et al. a (2008) has been greatly eextended and it is now posssible, with a siingle 1 μs pulsse, to produce a blind hole 1677 μm in depth aand 19 μm in tthe opening diameter on a 0..8 mm stainlesss steel plate. 3. Summaary of Experim mental Resultts 3.1 Profilees of Modulateed Fiber Laser Pulses A continuuous-wave, sinngle-mode, Ybb-doped fiber llaser (YLR-3000, IPG) was used to drill bblind holes on n 316 stainless ssteel plates (S SUS 316). Thhis laser emittted a beam w with a waveleength of 1,0775 nm and a CW, steady-statte power outpuut of 300 W. IIn this study, aan external conntrol circuit waas developed w with a capabiliity of modulatingg laser pulsess with duratioons from 1 μ μs to 1 s. Thiis laser moduulation controll is different from Q-switchinng as the laser power remainns constant whiile the depositeed energy is deetermined by tthe pulse durattion. The moduulated pulse off the laser wass measured byy an InGaAs pphotodiode (Thhorlabs 410/M M) through a 10 0 μm pinhole to avoid saturatiing the photoddiode. An osciilloscope (Tekktronix 3012 B B) with a 100 M MHz sampling g rate was used tto measure the signal from thhe photodiode and to determ mine the actual laser pulse durration. Figure 1 illlustrates the measured m profi files of the 1-μ μs and 15-μs laaser pulses. Foor the 1-μs pullse, the laser power initially risses to about 1,,500 W at 500 ns and then faalls to the steaady state value of 300 W afteer 1 μs. The ov verall pulse graddually decays to zero after 110 μs. For thee 15-μs pulse, the same initial spike and the same deca aying pattern at the end of thee pulse are obsserved. Howevver, the laser ppower reboundds to about 5000 W after 1 μss and then settles to the steadyy state power oof 300 W for ann additional 144 μs. The initiaal spike was m marked by a red d line in a zoom--in plot in Figuure 1. Laser pulse proofiles of the 1--s and 15-s pulses. Both ppulses have an identical initiaal spike at 1,50 00 W Figure 1. L whhich is approxximately five tiimes of the steaady state valuee of 300 W 3 www.ccsennet.org/apr Applied Physics Researrch Vol. 5, No.4; 2013 Figure 2. Hole ggeometry by thhe 1, 2, 4, 5, annd 8 microsecoond pulses 3.2 Micro--Hole Geometrry Typical prrofiles of microo-holes producced by a singlee pulse with puulse durations at 1, 2, 4, 5, aand 8 s are sh hown in Figure 22. For the hole produced byy the 1 s pulsse, the diameteer of the hole is 18.9 m annd the depth of o the hole is 1666.7 m, equivvalent to an asppect ratio of 88.8. The result of Figure 2 iss a significant improvement over the previoous results repoorted in Harp et al. (2008). Overall, the eexcellent holee profile and thhe narrow ope ening diameter is mainly due to the excellennt beam qualitty of the singlle-mode fiber laser. It is cleaar that longer laser pulses prooduce deeper holes h while thee hole diameteer does not inccrease substanttially. The mellt ejection beco omes less effecttive when the hole depth reaaches 200 m as hole openiing blockage sstarts to appeaar. With 5 and 8 s pulses, thee hole is complletely blocked.. 4. Time Line of the Driilling Process with a Short M Micro-Second d Pulse 4.1 The Fiirst 5 Microsecconds Two silicoon photodiodees (Hammatsuu S1336-18BQ Q) were usedd to measure the intensityy evolution off the vapour/plaasma plume whhen the laser w was irradiated oon the substratte. The responnse time of thiss photodiode iss 5 ns. A tube waas placed arouund the photoddiode sensors iin order to aim m at the vapouur plume preccisely. A short-pass filter (Thoorlabs FES09000) was placed in front of thee photodiodes to cut off raddiations above 900 nm so tha at the laser radiaation (1075 nm m) would not aaffect the meassurement of thhe plasma radiaation. Two photodiodes arra anged at differennt angles were used, one at a steep angle aand one paralllel to the platee. The photodiiode measurem ments and the lasser beam tempporal profile w were shown in F Figure 3. The laser pulse staarted at t = 0, aand rapidly rea ached its peak poower at about 500 ns. The vapour/plasma signal was firsst detected at 2200 ns. This ddelay was related to the laser/m material interacction time neeeded to evaporrate and dissoociate the mateerial from the solid phase to o hot vapour/plaasma. This obsservation is coonsistant with tthe result repoorted by Trippee et al. (2004), in which the time needed to cause evaporration is foundd to be 100 nns. The vapour/plasma conntinued to groow in intensity y and reached too its peak at abbout 600-800 nns. After the ppeak, the vapouur/plasma inteensity decreaseed to nearly ze ero at 2.8 μs as indicated by the silicon phhotodiode paraallel to the pllate, while som me spurts of iintensity were e still registered by the steep angle a photodiode. This was bbecause the steeep angle phottodiode could oobserve the plasma trapped insside the hole. At A this time, thhe laser powerr dropped below w 200 W. Anoother observatiion based on Figure 3, was thaat, under the cuurrent setup, laaser power lesss than 200 W was not capabble of producinng a vapour/plasma with intennsity high enouugh to be regiistered by the parallel photoodiode. After 5 μs, the laserr power dropped to below 1000 W and downn to zero afterr about 10 μs. One reason fo for this is probbably not due to the steep cavity which wass already form med so that the incident anglee of the laser bbeam to the suubstrate is far from 90 degre ees to reduce thee energy absorpption efficiencyy. 4 www.ccsennet.org/apr Applied Physics Researrch Vol. 5, No.4; 2013 Figure 3. V Vapour/plasmaa and laser intennsity measurem ments 4.2 Entire Process Time Line Although tthe photodiodees could not detect any signaals after aboutt 10 μs, it did nnot mean the ddrilling processs had completedd. To observe the t entire drilling process, a high speed ccamera was uused. The fram me rate of this high speed cam mera was 40,5000 frames/secoond; thus, the time interval between each frame was 244.6 μs. The camera was startedd before the laaser radiation aand took contiinuous frames of images throoughout the drrilling process. The high speedd photographyy images were shown in Figuure 4. If we seet the start of the laser pulse as t = 0, the e first image of F Figure 4 occurrred some timee between 0 too 24.6 μs becaause the camerra was not synnchronized with the start of thee laser radiatioon. We denoted the first fram me time as t1, as shown in F Figure 4 and 0<t1<24.6 μs. In the first framee, a coherent white w flash starrted. Similar w white flash wass also observedd in frames #22 to #4, which is 72 μs later. Inn the first four frames, the CC CD sensor of tthe high speedd camera was oobviously satuurated. At fram me #5, the white flash reduced to be gray andd became fainnter in frames #6 and #7, 1444 μs later. It w was not clear if i the white flashh in frame #1 is the high inntensity vapouur/plasma obseerved in Figurre 3. Note thatt the high inte ensity vapour/plaasma in Figure 3 was no loonger detectabble by the phootodiodes afteer 3 μs when the vapour/plasma intensity bbecame too low w to be registerred by the phootodiodes. How wever, the intennsity of the vaapour/plasma might m be too low w for photodioodes after 3 μss, it was still sstrong enough to saturate thhe CCD sensorr of the high speed s camera. Because similarr saturated white flashes werre still observeed in frames ##2–#4, it was m most likely tha at the first framee did not captuure the high inntensity vapouur/plasma indiccated in Figuree 3. As shownn in the red va apour intensity liine in Figure 4, 4 the vapour/p /plasma was veery intensive w within the firsst 3 μs, it then decayed gradually into weakeer vapour and disappeared after almost 100 μs. In the seecond frame (t = t1 + 24 μs, w where t1 is the time for the firrst frame), ejeection of particcles could be seen, which continued in tthe subsequennt frames. Partticles became visible in framess #6 and 7. 5 www.ccsennet.org/apr Applied Physics Researrch Vol. 5, No.4; 2013 Figuure 4. High speeed images of tthe vapour prooduced during laser drilling Based on F Figure 4, the laser l pulse waas completed inn 10 μs but the entire drillinng process did not complete until more thann 144 μs laterr. Due to the existence of vvapour long aafter the laser pulse, we had to conclude e that significantt melting occuurred and the white flashes captured by the high speeed camera werre low temperrature vapour hovvering over moolten metal. Thhe rise and deccay of the vapoour/plasma waas plotted in Fiigure 4 in a red d line under the hhigh speed cam mera images. 4.3 Spectrooscopic Analyssis of the Initiaal Vapour/Plassma A spectrom meter was used to characteriize the hot vappour/plasma aat the beginninng of the proceess. Three diffferent tests were conducted forr producing diifferent vapourr/plasma conditions, which iincluded the single pulse driilling at 1,500 W and 1050 W, as well aas CW weldinng at 1 mm/s at 300 W. F For the first ttwo cases, the e hot vapour/plaasma was not at steady statee but expandinng. Measuring expanding plaasma was diffiicult and very poor signal to nnoise ratio wass expected. Wee did not preseent detailed infformation of thhe spectrometeer measuremen nts in this paper because of paage limit. Tabble 1 listed thee calculated peak vapour/plaasma temperaature based on Cr I spectral linnes to reduce errors e due to seelf-absorption.. It is impoortant to note here that thee error listed was estimateed based on tthe uncertaintyy in the transsition probabilitiies of some off the chromium m lines. The eerror representted the worst case scenario,, assuming tha at the transition pprobabilities of o the lines werre off by the m maximum amouunt. Table 1. Ellectron temperratures (in Kelvin) calculatedd from Boltzm mann plots (95 % confidence level) Usiing Cr I lines 1 µs pulsing, 1,500 W 43,611 ± 27,623 1 µs pulsing, 1,050 W 29,482 ± 12,624 1 mm/s weldding, 300 W 8,290 ± 998 Accordingg to Table 1, with w 95% confiddence level, thhe plasma tempperature at the quasi-static w welding conditiion at 300 W waas estimated to t be 7,000 too 9,000 K. The peak tempperature of thee expanding vvapour/plasma was estimated to be betweenn 17,000–42,0000 K at a peakk power of 1,0550W and 16,000 K–71,000 K at 1,500 W peak 6 www.ccsenet.org/apr Applied Physics Research Vol. 5, No.4; 2013 power. Based on the results of Table 1, we can conclude that a hot vapour/plasma over 16,000 K and as high as 71,000 K did exist in the first 1 μs of the process during the laser initial spike. Note that even at the highest temperature estimated in Table 1, the vapour/plasma was still optically thin with respect to the fiber laser wavelength of 1075 nm. Therefore, the study of Table 1 also allows us to conclude that the laser beam did not heat the vapour/plasma and nearly all laser energy was used to either evaporate or to melt the material. The vapour temperature measured for the steady state welding condition at 300 W indicated that a weaker vapour at temperature between 7,000 to 9,000 K could exist at the later stage of the drilling process. 4.4 Melt Ejection and the Expanding Vapour/Plasma The existence of a high temperature vapour/plasma indicates that its pressure would be high as well. Because the micro-hole was covered by this high temperature and high pressure plasma, the melt is likely to be superheated in the early stage of the drilling process. As the vapour/plasma cooled down to weaker vapour (after at least 24 microseconds), the pressure also dropped. The drop of pressure could cause the superheated melt to boil and to eject as fine droplets as seen in the high speed images of Figure 4. 5. The Hole Formation Simulation during the First One Microsecond Figures 3 and 4 provide the timeline of this drilling process; however, the actual hole formation could not be observed directly. Therefore, computer simulation based on a 3D finite-element thermo-hydrodynamic model was used to study the hole formation due to evaporation by the initial laser spike. 5.1 3D Finite-Element Thermo-Hydrodynamic Model This 3D finite-element based thermo-hydrodynamic model accounts for the effect of multiple reflections inside the cavity, the movement of the liquid-vapour interface in time, the effect of recoil pressure on the liquid-vapour interface and the mass loss by evaporation during the drilling process (Ohmura & Noguchi, 2010). The model contained the continuity, Navier-Stokes and energy equations: v 0 v v v p 2 v F t k H v H H w c t p (1) (2) (3) where v was the velocity vector of the material in the molten state, ρ was the density of the material, p was the pressure, μ is the material viscosity, F comprised the body force vector for all the recoil pressure force and the surface tension force at work on an element of material, H was the enthalpy, k was the thermal conductivity, cp was the specific heat and w is the source term which was the heat input into the system by the laser. The computational domain (Figure 5) was a 3D rectangular domain with the z axis parallel to the axis of propagation for the laser beam and the x-y plane parallel to the material surface. The bounds of the domain are: x(-42 m, +42 m), y(-42 m, +42 m), z(-180 m, +30 m). The plane z = 0 was considered the surface of the material and the point (0, 0, 0) was the center of the laser beam where it irradiated at the surface (see Figure 5, indicated by a blue dot). The whole domain is at the room temperature as the initial condition and the boundaries of the domain remain at the room temperature during the simulation. The laser beam was considered to be Gaussian in space. A triangular function was used to approximate the actual laser pulse shape (the red profile in Figure 1) so that only the effect of the initial spike was simulated. The conditions at the material boundaries were considered to be insulated with zero flow velocity. The model used a volume of fluid (VOF) method for handling of the liquid-vapour interface by computing the volume fraction of liquid, F, in each element. The range of F was from 0 to 1, with a value of 0.5 indicating that the element was an interface element. As the interface position was calculated, the normal vectors to the surface were determined and used to compute the angle of reflection for the surface. Using the Fresnel equation, the reflection coefficient was determined for each surface and the amount of reflected energy was calculated. 7 www.ccsenet.org/apr Applied Physics Research Vol. 5, No.4; 2013 Figure 5. Computational domain It was also assumed that, when the surface material was vaporized, the vaporized mass carried energy with it and traveled away from the surface. The amount of mass vaporized was calculated using an energy balance along the surface of the material. t t t t t t k H S c p n Qdt mv dSdt Lv Sin (4) where mv was the mass of the vaporized material, Q was the laser power absorbed at the surface area S and Lv was the latent heat of vaporization. As the vaporized mass traveled away from the surface, it generated a recoil pressure on the surface. To calculate the recoil pressure generated by the vaporization of the material, the recoil pressure, pr, was determined as the mass evaporated per unit area per unit time multiplied by the velocity of the vapour: pr mv vT St (5) where vT was the vapour velocity at the edge of the Knudsen layer and was defined by Anisimov et al. (1971) as one-quarter of the square mean velocity: vT 1 8kbTd 4 ma (6) where Td was the surface temperature and ma is the atomic mass of the vapour. This generated recoil pressure created a force on the surface of the material and acted against the surface tension force. These two forces acted as surface forces, whereas the momentum equation (Equation 2) required the input to be body forces. To convert the surface forces to body forces a continuum surface force (CSF) model was used (Brackbill, 1992). The pressure-correction method for the flow velocity-pressure coupling used was the Simplified Marker-And-Cell (SMAC) method by Harlow and Amsden (1971). The algorithm for the model involved a series of steps. The first step was to calculate the normal vectors for the surface. Next, the surface forces were converted to body forces through the CSF method and used in the momentum equation, which was solved with the continuity equation through the SMAC method. The volume liquid fraction was then determined for the elements and the multiple reflections were calculated for the walls of the hole. The energy absorbed at the 8 www.ccsennet.org/apr Applied Physics Researrch Vol. 5, No.4; 2013 surface waas used as the input source inn the energy eqquation, in whhich the enthalppy was compuuted. The vaporized mass and the recoil preessure were thhen calculatedd. The time sttep was then advanced andd the computa ations re-perform med until the siimulation was completed. In summarry, this model assumes that eenergy couplinng between thee laser and the material was mainly through the Fresnel abbsorption. The absorption beccame more effficient as the caavity forms, w which allowed m multiple reflec ctions of the laseer beam. Whenn the material was removedd by the evapooration processs, only a portion of the abso orbed energy waas conducted away a in the rradial directionn. Some laserr energy used to induce meelting in the radial r direction ccould be reclaiimed by the addvance of the ccavity as an addiabatic evapooration processs. In other words, if a material mass was evaaporated due too the irradiatioon of a laser beam with a veery high powerr density, this mass could be suuper-heated annd dissociated into plasma, cconsistent withh the measurem ments discussedd in Section 4. 5.2 Hole F Formation Simulation Figure 6 illlustrates the formation f of thhe hole in diffferent time stepps by the simuulation. The siimulation cond dition matched thhe experimenttal condition uusing a 1-s ppulse as show wn in Figure 1,, except that tthe pulse proffile is simplified as the red linne profile in F Figure (1). In tthis simplifiedd profile, the ppulse drops to zero at 1 s. This profile waas used to studyy the effect off the initial spike alone. The hole was seenn to form very quickly during the laser pulsee, but stopped abruptly whenn the pulse ennded at 1 s. T This result wass due to a simpplified laser prrofile was used and only evvaporation wass considered as the material removal m mechanism byy this model. The contributioon of the moddel is its abilitty to show thee evolution off the hole form mation via adiaabatic evapora ation, which is nnot observable via experimenntation. Figure 6. Holee formation byy adiabatic evaaporation by sim mulation t opening diiameter of the hole did not cchange after 5500 ns, which indicated that little Accordingg to Figure 6, the heat transffer occurred inn the radial ddirection once the hole was established. T This could alsso be explaine ed by multiple reeflections as shown s in bottoom figures in Figure 6. Oncce the hole became sufficienntly deep, the laser energy waas reflected to the t bottom of tthe cavity to fuurther deepen tthe hole. Another innteresting obseervation of Figgure 6 was thaat the majorityy of material rremoval by adiiabatic evaporration was complleted by 750 ns. n Because thee evaporated m material receivved a large amoount of laser eenergy deposite ed by the initial laser spike, it i was dissociaated into hot plasma, as coonfirmed in Section 4.3. Thhis result was also consistent with the meassurement of vaapour/plasma inntensity whichh peaks at abouut 600 to 800 nns (Figure 3). 5.3 Data aand Model Com mparison The experiimentally obtaained hole had a depth of 166.7 m, an opening diameteer of 18.9 m, and an aspect ratio of 8.8 (Figgure 2). In com mparison, the simulation prooduced a hole with a depth of 50 m, a ddiameter of 27 7 m, and an asppect ratio of 1..8. Therefore, the simulationn produced a hhole wider andd shallower thaan the experim mental result. As the model coonsidered onlyy the adiabaticc evaporation, the discrepanncy between thhe experimentt and simulationn indicated thee important rolle of other meechanisms negglected by the model, such aas the laser en nergy deposited after 1 s, melt ejection, expplosive boilingg, and the enerrgy re-radiatedd by the vapouur/plasma. With h this comparisoon, the adiabatiic evaporation mechanism iss estimated to ccontribute to abbout 1/3 of thee material remo oval. 9 www.ccsennet.org/apr Applied Physics Researrch Vol. 5, No.4; 2013 Figurre 7. Volumetrric removal ratte comparison Figure 7 pplots the Volum metric Materiaal Removal R Rate (VMRR) during the earrly hole formaation. To provide a comparisoon, a one-dimennsional drillingg model by voon Allmen and Blatter (1995)) was used to ccalculate its VM MRR. This modeel assumes thaat adiabatic evvaporation occcurs at the botttom of a cylinndrical volumee; thus, there is no heat transffer in the radiaal direction. Baased on this moodel, the drillinng speed equattion is: u Ia Vd H (Td ) H LV (7) where Ia w was the absorbed power denssity, Vd is the molar volumee, ΔH(Td) was the enthalpy nneeded to reach the surface tem mperature Td, and ΔHLV waas the enthalpyy of vaporizattion. Using ann absorbed laseer power of 80 00W, which wass the average value v of the laaser power ovver the pulse, aand the area oof the cylinder equal to the beam b spot size, the corresponnding VMRR w was calculatedd to be 8.81x110-9 m3/s, which was also pplotted in Figu ure 7. t VMRR preedicted by the 1D model waas only slightlyy lower than thhe average valu ue of Accordingg to Figure 7, the the 3D sim mulation. Becaause these twoo predictions matched eachh other very w well, the mechhanism of adia abatic evaporatioon could be assumed in the early stage (beefore 750ns) oof the drilling process. The fact that the actual a hole depthh was much deeper d than thhat of the sim mulated hole, it again suggeested significaant contributio on of material reemoval by mecchanisms otherr than evaporaation. 6. Other M Material Rem moval Mechaniisms Based on tthe analysis inn Section 5, it iis estimated thhat adiabatic evvaporation conntributes to onnly 1/3 of the actual a hole formaation. The rolees of other maaterial removall mechanisms,, such as the laaser energy deeposited after 1 s, melt ejectiion, explosive boiling, and thhe energy re-raadiation by thee vapour/plasm ma, need to be iidentified. 6.1 Materiial Removal byy Laser Energyy Deposited att a Lower Laseer Power The effectt of the laser ennergy depositeed after 1 s att a low laser ppower was deteermined in thiss section. In Figure 8, a 1-μs ppulse was plottted against a 44-μs pulse. Forr the 1-μs pulsse, the laser ennergy deposited between 1–1 10 s (the area bbelow the laserr power curve)) was calculateed to be approxximately 2.4 m mJ, while the eenergy depositted in the first 1 s was 0.8 mJJ. The laser ennergy depositedd at this low laaser power perriod was not abble to produce high temperaturre plasma (Figgure 3) but it coould induce melting and mildd evaporation to advance thee hole depth. To determ mine the materiial removal byy the lower pow wer energy, w we compared thhe holes produuced by a 1, 2,, 4, 5 and 8-μs ppulses (Figure 2). The additional energy deeposited by lonnger laser pulsses was 0.3, 0..9, 1.2, and 2.1 1 mJ, respectivelly. The extra laser energies led to 19.5, 338.4, 52.5, andd 80.7 μm addditional hole ddepth, respectiively. Dividing tthe additional depth by the additional eneergy, we obtainned an average depth versuss additional en nergy ratio as 655.00, 42.6, 43.8, and 38.4 μ μm/mJ, respecttively. It appeeared that the energy deposiited near the initial 10 www.ccsennet.org/apr Applied Physics Researrch Vol. 5, No.4; 2013 spike was more effective. It should bee noted that the energy depoosited after thee initial spike iin a 1-μs pulse e was not at a coonstant powerr. Due to this ffact, we use thhe average off the above rattios, 47.2 μm/m mJ, for estima ation. Based on tthis averaged ratio, the addiitional energy deposited betw ween 1 to 10 μ μs (2.4 mJ) forr a 1-μs laser pulse p likely conttributed to 1133 m, which aaccounted for 668% of the tottal hole depth of 166.7 μm. On the other hand, h based on tthe simulation,, the initial spiike of the 1-μss likely was reesponsible for 30 % of the hole drilling (50 0 μm of 166.7 μ μm). Both resullts were consisstent. Figure 8. E Energy differeence between tw wo pulse durattions However, material remooval by meltinng needs effecttive melt ejecttion mechanissms. As shownn in Figure 2, with laser pulsees over 5-s and a hole depthh over 220 m m, significant blockage at thhe opening byy re-solidified melt started to aappear. 6.2 Melt Ej Ejection As the holle depth becam me deeper, it w would take morre pressure to ddrive the melt at the bottom of the hole upward and out off the hole. Thiss melt ejectionn process mustt be effective iin order to keeep the blink hoole open at the e top. In this studdy, we did nott attempt to im mprove melt ejeection by an asssist gas jet, blowing side w way to enhance melt ejection. H However, suchh strategy shouuld be investiggated for multipple-pulse drillling to achievee hole depth ov ver 1 mm or asppect ratio over 20. 7. Three M Media Interacctions From the aabove analysiss, it became evvident that the ddrilling investiigated in this ppaper involvedd three media, laser, bulk materrial, and vapoour/plasma. Reegarding energgy sources for this drilling pprocess, the hiighly focused laser beam was the primary energy e source, depositing ennergy at two diifferent powerr levels, while the vapour/plasma was a secoondary energy source, whichh re-radiate som me energy bacck to the bulk material to prromote melting g and is the onlyy energy sourcce after 10 ss. Note that alll energy camee from the lasser beam, but the vapour/plasma helped to ppreserve some energy. A disccussion of the interactions beetween these thhree media is iin order. 11 www.ccsennet.org/apr Applied Physics Researrch Vol. 5, No.4; 2013 7.1 Laser/B /Bulk Material Interaction Initial Lasser Spike on thhe Bulk Material: The initiall spike (1,500 W) of the laseer beam offereed sufficient power density too initiate a cavity into the bulk materiall through adiaabatic evaporaation (Figure 6). As the en nergy absorbed bby this evaporrated material far exceeded the latent heatt of the materrial due to veryy high laser power density (~ GW/cm2), it superheated s annd partially ionized the vapoour into hot annd high pressuure plasma at about a 16,000–711,000 K. The expansion e of tthis vapour/plaasma also com mpressed the am mbient air to fform a shock wave w which it eexpanded. A popping p soundd was clearly audible durinng the drillingg process. Thee initial spike was estimated tto produce 1/33 of the depth oof the micro-hoole. The Bulk Cavity on thee Laser: The ccavity of the bbulk material ccreated favorabble multiple rreflections to direct d substantiall portion of thee laser beam tooward the caviity bottom to fu further deepen the cavity (Figgure 6). Lower Pow wer Laser on the t Bulk Mateerial: As the laaser beam pow wer fell from itts peak to the steady state power (300 W), tthe power dennsity of the laseer beam was nno longer suffiicient to evapoorate and ionizze the bulk into hot plasma. Thherefore, the energy e depositted by the low wer power laseer beam inside the cavity m mainly was used to create superheated melt inside the cavvity. Without ffurther feedingg, the vapour/pplasma started to cool (Figurre 3). The hole ddepth contributted by the lower power portiion was estimaated to be 2/3 oof the total hole depth. Melt on thhe Laser Beam m: Due to multiiple reflectionss, substantial aamount of laseer energy was ddirected towarrd the bottom off the cavity (Fiigure 6) and tthe lower beam m power contrributed more m melt at the bottom. On the other hand, becaause of its low wer reflectivity,, the melt coulld absorb the bbeam energy m more efficientlyy, cutting down the beam refleection. As a result, r as the hhole became ddeeper, the lasser energy thaat could be delivered to the hole bottom beecame less annd the hole drrilling becamee less effectivee. As shown in Figure 2, a 4-μs laser pulse p contained about 30% moore energy thann that of a 1-μss pulse; howevver, it only prooduced 16% moore in hole dep pth. Figure 9. Interaction among thrree media durinng rapid microo-hole drilling 7.2 Laser//Vapour-Plasm ma Interaction Laser Heatting of Vapourr/Plasma: The IB absorption coefficient caalculated basedd on the electroon temperature e also indicates llow laser/plasm ma interactionn (Table 1) evven at the peakk temperaturee of the vapouur/plama. The laser beam did nnot heat the vaapour/plasma ddirectly and the energy contaained in the plaasma was origginally absorbed via the laser/bbulk interactionn. The above sstatement is alsso supported bby the photo-diiode measurem ment of the pla asma. For exampple, in the one-microsecond ablation, the m measurement oof the plasma emission droppped to almost zero at approximately 3 micrro-second evenn though the llaser power staayed over 2000 W during thee same time period (Figure 3).. Vapour/Plaasma on Laserr Beam: Basedd on the plasmaa measuremennt of Table 1, thhe existence oof plasma insid de the 12 www.ccsennet.org/apr Applied Physics Researrch Vol. 5, No.4; 2013 cavity likeely did not blocck or affect thee laser/bulk intteraction. 7.3 Vapourr-Plasma/Bulkk Interaction As the higgh temperaturee plasma was a high energy source in itseelf, the plasmaa re-irradiated some of its en nergy back to thhe bulk materiial to enhance the hole drillling. The highh pressure, couupled with thee high temperrature plasma, m might also allow the superheeating of the m melt. Subsequuently, the mellt would boil when the pressure dropped aas the plasma expanded andd exited out off the cavity. T The reduction of pressure ppromoted explo osive ejection off melts as fine droplets long after the laser irradiation, as observed in F Figure 4. 8. Processs Anatomy Based on the experimenntal and simullation results ppresented in pprevious sectioons, a temporaal process anatomy diagram of the short miccrosecond laseer drilling, usinng the single-m mode fiber lasser, was compiiled. Four stag ges of the process were depicteed in Figure 100, from shortlyy after the laseer irradiation too long after thee completion of o the laser irraddiation. This process anatom my diagram waas also color-ccoded to illusttrate corresponnding tempera atures during thee process. Thiss process anatoomy diagram summarizes thhe laser/materrial interactionn mechanisms, hole formation,, material rem moval mechannisms, and vappour/plasma ccharacterizatioon as discusseed in the prev vious sections. A summary of time t line, togeether with the pprocess anatom my, is discussedd below: ya Figure 110. Process anaatomy of the raapid drilling prrocess using a one micro-seccond laser plusse generated by single-moode CW fiber llaser my Diagram #11): The laser ppower rapidly increased to be high enoug gh to Stage 1 (00~250 ns) (Proocess Anatom evaporate a small amounnt of solid into hot vapour/pllasma, first dettected at 200 nns. At 250 ns, tthe laser powerr was 600 W andd the cavity waas estimated too be 5 μm deepp (Figures 3 annd 6). Stage 2 (2250~500 ns) (P Process Anatoomy Diagram #2): The intennsity of the vapour/plasma continued to grow along withh the increase of o the laser pow wer. When thee laser power inncreased to itss peak value off 1,500 W at 50 00 ns, the vapourr signal reacheed 1/4 of its peaak intensity. The hole was deeepened to 20 μm. Stage 3 (500 μs ~ 1 μs) (Process Anattomy Diagram #3): The laserr power rapidlly dropped from m its peak to about a 400 W at 1 μs. Howeverr, the vapour/pplasma intensitty continued too grow and reaached its peak value at about 600 to 800 nss. After 800 ns, n the vapouur/plasma inteensity started to drop. Based on the eleectron temperrature measurem ments and subseequent calculaations of the ellectron densityy and absorptioon coefficient, the vapour/plasma was opticaally thin and the t laser energgy could be deeposited over tthe cavity walll without beinng absorbed by the vapour/plaasma, even at its i peak. The hhole was deepeened to 50 μm by evaporationn alone. 13 www.ccsenet.org/apr Applied Physics Research Vol. 5, No.4; 2013 Stage 4 (1 μs ~ 2.5 μs) (Process Anatomy Diagram #4): The laser power fell to its steady state (300 W) at 2.5 μs. The vapour/plasma intensity continued to fall but at a slower rate than that of the laser power. The intensity of the vapour/plasma was still high enough to be registered by the photodiodes, which indicated that its temperature was still high, so was its pressure. The melt produced by the laser at the cavity wall was likely super-heated because it was covered by the high temperature and high pressure vapour/plasma. The hole continued to deepen via mild evaporation and melting. Stage 5 (2.5 μs ~ 10 μs) (Process Anatomy Diagram #4): Laser power dropped below 200 W and continued to drop to zero after 10 μs. At 2.8 μs, plasma had turned into weaker vapour, not detected by the horizontal photo-diode. The laser energy deposited at lower power could still produce some spurts of vapour/plasma inside the micro-hole registered by the steep angle photodiode. This part of laser energy deposited at lower power most likely produced more melt than vapour. The hole continued to deepen mostly via melting. Stage 6 (10 μs ~ 80 μs) (Process Anatomy Diagram #4): No laser energy was deposited in this stage, but hot vapour still covered the micro-hole. This intensity of this hot vapour was too low to be measured by the photodiodes but was high enough to saturate the CCD sensor of the high speed camera (first four frames of Figure 4. Therefore, the temperature of the vapour should be much lower than the vapour/plasma observed in Stages #1-5 to render its pressure lower. The drop of vapour pressure likely would cause the superheated melt to boil and eject outward as seen in frames #2-4 of Figure 4 and the 4th process anatomy diagram. The hole likely stopped deepening and was partially filled with melt, ejecting upward and out. Stage 7 (80 μs ~ 150 μs): Vapour was no longer visible after around 80 μs. The last melt ejection was observed around 150 μs, which was the end of the drilling process. Some melt was re-solidified around the hole as recast. 9. Conclusion This paper presented a single-pulse micro-hole drilling technique using short micro-second pulses by modulating a CW single-mode 300 W fiber laser. The capability of this drilling technique was demonstrated and several in-process monitoring experiments, such as photodiode measurements of the vapour intensity, high-speed photography, and spectroscopic plasma measurements, were used to identify the laser/material interaction mechanisms. For the drilling process with a 1-μs laser pulse, the process started with drastic evaporation and concluded with melt ejection approximately 150 μs later. It is concluded that two distinct drilling mechanisms occurred, one as adiabatic evaporation by the high power initial spike and one as melt ejection by the low power energy deposition. The time line of this drilling process was established experimentally based on measurements by several in-process sensors, such as photodiodes, a high-speed camera, and a spectrometer. The theoretical modeling zoomed in the early stage of the process to investigate the hole formation which could not be observed experimentally. Both experimental and theoretical results were then compared to determine the laser-material interaction mechanisms among three media involved in the process: laser, material, and vapour/plasma. Finally, a series of temporal anatomy diagrams, denoted as process anatomy, were presented to describe the entire drilling process by a one micro-second laser pulse. This process anatomy summarizes the laser/material interaction mechanisms, hole formation, material removal mechanisms, and vapour/plasma characterization of this short micro-second laser drilling process. Acknowledgments This investigation is supported by the Department of Mechanical and Aerospace Engineering at North Carolina State University, NSF Grants CMS-0402857, DMI-0355481, DMI-0355214, DMI-0944509. The authors would like to acknowledge the assistance of Prof. W. Roberts of MAE, NCSU for the loan of the high speed camera. References Bauerle, D. (2000). 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