㄀ϗゴ 䜡ড়⠽ⱘড়៤࣪ᄺ
㄀ϔ㡖 ড়៤࣪ᄺᮍ⊩䆎
䜡ড়⠽ⱘড়៤ᰃ䜡ԡ࣪ᄺⷨおⱘϔϾ䞡㽕㒘៤䚼ߚˈ಴Ўড়៤ᮄⱘ䜡ড়⠽ˈᇚӮᇐ㟈ড়
៤࣪ᄺ੠⧚䆎࣪ᄺⱘ䖯ϔℹথሩˈгЎ⾥ⷨˈए㥃ˈᎹ‫ݰ‬Ϯㄝⱘথሩᦤկᮄⱘᴤ᭭ˈ᠔ҹ࣪
ᄺᆊᇍࠊ໛ᮄⱘ䜡ড়⠽᳝ᵕ໻ⱘ݈䍷ˈৠᯊ䖭гᰃ೼๲䭓࣪ᄺⶹ䆚ⱘϔϾᵕདⱘ䗨ᕘDŽ⬅Ѣ
䜡ড়⠽ⱘ⾡㉏੠᭄Ⳃ䴲ᐌ㐕໮ˈᮄൟ䜡ড়⠽ϡᮁ⍠⦄ˈሖߎϡかˈᕜ䲒㒭ᅗӀⱘড়៤ᮍ⊩ᘏ
㒧ߎϔϾ㾘ᕟˈϔ⾡῵ᓣˈ಴ℸᴀゴা㛑ҟ㒡ϔѯ‫݌‬ൟ䜡ড়⠽ⱘড়៤ᮍ⊩DŽড়៤Ꮉ԰ৃߚЎ
ড়៤䏃㒓䆒䅵੠ᅲ偠˄ᅲᮑড়៤䏃㒓˅ϸ䚼ߚˈࣙᣀབϟℹ偸~
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ᑆ➹‹uò∈∃䩭wᑆ➹ㅵwÊ1F⇻þ∈þÎᬣᛳƒ„„䞛Ä Schlenk 㺙㕂­
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Í2ëáâ‘ÎP6:ÐÑÄ_b\]Ã;‘D<MŒ
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š?£•¾ÝÞu1)âw˜˜Þu1áâw›œå/­Ž×žŸ
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ï\]Š§6NI¨ÚÄL©ƒ„ŽDªÄÜÍ
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3
2
3
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\]DZn/þƒ„˜)ƒ„"n/)áµ²xᵃ„Pû
µ¶‘û·¸—¸XD
r{[BF ·NH ¹:/uþ BF þ⺻2
ˆGúû6@¼½¾M
ª4¿EÀÁ–ýDÁ
<ß|̓„)â qƒ„þâ:nÄP9<=D{23
ÃBF ·OEt ¹:n/NOIÄźúp]Ä)*@¼½¾MÍÆÆ
½¾:ƒ„/n/»2ÇΎDÁ
Íxƒ„<ß|¨)â:n/³´Žƒ„²¶<GÈäÉ¦
Œ‹MŽD{t7ÊIPøË23ì<ɦŒ‹ÌÍOMƒ„DÁ
{Snh΄ÏÐá⃄ÃÄDr{ˆƒ[BF ] nEÅöÑÄöµ
²ƒ„2ëÑÄöÄÄÒÉsöƒ„–ýDÁ
Íá⃄PnÏÐ:–—*‘nh¸Xkm6ˆˆƒ[MX ] ;Ó23DÁ
Á
㄀ϝ㡖߽⫼পҷডᑨড়៤䜡ড়⠽
Á
òûԛœ¢Kûԛœ6NI¨úûL©ƒ„ 23DÁ
˜Œ)ML©ƒ„Á
Œ)ML©ƒ„«¬LÄ\]DijsötuvuÕwÁ
23ìrƒD1Fɦ«¬ŽL©ƒ„ÐÑėÖ×st…†D
{…23 K [Rh(C O ) ],ì K [RhCl ] K C O [Œ)ØÝx:µŽé
?•–ïŒ)M_bUŠD
3
3
3
3
2
-
4
m-
n
3
2
4 3
3
6
2 2
000
K3[RhCl6] + 3K2C2O4
4
K3[Rh(C2O4)2] + 6KCl
|°ƒ„<ß|ƒ„Æ <éÙÚôŽƒ„™WD
000
[Co(NH3)5Cl]Cl2 + 3en
[Co(en)2]Cl3 + 5NH3
ôÛrƒ23gÜGpâuÝwD;GuÝwäF23
n/pûˆâÃÞßàáí,L©DïôzL©ƒ„
âŽdë]Mµ’âu’wnhD EF¸Xs®
ãrƒGPND<|°rƒMEF‰-–ŒÌ¦ä6åæhã’
D
K2[PtCl4] + en
000
[Pt(en)2Cl2] + 2KCl
(yellow)
[Pt(en)2Cl2] + 2NH3
(yellow)
00
[Pt(en)2(NH3)]Cl2
(colorless)
¿˜<KŒ)ML©ƒ„
{S«¬ƒ14W6çè<Œ)MŽL©ƒ„4¸X LL«¬
ƒÌÏÐÌL©ƒ„£<KŒ‹MŽDq0{SâXŒF"£
<KŒ‹MŽDG Cr(éê%uCrCl ⋅6H OwŒ)N¿Ë ýƒ„ìPh2ë
IN¿Ëëuéw ŽÌƒ„ýÑ:ëDÄò%uCr (SO ) w
‰-ÚÄ|°ƒ„n/ÃCr(en) ]Cl DÁ
Á
3
2
2
3
[Cr(en)3]I3 +
3
000
en/ether
Cr2(SO4)3
KI
00
Á
[Cr(en)3]I3
Á
00
3AgCl
«¬4ÔX<KŒ‹MŽDÁ
THF
NiCl2 + 2NaCp
4 3
[Cr(en)3]Cl3 +
00 00 00
3AgI
00 00
Á
Á
NiCp2 + 2NaCl
Á
Á
§ìefÃÄG4Ԍ‹¿PøPËuDMFwDr{ÃÄdŒ‹hí/
–Ÿ ý|DÁ
000
000
DMF
[Cr(DMF)3Cl3] + 2en
(pale blue)
cis-[Cr(en)2Cl2]Cl
(purple)
Á
Á
4kâPŒFïï‰âŒÌ<GɒŒ4Ԍ‹MµdŒ)
p]«¬ƒŒ)MªnD{[Fe(bipy) ]Cl :ðñòXŒF;ŒÌ<
N~MµÉ FeCl Œ)’ªn23„DÁ
I˜ÚÄá¯Ìƒ„Á
ÌÍF<á¯ML©ƒ„D<ß|n ¦âóUZ[<ôõ/
ïïÈäöˆƒ.÷ºDÁ
0 0 0 [Cu(SO )] + 5H O
[Cu(H O) ]SO . H O
Á
0 0 0 [Rh(NH ) I]I + H O
[Rh(NH ) (H O)]I
Á
00 00 00
trans-[Pt(NH ) Cl ] + 2NH
[Pt(NH ) ]Cl
Á
48rƒø E[Co(H O) ]Cl Œ)n/mòEùú<ûôÍü&:ý
UyEþ䗍;"̃„D
3
2
2
2
4
3 5
4
2
3 4
2
4
3
2
2
2[Co(H2O)6]Cl2
6
2
3 5
2
3 2
2
2
3
2
000
Co[CoCl4] + 12H2O
Á
⸙㛊&-‹ᦎ4 CoCl ਜyEFµì EÍ⸙㛊, E:’⼎Z|
༅†Ph„&-mÄmÍü&㜅µজyE⸙㛊nÃÄDÁ
Á
Á
(blue)
2
t˜L©ƒ„Mƒ†„Á
uwƒ†„`aÁ
<
23 3WÕêÁû·M SWûL©ƒ„/µë]–Vԩ‘O
u乎c²ƒcwnhɉŠÓ"nhPÓDr{€23 cis-[Pt(NH ) Cl ]
ÐÑÄ[PtCl ] ‰- 230 trans-[Pt(NH
) Cl ]ÐÑ/[Pt(NH ) ] ‰-DÁ
0
0
000
NH 0 0 0
NH 0 0 0
cis-[Pt(NH ) Cl ]
[PtCl ]
[Pt(NH )Cl ]
Á
0
0
0
0
0
0
HCl
0 0 0 [Pt(NH ) Cl] HCl trans-[Pt(NH ) Cl ] Á
[Pt(NH ) ]
ïô°xstSC§U~&O ƒâÈäöL©D^_…6ˆst
gs*U…ƒ†„`aD.ƒ†„ª~
41M«¬ôõ
â4;ƒâÈäöL©†„D;ïèAÞU ¯ƒ†„~
ª41M«¬ôõâM‰ƒµïï]JF;ƒâ
_!
DúûstëU<L©ƒ„M¾¦ƒ†„"î~C H #NO#CO#
CN > R P#SR >>NO >I #SCN >Br >Cl >py>NH >OH >>H ODÁƒ†„`a S1…
ÌL©ƒ„eK/­$%ƒ„\á1)\°Ý4¾s®&
'Dƒ†„`aP(ÜÄF ÕêÞ°À\}L©ƒ„1;) d ‘O
*+Õê˜Á
Õê˜Á,-éê˜./0êÁ120êÁ)„Ä"4”•m3°â‘O
ƒ†„—Dq0P9«¬ƒ;ƒ†„Y"P9456š7]
1.4«¬¨ÜÄ⃆„"îDÁ
u¿wƒæ‘âÁ
ƒæ‘â4xGBC~7](hýGæ‘⃄…†²¶ÚČÌÎ)
¦KP99:ýxGæ‘âDƒ„M(ýGæ‘â{c8¿7tu
‚uéw7u¢E%wn/9:ö;<ö‚ŒFuMúû¼þ:1ý
cis-[Co(NO ) (NH ) ]NO ‹Œµá‹ŒMp[ HCl™nëcD<
Þ°À\}=;>:n/ÚÄ?°@ƒ†„`aAB
¾æ‘âD
Cên/ÈäD2ëƒcæ‘â 23cæ‘♸—¸XD{
ÕêÞ°À\}:Xë] trans-[Pt(NH ) Cl ] uEEwD{S:‹
Br ² H O ™ºýƒc¿Fƒc¿GøDcæ‘âuE
Ewn/úû|°ƒ„DÁ
3 2
2-
2
2+
4
3 2
2
3
4 2-
3 4
3
-
3
3 2
3
2
+
3 4 2+
3 2
3 3
2
2
2
-
3
2
-
-
-
-
4
-
3
2
8
2 2
3 4
2
2+
3 4
2
2
2
2
Cl2
+
000
NH3
+
000
cis-[Pt(NH3)4Cl2]2+
Á
{S<ƒ„û·Mýƒæ‘â’™ÐÑúû_b˜ƒHI˜²
;™<=™[DSJxrƒ/z{Dƒc¿7¿N¿ËKuéw
~Í KOH Æp]
RhCl ·3H O en·2HCl L EŒ)M:ë]
GMNEE)⪃c¿7¿N¿ËKuéw’dŒ)GÄ HNO
öë]«EEbâ|O{ trans-[Rh(en) Cl ]NO PûZµŒ)é [\ÌÌ
Η6QEE cis-[Rh(en) Cl ]NO åUD;rƒz{̓„ý…æ‘â’
:n/ÚÄZ[<ŒÌÎôåæ;/Dƒc¿RŽN¿Ë‚uéw7
~IN¿Ë‚uéw7ŒFMG4 0°Cp KCNÁŒ
) S p . 4 ¾ ˆ T ¦ U H I V W X ƒ M Ä 2M LiCl Y ü Z E
trans-[Co(en) (CN) ]ClÁ1öYü|Š§µEE cis-[Co(en) (CN) ]ClPYü)Wû[\
pN~™nåU[\–—Ddrƒz{̓„ý…æ‘â’:nú
ûƒHI]Z[/DÁ
[Pt(NH3)3Cl]
HCl
mer-[Pt(NH3)3Cl3]
3
2
3
2
2
2
2
2
2
3
3
2
2
Á
]˜L©ƒ„M^mÄÁ
1FÇÎWÆL©ƒ„23.£LL£ßÎ_>ƒ„:µDJ?
|Ä^‹ƒ„ÇÎmãÚÄ^‹rƒ¢P`NDr{
Cê
23—¸Xƒ„ÇÎÆ ÚÄ uÕw^mÄhãD23 Cê
DPÄ^‹™ trans-[Pt(NH ) (SCN) ] ìPhDÁ
[Pt(NH ) ]0 0 0
trans-[Pt(NH ) (SCN) ]
+ 2Cl
trans-[Pt(NH ) Cl ] + 2SCN
Á
dƒ„Ý^rOD¢4k¬FN^§lO„Ä[Co(NH ) ]Cl
23DÍ CoCl Œ)Éûˆ NH NH Cl ƒ„’Ž¼þ:aµ
Äûˆ%ööë]–l[Co(NH ) Cl]Cl m<9Ӆ†|4T¦U­<:
–Vb,¨ [Co(NH ) ]Cl DÁ
2+
3 4
3 4
2
3 4 2+
-
2 2+
-
2 2+
3 4
3 6
2
3
4
3 5
3 6
3
2
3
㄀ಯ㡖߽⫼⇻࣪䖬ॳডᑨড়៤䜡ড়⠽
ÁÁÁÁÁÁÁÁÁÁcN«¬23ïïdaeM«¬ƒ:¯ª ý…:¢‰ƒ„D
:¢‰ƒ„LLyzäL©]ɦL©û·r{~fÕêgféêÊ2ÕêgÁ
2éêD23I®‚/¿®‚‰-µ¿®‚:ɦI®‚
Á
˜M«¬:Á
§A:‹¼þ˜û:ÑD¿:h"GWA:‹Í­<7ƒ:ý
¿7h¿E‹ŒäFûZêõD9Ó¿:i"GWA:‹¢‰–
jk lE‹Œ"äFûZêõDKMnO K Cr O "hm:‹m<ƒ„’Mnp
P䐫¬ƒDoœ X "nÄm:‹mnpoƒ X D?|Û­<‚
23û·ML ý fÕêgféêS<±¦%M fÕêǾ M féêǾDlO¿®‚WX2ëêK<ɦþâpq|²¶
­<r¢‰‹D23I®‚úLÃÄ:‹¼þû:ÑDr{/
CoCl ·6H O ‰-<Ü4Ò%Œ)MÄT¦Um^‹û:Ñ:‹n ýƒ„D
ؐᕫ⊼ᛣⱘᰃডᑨѻ⠽᳝ᯊ‫އ‬ᅮѢ᠔⫼ⱘ⡍ᅮ⇻࣪ࠖDr{Ä[Fe(CN) ] :[Co(EDTA)]
n/2ë[Co(EDTA)] {SÄ Br m:‹™ƒ„[Co(EDTA)Br] DÁ
4
2
2
7
-
2
2
2
3-
2-
6
-
2-
2
000
00 00 00
[Co(edta)]2- + [Fe(CN)6]3-
-
[Co(edta)]
+ [Fe(CN)6]4-
Á
Á
ꅂä ý:¢‰ƒ„/0;Z¢4/sösötŒ)Š¢‰
ëötëIsöëötD{<uMWN/v :¯­<úLÄ wxÕê
%Ž:ƒ„²¶ wxÕêÉ MnO :¢‰ƒ„Š23Dr{ÚÄ MnCl ·4H OP
E:öyö’:ýI®yö%µ KCN ƒ„2ë K [Mn(CN) ]DÁ
Á
[Co(edta)]2- + Br2
-
[Co(Hedta)Br]
-
+ Br
4
2
3
6
2
¿˜M«¬¢‰Á
LÄ¢‰‹4~)uM;²tÊtÑz{M|²}Ê;~˜€~ʁ˜GuÊ
YyöÊÅÑt)DÁ
K/liq.NH3
K2[Ni(CN)4]
000
K4[Ni(CN)4]
PPh3/ N2H4
[Pt(PPh3)2Cl2]
000
Á
Á
[Pt(PPh3)4]
㄀Ѩ㡖߽⫼䜡ԧϞⱘডᑨড়៤䜡ড়⠽
|W SAk«¬n/<P ý«¬8âQ‚çè|ýD{ï
rö23[Co(NH ) H O] û·Mûõ? H O L©… CO ƒ
s®ôÄ ƒ!nO{Œ‹„4á–*+:‰ƒ :оƒ„…†|
ŠDÁ
23
3+
[Co(NH3)5CO3]
18
O
3 5
[(NH3)5Co -O
+
CO2]
2
2
000
+
+ 2H
[(NH3)5Co -OH2]3+ + CO2
Á
¢4;Zƒ„n/<P ý«¬8âQ‚çè|ŽD;GHOƒ„|ö„ÄF
Ü*âSus®rƒM¢4 *8sRö‡ƒö:/­ *89
:ö‡ƒö¢‰DÁ
[(NH3)5Co -N
CS]2+
[(NH3)3Pt -NO2]
+
H2O2 / H2O
Zn / HCl
000
00 00 00
[(NH3)5Co -NH3]3+
[(NH3)3Pt -NH3]2+
Á
Á
<|°rƒMMâ’SU\EâeˆB“ƒ„~Á
[Cl2Pt(PCl 3)2] + 6H 2O
000
[Cl2Pt(P(OH) 3)2] + 6HCl
00 00 00
000
SbF3
Ni(PCl 3)4
Á
Ni(PF 3)4
Á
Í?h[478Hƒ„F«¬ƒô4ԃƒ„L©ƒ„Dr
{IN'(ë<#<öMh‰Ç9F ýƒ„ýDhL©N'(øô
TŠÑøù¢4~- NH ˜- N ˜-CHO˜-COCH -SCl )Dúûâô ýkƒ„
n/23P‹DÁ
ROH
2
+
3
3
Ni(P(OR)3)4
˜6ŒâÁ
6Œâ4‹Ü4tŽGhí,y«¬ƒâD‘øɒËý9Ë
ujî/+““Á”¶•kwƒ„NŽâ6ŒâGƒ„DÁ
OH
-
OH
+ Cu2+
000
O
C=O
CHO
H
0
0
0
O=C
0 0 Cu
0
O
H
nBuNH2
nBu
00 00 00
O
C=N
0 0 Cu
0 0 0 0 N=C
000
H
en
O
H nBu
00 00 00Cu00 00 00
C=N
O
O
+ 2nBuNH2
N=C
H
H
Á
[Cu(Salen)]
¿˜b†„Á
EFF«¬ƒâ}6ŒDÁ
000
CHO OCH
N
H
N
en
H
Cu2+
00 00
Polymer
0 0 0 0N=CH
HC=N
Cu
N
N
Á
Á
2+
O
2
+ 2H2NCH2CH2CH2NH2
O
Á
Á
Ni(OAc)2
00 00 00
00 00 0 00000 N
Ni
0
0
0000 N
N
N
Á
Á
Á
R
00 00 00
O
+ 2H2NCH2CH2SH
R
O
R R
S
S
N
H
N
H
I
Ni(OAc)2
000
R
N
N
00 00 0 0 0
R
N
SH
R
N
SH
II
00 00 00 S
0 0Ni0
S
Á
PǾtŽâu11w
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™‹ˆ­<mÍα8¿(É ‡8uøNs~<<ö™­<|ƒ„:h/ š›œ–Ÿë]Jƒ
uPǾâu11wwD;GEFF«¬ƒÃPǾMµâhý
Ǿ†„⛁࡯ᄺ῵ᵓᬜᑨD.ࡼ࡯ᄺ῵ᵓᬜᑨ~Ä«¬ƒƒ„ø
ù/ÜÍV}Âá¾Ã¾áNƒ„ë/ŽDÚÄbƒ„n/ë]6Œâ
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Ÿ =NDênh¤4ýT¦06ŒâLLë]4æL«¬8‰ƒð
>/­hǾ¤4¡æ:¯«¬ƒDÁ
¢£~Á
¤@*‘áâ[G\]DÁ
‡¤Ìƒ†„b†„Á
¤/[Pt (Cl) ] ‰-ÃPt(py)(NH )(Br)(Cl)¹IGæ‘âDÁ
Á
R
2-
4
3