Advanced Materials Research Vols. 393-395 (2012) pp 453-457 Online available since 2011/Nov/22 at www.scientific.net © (2012) Trans Tech Publications, Switzerland doi:10.4028/www.scientific.net/AMR.393-395.453 The Model Theory on Structural Mechanics of Cell Disruption Force in the Preparing Process of Superfine Wood-flour With Cryptomeria Fortunei Dongxia Yang1,2, a, Yan Ma1,b and Chunmei Yang1,c 1 College of Mechanical and Electronic Engineering Northeast Forestry University, Harbin,150040, China 2 Harbin University, Harbin,150040, China a [email protected], [email protected], c [email protected] Keywords: Superfine wood-flour, Cell disruption, Structural mechanics, Truss. Abstract. In the process of preparing superfine wood-flour with physical method, when the size of wood-flour particle reaches to the corresponding level, a single wood cell will be destroyed. In the process of analyzing micro-nano wood-flour’s cutting power, the process of cell disruption of the wood cell needs to be computed. Based on the relevant theory of finite element and structural mechanics, this article builds a structure mode of 12 lever hexagon truss model to simulate the cellular structure. There are 6 levers outside to simulate the cell and 6 levers inside to simulate the internal pressure. This establishes a single cell stress model to analyze its stress. It can be obtained that when the size of the force acting on the node reaches the unit force, the minimum tensile stress of the bar element is bigger than the macroscopic tensile strength of the wood. According to the structural characteristics of the cell wall, this paper compares the tensile stress along the grain of the bar element with the tradition cutting stress. Using tensile strength as the criteria to test the rupture failure of Cryptomeria fortunei cell, the wood cell’s disruption force can be concluded. When preparing superfine wood-flour with Cryptomeria fortunei as experimental raw materials, the calculated results of applying the traditional cutting theory to calculate the cutting force has proved the analysis structure of Cryptomeria cell micromechanics with the method of finite element and structural mechanics, so that it can be concluded that certain cutting force can make Cryptomeria fortunei cells disruption. Introduction When the wood is processed to several thousand nm, the wood is called ultrafine powders or nano-particles. Now the granularity of the ultra-fine wood flour particle is defined between 1000 ~ 20000 nm [1], but the general equivalent circle diameter wood cells is about 10 ~ 80µm, so when the wood is processing to the ultra-fine wood flour particle size, the wood cell wall must be destroyed. Therefore, the discussion of the broken force of the cell wall has important theoretical significance. 1. The establishment of the unicellular mechanical model Plant cell consists of cell wall and cavity material, and the cell wall is a specific structure of the plant cell. Wood cells are mainly composed of cellulose and hemi-cellulose ingredients. Cellulose molecular chains give the mechanical strength to the wood and the hemi-cellulose can increase the rigidity of the cell wall. The cell wall contains lignin which can enrich and rigid the cell wall [2]. The cell structure of the wood cross-section is similar to the hexagonal form observed by the optical microscope, and the tracheid lumen which is on the inside of the regular cells can be approximated to a circular cavity tube. According to the characteristics of wood cell structure and though the structural principles of the three-dimensional simulation algorithm, the micron wood fiber images can be transformed in three-dimensional coordinate according to the arrangement way of the All rights reserved. No part of contents of this paper may be reproduced or transmitted in any form or by any means without the written permission of TTP, www.ttp.net. (ID: 130.203.136.75, Pennsylvania State University, University Park, USA-26/02/15,22:30:04) 454 Biotechnology, Chemical and Materials Engineering cell tissue. Then the three-dimensional morphological modeling of the wood cells can be achieved on the computer and the three-dimensional simulation diagram of the cell structure can be obtained which is shown in Fig.1 [3]。 The length of wood cells is far greater than its sectional dimension, so we got the establishment of the simplified mathematical model by the statistical analysis of the extra cellular profile. After that we assume that the stress analysis of wood cells can meet the plane strain state and the stress of wood cell characteristics can be discussed under the plane state. Fig. 1 The cross section of wood rules cells and solid simulation of cell structure The regular wood cells shown in Figure 1 will fall to pieces if it subject to greater cutting forces and if it is processing to the micro-nano level, almost every cell must be broken in the crushing process, so the research on cell-wall breaking is the basic research of wood crushing. In the processing of the ultrafine wood powders the raw materials should be dried at first, because the wood fiber is brittle in the low-water-content and which is in favor of the processing. The actual photo of the cells crushing is in Fig. 2, Fig. 2 The photos of cells were processed to cell disruption state Wood is a natural non-homogeneous anisotropic polymer composite engineering material, and the traditional research methods can not get the true mechanical properties of it. In this paper, the structural model of wood cells was established by homogenization and the finite element method. For the uniform and periodic microstructure shown in Figure 1, we can use a smallest unit cell as the representative volume element and the strength of the wood cells are mainly in the cell wall. Therefore, when the mechanical model of the wood cells was established, it was set in truss structure. Two-dimensional hexagonal model of wood cell is composed of 12 linear elastic rods, 6 of them is used to make the hexagonal simulation cell wall by rigid joint and the others are articulated into star-like to simulate the internal pressure of the cell. As a mechanical model, this paper analyzed the ideal state, for the triangular-shaped, quadrilateral, pentagon, etc. As long as one side is zero, that you can get the ideal state. For non-regular hexagonal type, we just should change the length of rod. Now for calculate the force of a single cell, we assumed that the model in Fig. 1 was subject to a one-way compression force from top to bottom and take a cell unit i from it, the force of the unit can be expressed in Fig. 3 by step. Fig. 3(1) shows the forces between cells and the vertical downward compressive force of the cell unit i from two-dimensional tissue model can be replaced by node load and node moment in the trusswork. Fig. 3(2) shows the supporting force of the cell unit under pressure in the two-dimensional tissue model, and it can be expressed by axial force on node 4 and 5 along the direction of the rods in the trusswork. Incorporate the force of Fig. 3(1) and 3(2), we got Fig. 3(3). Fig. Advanced Materials Research Vols. 393-395 455 3(4) shows the compressive force of the cell unit in the two-dimensional tissue model, and it can be expressed by F on node 4 and 5. The force of the single-cell unit in Fig. 1 can be expressed by the superimposed force in Fig. 3(4) and 3(3). Fig. 3 (3) and 3 (4) has become the standard force structure, and the results can obtained in convenient by the finite element software. Fig. 3 The forced model diagrams of a single cell 2. The broken force calculation in cell wall During the analysis of the structural force in Fig. 3, the unit compressive stress of the rod unit (4) was calculated by finite elements method in micro-mechanical. The core issue of the finite element method was to derive the element stiffness matrix, and the displacement method was used in this paper. Displacement values were calculated by using the formula {F} = [k] {∆}. When the force is 1kN, axial force diagram and deformation pattern in the two-dimensional model of cell organization can be obtained by software simulation, shown in Fig. 4.On condition that the blade radius is close to or greater than the average thickness of one pair cell wall, the fiber of the front cutting edge is pressed bending not cited by the cutting edge at the cutting begin. Then the fiber in the front of the cutting edge including below the cutting plane all generated tensile stress and the maximum value occurs in minimum curvature radius of the cutting edge. When the tensile stress exceeds the ultimate tensile strength of wood, the fiber in the front of the cutting edge pulled off and the cutting edge plays the role in fiber cutting. With the increasing of the cutting force, the maximum force of the bar unit is the 6 bar unit that imitate the intracellular pressure, the 4 bar unit at right and left sides which imitate the cell wall take second place, and the minimum is the 2 bar unit at the top and bottom which imitate the cell wall. This process happened to coincided with the destruction process of the wood cells after the compression deformation under the effect of cutting force. 1. Axial force diagram 2. Deformed Shape Fig.4 The axial force diagram and deformed shape diagram of cell tissue two-dimensional model From the axial force diagram two-dimensional model of cell tissue we can see that different parts of the rod unit are exposed to different axial force, and in the calculation we take the smallest axial force of the upper and lower rod unit as the basis. Take the Japan cedar for example, tracheid cross-section length of Japanese cedar is related to the earlywood and latewood. Here we take the 31µm as average value of the latewood[4],when the pressure on node 4 and 5 in the cell model is 1kN, the minimum axial force of the rod is 0.07kN, and the tensile stress of the rod is 72.84MPa. The tensile strength of the Anhui Xiuning cryptomeria in the fiber direction is 28.5MPa, and the tensile stress of the rod is much greater than the macro tensile strength of wood. In the calculation of tensile 456 Biotechnology, Chemical and Materials Engineering stress of the rod unit in the cell model, the tracheid wall thickness affects the physical and mechanical properties of wood, the thicker of the cell wall, the smaller the cell cavity is, the wood density is larger, and the intensity is higher. Therefore, the tensile strength of the cell with thin and thick cell wall can be simulated by structural mechanics. The critical value of axial force of the corresponding rod unit was calculated between 5.14~9.34kN. It can be seen that so long as the cutting force applied to the model is more than 9.34kN, the broken will occur in the rod unit of the cell model. 3. Make evidence for the cutting forces calculation of ultrafine powders in micromechanics by the application of traditional cutting theory The cutting of the ultrafine powders belongs to micro-nanometric cutting, and its stress analysis is the scope of micro-mechanical, so the experimental verification of this result is almost impossible at this stage. But it should be similar to the result go through with the traditional experimental verification. During the cutting of raw materials, the cutting angle, cutting speed, species and the cutting direction relative to the fiber direction all have an influence on the unit cutting force, reference to the empirical formula of the cutting force[5]: (1 − x)a h H H − f 1' (1) ] ( MPa) x = H eµ In the equation, Kµis unit cutting force, µis friction coefficient between the cutter and material, eµis the equivalent diameter of cellulosine, H is the relational functions between the main cutting force and cellulosine, the coefficients A, B, C, H depend on tree species,cutting direction relative to the fiber direction and the cutting method in vertical, horizontal or end grain cutting, aq, ah, x is the modified coefficient in unit cutting force by the sharp blunt degree of the cutting edge. When the ultrafine powders is being processed using the Japan cedar as the experimental materials, take the cutter diameter D=280mm, the main shaft speed of the cutter n=7000r/min, the cutting angle δ=5°. Through the calculation we got the unit cutting force Kµ=16.83MPa, and the cutting force of the main direction F= 13.33kN, which is much larger than 9.34kN. In the wood cutting theory, the traditional method of calculation is often in less accurate within the safe range, therefore, the value calculate which is greater than the finite element analysis is normal. If this calculation model considers the anisotropy, the gap between the two calculations will be even greater. According to this calculation, when the cutting force in the main direction F= 9.34kN, the truss rod in cell model was fractured and the cell wall is broken. K µ = 9.807[10 xa h H + a q ( Aδ + Bv − C ) + 4. Conclusion This paper analyzed a damage case in cell wall which was one of the most common models of the wood cell structure. Wood cross-section of the cell mode is closely related to its species, age, early wood or late wood, and growth characteristics of each season's. The structural model is also different, rectangular, triangular, curved six prism, etc. In this paper, the cell-wall breaking in various shapes cells were all analyzed. Other structure models can also be analyzed and calculated in subsequent work to improve the calculation accuracy. And it also can be analyzed as a thin-walled bar, which can make the calculation of the broken cell wall more useful reference. After the comparison with the traditional method, the results in this paper have a certain amount of accuracy and credibility. Biography: Yang Chun-mei(1977-),female, Associate Professor in Northeast Forestry University, Harbin 150040, P.R. China Biography: MaYan(1955-),male, Professor in Northeast Forestry University, Harbin 150040, P.R. China Advanced Materials Research Vols. 393-395 457 Acknowledgements This work was financially supported by the National Natural Science Foundation of China (30800869) and the National Natural Science Foundation of China (31070500) and Natural Science Foundation of Heilongjiang Province (C201018) and Central university basic research special fund operating expenses (DL09BB14). References [1] Yang Chunmei, Qi Yingjie and Sun Yonghua, in: Practical Analysis of Formation of the Sub-nanometer Cellulosine and Application Prospect, Journal of Northeast Forestry University, 63-65(2008), 36(10). [2] Li Jian: Wood Science, Harbin, Northeast Forestry University Press, 1994, 12. [3] Qi Yingjie, Yang Chunmei and Ma Yan, in: The Establishment and Simulation of the Simplified Model of External Outline of the Pine Cells, Scientia silvae sinicae, 93-95(2006), 42(9). [4] Cheng Junqing, Yang Jiaju and Liu Peng, in: China Wood Chi, Peking, China Forestry Publishing House, 1992, 3. 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[12] Wang Shizhong: Structural Mechanics and Finite Element Method, Harbin, Harbin Institute of Technology Press, 2003, 4. Biotechnology, Chemical and Materials Engineering 10.4028/www.scientific.net/AMR.393-395 The Model Theory on Structural Mechanics of Cell Disruption Force in the Preparing Process of Superfine Wood-Flour with Cryptomeria fortunei 10.4028/www.scientific.net/AMR.393-395.453
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