ÓASM International 1059-9495/$19.00 JMEPEG (2013) 22:3222–3227 DOI: 10.1007/s11665-013-0632-x Finite Element Analysis of Deformation Homogeneity During Continuous and Batch Type Equal Channel Angular Pressing Jaimyun Jung, Seung Chae Yoon, Hyun-Joon Jun, and Hyoung Seop Kim (Submitted March 3, 2013; in revised form May 17, 2013; published online June 29, 2013) Equal channel angular pressing (ECAP) is the most promising and interesting process for refining the grain size to an ultrafine grain or nanosize by imposing severe plastic deformation into the workpiece and repeating the process while maintaining the original cross-section of the workpiece. In this paper, we simulated the batch type ECAP and the continuous type equal channel multi-angular pressing (ECMAP), which can impose large deformation by repeating the shear deformation, using the finite element method and investigated the similarity and difference of the two processes. In particular, modified die design of the continuous type ECMAP was proposed for strain uniformity. Keywords batch type and continuous type pressing, die optimization, equal channel angular pressing, equal channel multi-angular pressing, finite element method, strain uniformity 1. Introduction Equal channel angular pressing (ECAP) is a process that enhances physical properties of a material by applying severe plastic deformation (SPD), and is a widely used technique for processing bulk ultrafine grained (UFG) or nanostructured metallic materials (Ref 1-4). Unlike powder metallurgical technique for producing bulk materials, ECAP is capable of not only preventing emergence of pores, secondary phases, or any unwanted contamination to the materialÕs integrity, but also of emanating variety of novel and interesting material properties by controlling the materialÕs plastic deformation without changing its original cross-section (Ref 5-7). In general, the ECAP technique is an intermittent process that progresses using various routes with repetitive and rotational workpiece motions: route A represents purely repetitive processing without any workpiece rotation, route B represents a process with 90° rotation, and route C represents a process with 180° rotation of the workpiece (Ref 1, 2). Jaimyun Jung, Department of Materials Science and Engineering, Pohang University of Science and Technology (POSTECH), Pohang 790-784, Korea; Seung Chae Yoon, Research & Development Team, Hyundai HYSCO, Chungnam 343-831, Korea; Hyun-Joon Jun, Power Reactor Fuel Development, Korea Atomic Energy Research Institute, Daejeon, Korea; and Hyoung Seop Kim, Department of Materials Science and Engineering, Pohang University of Science and Technology (POSTECH), Pohang 790-784, Korea; and Center for Advanced Aerospace Materials, Pohang University of Science and Technology (POSTECH), Pohang 790-784, Korea. Contact e-mail: hskim@ postech.ac.kr. 3222—Volume 22(11) November 2013 The actual ECAP that is often used is a modified version to fit industrial appliances, and an active field of research has been dedicated in designing ECAP channel and die to optimize the process. In fact, adding various channels to maximize effective strains imposed by the process has been an ongoing research, and equal channel multi-angular pressing (ECMAP) (Ref 8) or parallel-ECAP (Ref 9) represents the very core of the research. It is considered that ECMAP is apt in enhancing materialsÕ physical properties because ECMAP, even in a single process, provides more effective strain than the conventional batch type ECAP processes offer. In reducing the grain size of a workpiece material, ECAP demands repetitive processing in which the development of the material deformation takes on a new aspect, especially in the case of deformation uniformity. Also, for effectively controlling the strain that develops in each channel of ECAP, KimÕs proposals on deformation behavior of materials through the ECMAP processes of routes A and C (Ref 8) and the consecutive ECAP process (Ref 10) have been considered, and the finite element method (FEM) analysis for such processes was introduced. The physical properties of the processed materials strongly depend on processing routes and conditions, which is why a precise analysis of processing routes and conditions should be precedent. Notably, processing conditions regarding the materialÕs strain uniformity are essential (Ref 11-13). That is, the route A of batch type ECAP processes is not the same as the route A of continuous ECMAP process in terms of strain uniformity, and thus a modified design of ECMAP becomes necessary. Therefore, in this paper we will investigate the deformation homogeneity and behavior of materials through FEM analysis with modified design for route A of ECAP applied to the continuous ECMAP process. 2. FEM Analysis Figure 1(a) represents the original ECAP process with width of W and height of 6W. Figure 1(b) represents the formerly Journal of Materials Engineering and Performance 500 Stress, MPa 400 10W 300 200 100 6W 0 W 0 1 2 3 4 5 6 Strain Fig. 2 Stress-strain curve used in the FEM simulation W (a) W (b) Fig. 1 Finite element mesh system for (a) batch type ECAP and (b) continuous ECMAP suggested design of route A for continuous ECMAP with width of W, height of 10W, and distance between each channel of W (Ref 8). Here, W is 10 mm. The die consists of 90° channel angle and 0° corner angle so that the ECAP and ECMAP processes can offer greatest degree of deformation. The friction coefficient is designated as 0.1 the common value for cold metal forming. The mesh number of ECAP is assigned to be 3000, while that of continuous ECMAP is 5000. Plane strain condition is assumed with isothermal strain rate of 1 mm/s. The specimen used for the calculations is pure Cu with stress-strain data extracted from the dislocation cell evolution model (see Fig. 2) because data measured from tensile tests is not capable of providing large strain data that is necessary for SPD process simulations (Ref 14). The analysis software used for the simulations is commercial FEM package DEFORM-2D (Scientific Forming Technologies Corporation, USA). 3. Results and Discussion 3.1 The Deformation Behavior of Materials Processed Under Original Continuous ECMAP The original U-type continuous ECMAP process was designed to exhibit twice the performance compared to the repetitive ECAP processing through route A in a single procedure (Ref 8). To observe the deformation homogeneity, the ECAP processes with single and repeated procedures were executed. Figure 3 shows the effective strain distributions of processed specimens after ECAP process through route A: Fig. 3(a) represents the effective strain distribution of the single pass, while Fig. 3(b) represents the strain distribution of the pass 2 sample without any rotation. Figure 3(a) reveals an overall well-matched result compared to the original work (Ref 13): the arrow A indicates the folding defect (Ref 11). Figure 3(b) represents the repeated procedure through route A, and shows an Journal of Materials Engineering and Performance overall increase in effective strain compared to single procedure and a diminished corner gap (Ref 13). Less sheared zone (LSZ) becomes evident near the bottom of the specimen where a lower strain distribution is observed. More so, in the case of repeated procedure through route A, from the arrow, one can observe the preliminary folding defect has retreated back with the emergence of a new folding defect where arrow B points to. The general shear deformation behavior seems to be an elongation along the extruding direction (Ref 15-17). Figure 4 shows the effective strain from top to bottom in a steady state region in ECAP where the single procedure curve coincides with the general results (Ref 18), but not in the case of repeated procedure. The specimen processed through the repeated procedure through route A has a significantly less deformed region at the bottom. In fact, while the difference in effective strains of top and bottom in single procedure case is only 0.76, the case of repeated procedure renders a significant difference 1.403, indicating an increase in effective strain deviation in repeated procedure through route A. Based on this information, Fig. 5 shows the average effective strain and standard deviation: the lower the standard deviation, the more the homogeneity of deformation (Ref 11). The single procedure case holds to a 0.884 average effective strain with standard deviation of 0.352, while the repeated procedure case estimates to a 1.8 average effective strain with standard deviation of 0.586, which is 0.23 higher than the value from the single procedure. It is considered that the repetitive processing without any rotation forms corner gaps due to accumulation of LSZ, which leads to limited strain near the bottom (Ref 13). Figure 6 displays each stage of the continuous ECMAP process that is designed to exhibit twice the performance compared to the repetitive ECAP process through route A in a single pass. Stage (A) is the initial stage, (B) is the stage after first deforming zone, (C) is the stage through the second deforming zone and a moment before the specimen exits, (D) is right after the specimenÕs head exits the second deforming zone, and (E) is the final stage. Like each stage, stage (B) is very similar to the single procedure ECAP with a corner gap. At stage (C), when the specimen head is just about to pass through the second deforming zone, the material in the first deforming zone experiences a back stress developed in the second Volume 22(11) November 2013—3223 Fig. 3 Deformed geometry and effective strain distribution for the batch type multi-pass ECAP Route A 2 Passes Initial 1 Pass 2.5 Effective strain Effective strain 2.5 2.0 1.5 1.0 *SD: Standard Deviation *AES: Average Effective Strain SD:0.586 2.0 AES:1.8 1.5 SD:0.352 1.0 AES:0.884 0.5 0.5 1 Pass 0 2 4 6 8 Distance, mm Fig. 4 2 Passes 10 Fig. 5 Average effective strain and standard deviation values after 1 pass and 2 passes of ECAP route A Path plot of effective strain along the thickness direction deforming zone to the direction of the arrow (Ref 12). Due to the back stress, the corner gap shrinks. At stage (D) most of the corner gap in the first deforming zone vanishes, but another corner gap arises from the second deforming zone. However, the corner gap in the second deforming zone is smaller than the first corner gap at stage (B) due to low strain hardening of the already deformed material. At the final stage (E), the specimenÕs bottom edge features a very different behavior in regions F and G, both of which have an approximate length of 3.5W (Ref 12, 13). The corner gap developed at first and second deforming zones accumulates LSZ near the bottom of the specimen, leading to a low effective strain at the bottom of the specimen in region (F). The bottom of the specimen in region (G), on the other hand, contains high effective strain due to the 3224—Volume 22(11) November 2013 back stress that filled up the corner gap at the first deforming zone. Figure 7 shows path plots of the effective strain from bottom to top in regions (F) and (G). The figure indicates no significant discrepancy in effective strain distribution at the upper region, but it did present a conflicting deformation behavior between regions (F) and (G) 0-3 mm near the bottom of the specimen. The effective strain value at the bottom region of region (F) is approximately 1.03, while in region (G) the effective strain is approximately 4.23. This disparity seems to be originated from the back stress that filled up the corner gap at the first deforming zone (Ref 12, 13). Hence, the continuous ECMAP process that was designed as an improvement to the ECAP process is, within the region from the specimenÕs tip to 4W, similar to the repeated procedure of Journal of Materials Engineering and Performance Fig. 6 Deformed geometry and effective strain distribution for the continuous type ECMAP 4.5 G part steady state F part steady state 4.0 Effective strain 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0 2 4 6 8 10 Distance, mm Fig. 7 Path plot of effective strain along the thickness directions in regions F and G ECAP through route A, but the development of effective strain is dissimilar beyond 4W. 3.2 Deformation Behavior of Materials Processed Under Modified Continuous ECMAP For continuous ECMAP to accurately represent two pass route A ECAP in terms of overall deformation homogeneity and deformation behavior, a design that has an out corner angle of 20°, illustrated in Fig. 8, was considered after trying various angles for the optimum combination of deformation homogeneity and pressing load. The stages (A)-(E), like the ones previously mentioned, are specified. One can notice from stages (C) and (D) that by setting an out round corner, despite the back stress derived from the second deforming zone, the localized deformation at bottom region of the specimen can be manipulated. Figure 9 compares the effective strain distribution of the Journal of Materials Engineering and Performance original ECMAP process to the modified ECMAP process. From this figure one can detect a distinct difference in strain distribution from the specimenÕs tip to 4W under. Figure 10 plots the effective strain from bottom to top region of the specimen based on the information from Fig. 9. According to Fig. 10, the bottom region of the specimen processed through the modified ECMAP has an effective strain of 1.26, a significantly lower value than the 4.23 of the specimen processed through the original ECMAP. Average effective strain and standard deviation were employed to examine the homogeneity (Fig. 11), and the results indicate lower average effective strain and standard deviation for the case of modified ECMAP. Moreover, while the maximum difference in standard deviation of effective strain from the original ECMAP was 1.67, the modified ECMAP was 1.396, establishing the importance of the corner angle of the first channel in terms of deformation homogeneity. Hence, it seems reasonable to state that design that incorporates corner angles at every channel except the last should be considered in order to achieve deformation homogeneity. Figure 12 shows the comparison of load histories for ECAP, original ECMAP, and modified ECMAP. The load change for ECAP process can be divided into three stages. First stage is the increase in load due to the initial deformation of the specimen. The second stage is when the specimen tip exits the initial channel, causing a decrease in load. Lastly, the third stage is when the specimen deformation reaches a steady state condition (Ref 19). The specimen processed through the repeated procedure of ECAP through route A experiences a longer second stage compared to the one processed through the single procedure of ECAP because the former one consists of folding defect (Ref 11, 19). Also, the load histories of the original ECMAP and the modified ECMAP seem similar, but the latter one shows a smaller load because the folding defect was avoided due to the corner angle. Nevertheless, the overall load of modified ECMAP is still large because of the back stress caused by the multi-angular channel. Volume 22(11) November 2013—3225 Fig. 8 Deformed geometry with effective strain distribution under the modified ECMAP die 4.5 Modified-ECMAP ECMAP 4.0 Effective strain 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0 2 4 6 8 10 Distance, mm Fig. 10 Path plot of effective strain along the thickness directions in regions indicated in Fig. 9 3.5 Fig. 9 Effective strain distribution (a) in the original die and (b) in the modified ECMAP die 3.0 SD:0.835 3226—Volume 22(11) November 2013 Effective strain 4. Conclusions This research discussed about the effective design and the deformation homogeneity of the continuous ECAP process, which has been a heated research topic for processing bulk materials for ultrafine grains. Previously proposed design of the continuous ECMAP process that was designed to maximize the efficiency of the original batch type ECAP failed to maintain deformation homogeneity due to the back stress of multi-angle channels. To resolve the matter, this research has proposed a modified design of ECMAP that contains an out corner angle of 20°. The results presenting decreased average effective strain and standard deviation suggest that the proposed design is in *SD: Standard Deviation *AES: Average Effective Strain 2.5 2.0 SD:0.698 AES:1.98 AES:1.8 1.5 1.0 0.5 ECMAP ECMAP-Modified Fig. 11 Average effective strain and standard deviation values after original ECMAP and modified ECMAP Journal of Materials Engineering and Performance Fig. 12 Comparison of load histories for batch type ECAP, ECMAP of original die, and ECMAP of the modified die fact successful in controlling the degree of back stress, and thus the conservation of deformation homogeneity. Acknowledgments This study was supported by a grant from the Fundamental R&D Program for Core Technology of Materials (10037206) funded by the Ministry of Knowledge Economy, Korea. References 1. R.Z. Valiev, Y.V. Ivanisenko, E.F. Rauch, and B. Baudelet, Structure and Deformation Behaviour of Armco Iron Subjected to Severe Plastic Deformation, Acta Mater., 1996, 44, p 4705–4712 2. Y. Iwahashi, J. Wang, Z. Horita, M. Nemato, and T.G. Langdon, Principle of Equal-Channel Angular Pressing for the Processing of Ultra-Fine Grained Materials, Scr. Mater., 1996, 35, p 143–146 3. Y.C. Chen, Y.Y. Huang, C.P. Chang, and P.W. Kao, The Effect of Extrusion Temperature on the Development of Deformation Microstructures in 5052 Aluminium Alloy Processed by Equal Channel Angular Extrusion, Acta Mater., 2003, 51, p 2005–2015 Journal of Materials Engineering and Performance 4. I.H. Lee, S.I. Hong, and K.H. Lee, Microstructural Evolution of Cu-15 wt% Ag Composites Processed by Equal Channel Angular Pressing, Korean J. Met. Mater., 2012, 50, p 931–938 5. B. Hadzima, M. Janeček, Y. Estrin, and H.S. Kim, Microstructure and Corrosion Properties of Ultrafine-Grained Interstitial Free Steel, Mater. Sci. Eng. A, 2007, 462, p 243–247 6. S.C. Yoon, S.J. 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Imura, Impact Toughness of an UltrafineGrained Al-11 mass% Si Alloy Processed by Rotary-Die EqualChannel Angular Pressing, Acta Mater., 2005, 53, p 211–220 17. A. Ma, N. Saito, M. Takai, Y. Nishida, H. Iwata, K. Suzuki, I. Shigematsu, and A. Watazu, Effect of Severe Plastic Deformation on Tensile Properties of a Cast Al-11 mass% Si Alloy, Mater. Sci. Eng. A, 2005, 395, p 70–76 18. H.S. Kim, Finite Element Analysis of Equal Channel Angular Pressing Using a Round Corner Die, Mater. Sci. Eng. A, 2001, 315, p 122–128 19. S.C. Yoon, M.H. Seo, and H.S. Kim, Preform Effect on the Plastic Deformation Behavior of Workpieces in Equal Channel Angular Pressing, Scr. Mater., 2006, 55, p 159–162 Volume 22(11) November 2013—3227
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