UL PERFORMANCE MATERIALS UL Thermoplastics Testing Center (UL TTC) UL TTC Service Specifications Advanced Technology and Extensive Capabilities For speed to market The UL Thermoplastics Testing Center (UL TTC) at Chempark in Krefeld-Uerdingen is a leading international supplier for compounding, test specimen production and testing and certification of innovative plastics – from polyolefins to high-performance thermoplastics. The following pages provide specifics on the diverse processes and extensive testing capabilities at UL TTC. In addition, we regularly fulfill requests for special tests, specimens, or standards not listed. Let us apply our experience, resources and creativity to solve your unique challenges. When you choose the Thermoplastics Testing Center, you are opting for the proven performance of an accredited testing organisation offering all-inclusive services Compounding Twin screw extrusion One-STop Service • Small quantity compounds of at least 1,3 – 200 kg* • C ompounding • The main thermoplastics processed are: • P roduction of test specimens – Polycarbonates (PC, PC-HT) • S tandard testing – Polyamides and polyesters • T est engineering consultation (PA 6, PA 6.6, Co-PA, PET, PBT) • C ertification – Styrenics (ABS, ASA and SAN) • F ollow-Up Service – Blends of the above-mentioned plastics • Weighing in of formulations • Mixing of raw materials in high speed mixer • Shredding * Other quantity on request Production of Test Specimens Other test specimens on request. All dimensions listed in mm Sheet production Special test specimens Sheets with optical quality Flat test specimens (only unreinforced materials) 50 x 6 x 4,0 150 x 105 x 1,5 150 x 105 x 4,0 250 x 105 x 3,2 60 x 10 x 1,0 150 x 105 x 1,6 150 x 105 x 6,0 250 x 105 x 6,4 63,5 x 12,7 x 3,2 150 x 105 x 2,0 150 x 105 x 6,4 220 x 140 x 4,0 80 x 10 x 1,0 150 x 105 x 3,0 250 x 105 x 1,6 80 x 10 x 3,0 150 x 105 x 3,2 250 x 105 x 2,3 80 x 10 x 4,0 (with weld line) 120 x 10 x 4,0 120 x 15 x 4,0 Sheets with grained surfaces 150 x 105 x 3,0 150 x 105 x 4,0 150 x 105 x 3,2 220 x 140 x 4,0 Dumbbell test specimens 63,5 x 3,2 x 0,8 (Type L) 63,5 x 3,2 x 0,8 (Type S) Sheets 150 x 105 x d d = 1,0 / 1,2 / 1,5 / 2,0 / 2,2 / 2,4 / 2,5 / 2,7 / 3,0 / 3,2 / 4,0 / 6,0 / 10,0 63,5 x 3,2 x 3,0 (Type S) 85 x 5,0 x 1,5 (ISO 527-2 Typ 1BA) Sheets 150 x 150 x d 105 x 6 x 1,5 d = 2,0 / 2,5 / 3,0 105 x 6 x 2,0 Other Wall Thicknesses on request 105 x 6 x 3,0 105 x 6 x 4,0 Sheets for shrinkage measurement Rectangular sheet 60 x 60 x 2,0 Rectangular sheet 150 x 105 x 3,0 Rectangular sheets; also with optical quality Sample sheet 60 x 40 x 2,0 CAMPUS® test specimens Thin Wall test specimens Sample sheet 60 x 40 x 4,0 Sample sheet with step 60 x 40 x 4/2-step Rectangular sheet 60 x 60 x 1,0 60 x 60 x 0,4 125 x 13 x 0,4 Rectangular sheet 150 x 38 x 2,0* Rectangular sheet 60 x 60 x 2,0 60 x 60 x 0,5 125 x 13 x 0,5 Rectangular sheet 155 x 75 x 2,3 Flat test specimen 80 x 10 x 4,0 60 x 60 x 0,6 125 x 13 x 0,6 Rectangular sheet with hole 155 x 75 x 2,3 Dumbbell test specimen 170 x 10 x 4,0 60 x 60 x 0,7 125 x 13 x 0,7 Rectangular sheet with hole and ribs155 x 75 x 2,3 Flat test specimen 125 x 13 x 0,75 / 1,5 / 3 60 x 60 x 0,8 125 x 13 x 0,8 Rectangular sheet 60 x 60 x 1,0 60 x 60 x 0,9 Rectangular sheet 60 x 60 x 2,0 60 x 60 x 1,0 Rectangular sheet 60 x 60 x 3,0 Rectangular sheet 75 x 50 x 2,0 Rectangular sheet 75 x 50 x 4,0 125 x 13 x 0,75 125 x 13 x 2,0 125 x 13 x 0,80 125 x 13 x 2,2 Determination of processing properties 125 x 13 x 0,85 125 x 13 x 2,4 • Injection pressure Sample sheet with step 75 x 50 x 4/1-step Sample sheet with step 75 x 50 x 3/2-step 125 x 13 x 0,90 125 x 13 x 2,6 • Gate open time 125 x 13 x 1,0 125 x 13 x 2,8 • Plasticising performance 125 x 13 x 1,2 125 x 13 x 3,0 • Demolding properties / Friction coefficient 125 x 13 x 1,4 125 x 13 x 3,2 125 x 13 x 1,5 125 x 13 x 3,8 125 x 13 x 1,6 125 x 13 x 6,4 125 x 13 x 1,8 Other wall thicknesses on request Test specimens from semi-finished and finished parts • Produced by high-speed cutting, sawing and punching 63,5 x 3,2 x 1,5 (Type S) 63,5 x 3,2 x 3,0 (Type L) (shrinkage marks on one side) UL test specimens, flat test specimens 63,5 x 3,2 x 1,5 (Type L) Round test specimen; also with optical quality D25 x 1,7* D80 x 0,8 D80 x 2,5 D60 x 1,0 D80 x 1,0 D80 x 3,0 D60 x 2,0 D80 x 1,2 D80 x 3,2 D60 x 3,0 D80 x 1,5 D80 x 4,0 D60 x 4,0 D80 x 1,6 D100 x 0,75* D80 x 0,5 D80 x 2,0 105 x 10 x 0,75 105 x 10 x 1,5 105 x 10 x 3,0 120 x 7 x 2,0 130 x 10 x 1,5 130 x 10 x 2,0 130 x 10 x 3,0 130 x 10 x 4,0 170 x 10 x 1,0 170 x 10 x 1,5 170 x 10 x 2,0 170 x 10 x 3,0 (according to ISO 527-2 Typ 1A) 170 x 10 x 3,2 (according to ISO 527-2 Typ 1B) 170 x 10 x 4,0 170 x 10 x 4,0 with weld line 170 x 13 x 3,2 (ASTM D638 Typ 1) Others Flow strip 440 x 50 x 0,5 Flow strip 440 x 50 x 0,7 Flow strip 440 x 50 x 1,0 Flow strip 440 x 50 x 1,5 Flow strip 440 x 50 x 2,0 Flow strip 440 x 50 x 3,0 Flow Spiral – flat 1150 x 5 x 2,0 Flow Spiral – flat 1170 x 8 x 2,0 * not with optical quality Test Procedures Additional standards and tests (as well automotive- and electrical test-regulations) on request Electrical test procedures Dielectrical measurement Dielectric constant εr/ dissipation factor tan δ) • IEC 60250 Electrostatic charging • on the basis of IEC 61340 • in-house standard Electrical Resistance Surface resistivity of insulating material • DIN IEC 60093 • ASTM D257 Volume resistivity of insulating material • DIN IEC 60093 • ASTM D257 Mechanical test procedures Penetration test Tensile test with modulus of elasticity -40 °C to room temperature elasticity • ISO 6603-2 (to max. 10 kN) Melt index • ISO 604 Melt volume flow rate (MVR) • ASTM D695 Melt mass flow rate (MFR) • DIN 53454/53457* Time dependent melt -40 °C bis +200 °C • ASTM D3763 • ISO 37 • ISO 527 • ASTM D638 • DIN 53455/53457 * High speed tensile test optical deformation measurement Determination of hardness Compression test with modulus of Rheological test procedures Ball indentation hardness volume rate (IMVR) • ISO 2039-1 Shear test Time dependent melt flow rate (IMFR) Micro hardness IRHD • ASTM D732 • ISO 1133 • ASTM D1238 • ISO 48 Rockwell hardness by ultra high speed camera Taber abrasion test • ISO 2039-2 • ISO 9352 Melt shear viscosity -40 °C to +200 °C • ASTM D785 • ASTM D1044 • ISO 11443 0,1 m/s to 20 m/s Shore A/Shore D • DIN 53754 • DIN 54811* • in-house standard • ISO 868 Tensile creep test Solution viscosity Flexural test with modulus of elasticity -40 °C to +200 °C • ISO 178 • DIN 53505* Room temperature to 250 °C of Polycarbonate with/without film Tensile impact test • ISO 899-1 • ISO 1628-1/-4 • ISO 8256 • DIN 53444* • DIN 51562-3 Compression Set Oscillatory shearing • ASTM D790 • DIN 53448 • DIN 53452/53457 * • DIN EN ISO 8256 Izod & Charpy flexural impact tests (notched and unnotched) -60 °C to +40°C • ISO 179-1 • ASTM D1822 • ISO 815 (rotational rheometer) • ASTM D395 e.g. zero shear viscosity, frequency Tear propagation/separation/ sweep, time sweep/thermal stability -40 °C to +200 °C • ASTM D4440 peeling tests • ISO 180 • ISO 34-1 • ASTM D256 • DIN 53507* • DIN 53453 * • DIN 53515* Volume resistivity of conductive material Special rheological tests • ISO 3915 • Capillary and rotational rheometer Surface resistivity • IEC 60167 pvT-Behavior • IEC 62631-3-3 • ISO 17744 Dielectric strength Heat resistance Vicat • IEC 60243-1 • ASTM D149 to 300 °C Comparative Tracking Index/CTI • ISO 306 • DIN IEC 60112 • ASTM D1525 • ASTM D3638 HDT Heat distortion Arc resistance Temperature to 300 °C • IEC 61621 • ISO 75-1,-2,-3 • ASTM D495 • ASTM D648 Ball pressure • IEC 60695-10-2 (IEC 60335-1) Electrolytic Corrosion • IEC 60426 Inclined plane tracking (IPT) • DIN IEC 60587 • ASTM D2303 • ISO 6721-10 • DIN 53356 • DIN 53363 * These Standards are withdrawn but are still feasible at UL Test Procedures (CONTINUED) Additional standards and tests (as well automotive- and electrical test-regulations) on request Flammability Thermal aging Automotive Flame Tests UL94 Hot air aging in no-load conditions • PV 1306 • HB (Horizontal Burning) • DIN 53497 • PV 3929 (Kalahari-Test) • V (50Watt-20mm Vertical) • ISO 188 • PV 3930 (Florida-Test) • 5V (500Watt-125mm Vertical) • VTM (Vertical Thin Materials) • HBF (Horizontal Burning Foamed Material) Oxygen Index LOI (Low Oxygen Index) Determination of Relative Temperature Index (RTI) • IEC 60695-2-11 GWEPT (Glow Wire End Product Testing) • IEC 60695-2-12 GWFI (Glow Wire Flammibility Index) • IEC 60695-2-13 GWIT (Glow Wire Ignition Temperature) • ASTM D3874 HWI • IEC 60695-11-5 Ash Content • D27 1389 • D27 1911 • NES M 0135 • UL 746 B • GMW 14650 • VDA 75202 Weathering Artificial Weathering (Many Standards available on request for accelerated aging test with various Climate testing Climate Tests on request various standards for climate Optical test procedures Yellowness Index Differential scanning calorimetry (DSC) • DIN 6167 also temperature modulated method • ASTM E313 • ISO 11357 customer specifications with different change tests and constant climate Color measurement Delta E machines like Xenon-WOM, Xenotest, conditions • ISO 13468 Autoclave storage • ASTM E308 Flourescence (UVA-/UVB Licht 313nm, 340nm, 351nm)) (Hot Wire Ignition) Needle Flame Test • FLTM BO 116-01 • IEC 60216 • ISO 4589-2 Test with Electrical Ignition Source • PV 1303 • up to +150°C • ASTM E179 • DIN 5033 • AATCC TM 16 • DIN 5036 • AATCC TM 169 • DIN 6174 • ASTM G154 Conditioning • ISO 1110 • ASTM G155 • ASTM D7869 Automotive Gray scale determination • ISO 105-A02 • ISO 3451-1 Verfahren A • ISO 4892-2,-3 • In-House standard (rapid ash) • ISO 105-B • PV 2005 Gloss factor • DIN EN ISO 16474 • PR 303.5 • ISO 2813 Automotive • US-FMVSS 302 (KFZ-Interior) • PV 1200 • SAE J 2412 (SAE J1885) • ASTM D523 • SAE J 2527 (SAE J1960) • DIN 67530 •D IN 75200 (KFZ-Interior) • I SO 3795 (KFZ-Interior) •T L 1010 (KFZ-Interior) •P V 3343 (Fuel Pipe) Haze • ASTM D1003 • DIN 53765* Spectroscopic Methods Thermogravimetric analysis (TGA) • ISO 7111 UV-VIS-NIR Spectroscopy • ISO 11358 • von 175 nm to 3300 nm • DIN 51006 IR/ATR Spectroscopy Torsion pendulum test • UL 746A (shear modulus determination) • ISO 6721-7 forced vibration Thermal analyses Thermomechanical analysis (TMA) Microscale Combustion Calorimetry Coefficient of linear thermal expansion - 150 °C to 600 °C (MCC) • ASTM D7309 • ISO 11359-1/-2 • DIN 53752* • ASTM D1044 •P V 3357 (Insulation Material) * These Standards are withdrawn but are still feasible at UL Test Procedures (CONTINUED) Chemical resistance Physical test procedures Shrinkage Environmental stress cracking (ESC), Thermal conductivity Production and measurement of Bent strip test • ISO 22088-3 Internal stresses NanoFlash™-test method • ISO 22007-4 shrinkage station • ASTM E1461 • ISO 294-4 TnP-Test Determination of density • In-House Standard • ISO 1183 • ASTM D792 Petrol test • DIN 53749* (isooctane/toluene) Fuel resistance shrinkage sheets on fully-automated Density • ISO 845 Additional Services • Engineering Consultation: Compounding, test specimen production and testing • F ailure Analysis • DIN 51604-1 • DBL 5416 Apparent density • ISO 60 Media aging, no load • ISO 175 Determination of water content • ISO 1817 • ISO 760 • DIN 53715* • ISO 15512 Water absorption • ISO 62 • U L TTC Mold-Control (System for determining process data for injection molding) • Test Lab Implementation Dubai T: +971.4.558.5900 E: [email 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