X-ray counting system DM0011 1 SENS-TECH SENSOR TECHNOLOGIES description The DM0011 is a wide dynamic range, X-ray counting system. X-rays up to 100 keV are detected using a scintillator coupled to a photomultiplier and signal processing electronics to provide a TTL output. The detector uses a window discriminator to detect X-rays within a selected energy band. The width and threshold (lower limit) of the window and the HV of the photomultiplier can be set by the user with the DM0011CONTROL. A schematic of the window discriminator and read out is shown in section 5. Fast count rates are achieved by using a YAP(Ce) scintillator, selected for its very fast (30 ns) decay time, and high speed electronics, designed to minimise dead-time. A plot of indicated counts against true counts is shown in section 6. As well as counting X-rays in a set energy band, the unit can be used to generate an energy spectrum by using a narrow (energy) window and progressively increasing the lower threshold. This feature is also used to calibrate the detector, using gamma and X-ray sources of known energy. A sample energy spectrum is shown in section 7. 5 window discriminator schematic Only pulses falling in the window, between the lower level (LLD) and upper level (ULD) are detected. 2 applications The unit is designed to count X-rays in laboratory or production equipment and in synchrotron radiation experiments. shaping amplifier YAP(Ce) logic and O/P driver ULD pmt X-ray 3 features +HV +HV · 10 MHz count capability · 0.15 Hz background count · adjustable window discriminator · adjustable sensitivity · compact assembly · operates from a single low voltage supply · TTL output 0.100 V 3.00 V variable, 3 V max 10 MHz max (note 1) 5 MHz max YAP (Ce) 21.8 mm dia 0.15 Hz (note 2) +4.75 V min +5.25 V max ripple < 100 mV pk-pk 60 mA max at 1 MHz count rate note 1: after dead-time correction note 2: 0.15 Hz maximum (8 keV to 50 keV), unit shielded with 6 mm of lead signal > ULD 0V output 37 ns indicated counts vs true counts The true count rate N can be calculated from the measured -Nt value n by iteration, using the expression n = Ne , where t is the dead-time. This may be approximated for nt <<1 to N = n/(1-nt ). n MHz supply current 5 keV to 100 keV signal < LLD LLD < signal < ULD LLD 6 4 specification detection range window discriminator lower (min) upper (max) window width count rate actual counts indicated counts scintillator background counts supply voltage ULD LLD 10 9 8 7 6 5 4 3 2 1 0 0 1 2 n 3 4 5 6 N MHz linear response 7 8 9 10 n = Nexp(-Nt ) 9 outline drawing (mm) 35.0 dia The detector is calibrated using very low activitity sources; for 55 241 example, Fe (5.9 keV), Am (17.0 keV and 59.5 keV). The discriminator window is set, using the DM0011 CONTROL, to the lowest width of 50 mV. The lower threshold of the window is raised in steps, from a minimum of 50 mV up to a maximum of 3 V. The counts are recorded at each step and plotted against the voltage of the window centre (= threshold voltage plus half the window width). The voltage of the window centre has a linear relationship to the mean energy of the detected X-rays, enabling an energy spectrum to be produced, as illustrated in the figure below. 21.8 active dia ±0.25 ±0.25 ±0.25 31.00 29.00 62.0 calibration and generation of energy spectra 7 DM0011 data sheet page 2 'C' 'A’ 'B' 800 600 200 connectors 5.9 keV 0 200 400 600 800 1000 window centre mV 1200 55 Fe 1400 ‘A’ - TTL signal out BNC ‘B’ - power input Lemo EGG.00.302.CLL pin 1 +5 V pin 2 0 V ‘C’ - control unit interface 241 Am The coordinates of the three peak positions are transferred to a linear calibration curve relating X-ray energy to mV setting, as shown. Alternatively, the scale on the x axis in the above graph may be expressed in keV by using the calibration curve. The detector can then be used to generate the absolute energy spectrum of an unknown X-ray source by using the some procedure as for calibration. scintillation crystal photomultiplier type 9107SB08 ±0.5 59.5 keV 400 0 alternative connector positions for DM0011-01 shown dotted 80.0 count Hz 17.0 keV pin 1, signified by red dot on rim of aperture 'A' energy, keV ±0.25 60 'B' 50 80.00 70 40 30 'C' 20 10 0 0 200 400 600 800 window centre mV 1000 1200 standard connector positions for DM0011 ±0.25 118.00 10 precautions Avoid touching the scintillation crystal window. It is a very thin membrane and, consequently, is very delicate. Sens-Tech Limited 6A Langley Business Centre, Station Road, Langley Berkshire, SL3 8DS, UK tel: +44 (0)1753 214714 fax: +44 (0)1753 214715 e-mail: [email protected] The company reserves the right to modify these designs and specifications without notice. Developmental devices are intended for evaluation and no obligation is assumed for future manufacture. While every effort is made to ensure accuracy of published information the company cannot be held responsible for errors or consequences arising therefrom. an ISO 9001 registered company www.sens-tech.com SENS-TECH SENSOR TECHNOLOGIES © Sens-Tech Limited, 2007 DS_ DM0011 issue 1 30 march 2007
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