Stewart Assay and Environmental Laboratories LLC APPROVE Chief of АС МED КR ___________ D. Urmanbetov Seal Attachment to accreditation certificate № ________________________________________ of «_____»____________________________200___г. SCOPE OF ACCREDITATION Laboratory of Stewart Assay and Environmental Laboratories LLC No. 1 1 Name of testing objects Identification of the document on production, standards of control 2 Ores and their processed products, geological samples. 3 - Name of the tests/determinate indicators 4 Sample preparation (crushing, pulverizing, screening) for analysis Marking of document on testing methods/ determinate indexes 5 SAEL-SP-1 Range of dimensions, unit of measure* Fineness of crushing Fineness of pulverization 6 -2 mm -0.075mm 2 Ores and their processed products, geological samples. - Au by Fire Assay with Atomicabsorption finish. SAEL-AuFA1A Au 0.002 – 10 g/t 3 Ores and their processed products, geological samples. - Au by Fire Assay with Atomicabsorption finish. AuFA2 Au 0.010 – 10 g/t Managing Director of Stewart Assay and Environmental Laboratories LLC SEAL Schudro V.K. Laboratory Manager of Stewart Assay and Environmental Laboratories LLC Imanakunov S.B. page. 1 of 7 Stewart Assay and Environmental Laboratories LLC 1 4 2 Ores and their processed products, geological samples. Managing Director of Stewart Assay and Environmental Laboratories LLC SEAL Schudro V.K. 3 - 4 Multi-element analysis by atomicemission spectrometer with inductively coupled plasma after preliminary chemical digestion of samples. Elements to be determined: Silver Aluminium Arsenic Barium Beryllium Bismuth Calcium Cadmium Cobalt Chromium Copper Iron Mercury Potassium Lanthanum Magnesium Manganese Molybdenum Sodium Nickel Phosphorus Lead Antimony Scandium Selenium Tin Strontium Tellurium Titanium Vanadium Tungsten Yttrium Zinc Zirconium Uranium 5 6 SAEL-WA-1/1 SAEL-ICP-1 Silver Aluminum Arsenic Barium Beryllium Bismuth Calcium Cadmium Cobalt Chromium Copper Iron Mercury Potassium Lanthanum Magnesium Manganese Molybdenum Sodium Nickel Phosphorus Lead Antimony Scandium Selenium Tin Strontium Tellurium Titanium Vanadium Tungsten Yttrium Zinc Zirconium Uranium 1-100g/t 0.01-5% 1.5g/t-1% 0.25g/t-1% 0.05-500g/t 3.5g/t-1% 0.01-5% 0.25-500g/t, 0.25g/t-1% 0.5g/t-1% 0.25g/t-1% 0.01-5% 0.5-1000g/t 0.01-5% 1g/t-1% 0.01-5% 0.5g/t-1% 0.5g/t-1% 0.01-5% 0.5g/t-1% 5g/t-1% 3.5g/t-1% 2.5g/t-1% 0.1g/t-1% 1.5-1000g/t 2.5-1000g/t 0.25g/t.-1% 5g/t-1% 2.5g/t-1% 1g/t-1% 5g/t-1% 0.25-1000g/t 0.5g/t-1% 0.5g/t-1% 50g/t-1% Laboratory Manager of Stewart Assay and Environmental Laboratories LLC Imanakunov S.B. page. 2 of 7 Stewart Assay and Environmental Laboratories LLC 1 5 2 Ores and their processed products, geological samples. 3 6 Environmental samples (natural and sewage) - Managing Director of Stewart Assay and Environmental Laboratories LLC SEAL Schudro V.K. 4 Determination of silver by atomicabsorption method after a preliminary chemical digestion of samples. Multi-element analysis by atomicemission spectrometer with inductively coupled plasma. Elements to be determined: Silver Aluminium Arsenic Barium Beryllium Calcium Cadmium Cobalt Chromium Copper Iron Mercury Potassium Magnesium Manganese Molybdenum Sodium Nickel Lead Antimony Zinc Selenium Silicon Vanadium Uranium 5 SAEL-WA-3 SAEL-AA-2 Silver 6 1-100ppm SAEL-ICP-2 Silver Aluminum Arsenic Barium Beryllium Calcium Cadmium Cobalt Chromium Copper Iron Mercury Potassium Magnesium Manganese Molybdenum Sodium Nickel Lead Antimony Zinc Selenium Silicon Vanadium Uranium 0.003-1mg/L 0.03-10mg/L 0.04-1mg/L 0.001-1mg/L 0.0002-0.1mg/L 0.02-200mg/L 0.002-1mg/L 0.004-1mg/L 0.008-1mg/L 0.005-1mg/L 0.003-10mg/L 0.01-10mg/L 0.09-100mg/L 0.05-100mg/L 0.001-1mg/L 0.004-1mg/L 0.02-200mg/L 0.01-1mg/L 0.02-1mg/L 0.02-1mg/L 0.0007-1mg/L 0.02-1mg/L 0.01-20mg/L 0.006-1mg/L 5-10mg/L Laboratory Manager of Stewart Assay and Environmental Laboratories LLC Imanakunov S.B. page. 3 of 7 Stewart Assay and Environmental Laboratories LLC 1 7 2 Air dust on filter 3 - 4 Determination of metals by atomicemission method with inductively coupled plasma after a preliminary chemical digestion. Beryllium Manganese Zinc Calcium Barium Iron Aluminium Cobalt Magnesium Nickel Lead Copper 5 6 SAEL-WA-4 SAEL-ICP-2 Beryllium Manganese Zinc Calcium Barium Iron Aluminium Cobalt Magnesium Nickel Lead Copper 0.00020.1mg/L 0.001-1mg/L 0.0007-1mg/L 0.02-200mg/L 0.001-1mg/L 0.003-10mg/L 0.03-10mg/L 0.004-1mg/L 0.05-100mg/L 0.01-1mg/L 0.02-1mg/L 0.005-1mg/L 8 Air dust on filter - Determination of lead by atomic emission method with inductively coupled plasma after a preliminary chemical digestion SAEL-WA-27 SAEL-ICP-2 Lead 0.02-1mg/L 9 Air dust on filter - Determination of silica oxide by atomic emission method with inductively coupled plasma after a preliminary chemical digestion SAEL-WA-28 SAEL-ICP-2 Silica oxide 0.02-1mg/L 10 Environmental samples (ground waters) - Determination of total cyanide by photo colorimetric method or by titration. Determination of cyanide, CN WAD by photo colorimetric method or by titration. Determination of free cyanide by photo colorimetric method СЭВ. Унифицированные методы исследования качества вод. Ч.1, М., 1977г. стр. 775 CN total 0.005-30mg/L Managing Director of Stewart Assay and Environmental Laboratories LLC SEAL Schudro V.K. Laboratory Manager of Stewart Assay and Environmental Laboratories LLC Imanakunov S.B. page. 4 of 7 Stewart Assay and Environmental Laboratories LLC 1 11 2 Environmental samples (ground waters) 3 - 4 Determination of carbonate and bicarbonate by volumetric method 5 СЭВ. Unified methods of water quality research. P.1, M., 1977. page 222 12 Environmental samples (ground waters) - Determination of total alkalinity by volumetric method Total alkalinity 1-1000 mg/L 13 Environmental samples (ground waters) - Determination of total phosphorus photo colorimetric method P 0.01-50 mg/L 14 Environmental samples (ground waters) - Determination of suspended solids by gravimetric method Suspended solids 1-10000 mg/L 15 Environmental samples (ground waters) - Determination of nitrite by photo colorimetric method СЭВ. Unified methods of water quality research. P.1, M., 1977. page 813 СЭВ. Unified methods of water quality research. P.1, M., 1977. page 694 MH KR. Collection of standardized methods for water analysis. Bishkek, 2000, page 43 СЭВ. Unified methods of water quality research. P.1, M., 1977. page 419 NO2 0.001-50 mg/L 16 Environmental samples (ground waters) - Determination of nitrate by photo colorimetric method СЭВ. Unified methods of water quality research. P.1, M., 1977. page 397 NO3 0.1-50 mg/L 17 Environmental samples (ground waters) - Determination of sulfate by gravimetric method СЭВ. Unified methods of water quality research. P.1, M., 1977. page 613 SO4 1-1000 mg/L 18 Environmental samples (ground waters) - Determination of chloride by titration СЭВ. Unified methods of water quality research. P.1, M., 1977. page 743 Cl 0.5-1000 mg/L 19 Environmental samples (ground waters) - Determination of dry residue by gravimetric method Dry residue 1-10000 mg/L 20 Environmental samples (ground waters) - Determination of thiocyanate by photo colorimetric method MH KR. Collection of standardized methods for water analysis. Bishkek, 2000, page 51 СЭВ. Unified methods of water quality research. P.1, M., 1977. page 546 SCN 0.05-25 mg/L 21 Environmental samples (ground waters) - Determination of turbidity by nephelometric method SAEL-WA-23 Turbidity 0.01-1000NTU Managing Director of Stewart Assay and Environmental Laboratories LLC SEAL Schudro V.K. CO3 HCO3 6 1-1000 mg/L 1-1000 mg/L Laboratory Manager of Stewart Assay and Environmental Laboratories LLC Imanakunov S.B. page. 5 of 7 Stewart Assay and Environmental Laboratories LLC 1 22 2 Environmental samples (ground waters) 3 - 4 Determination of рН by potentiometric method 5 СЭВ. Unified methods of water quality research. P.1, M., 1977. page 252 23 Environmental samples (ground waters) - Determination of total hardness by titration Total hardness 1-1000 mg/L 24 Environmental samples (ground waters) - Determination of ammonium by photo colorimetric method СЭВ. Unified methods of water quality research. P.1, M., 1977. page 172 СЭВ. Unified methods of water quality research. P.1, M., 1977. page 69 NH3 0.04-50 mg/L 25 Environmental samples (ground waters) - 0.04-50 mg/L Ores and their processed products, geological samples. - СЭВ. Unified methods of water quality research. P.1, M., 1977. page 47 SAEL-WA-40 SAEL-ICP-1 TKN 26 Determination of total nitrogen according to Kjeldhl by photo colorimetric method Determination of gold by cyanidation method (BLEG test) Au 0.010-10 г/т 27 Ores and their processed products, geological samples. Ores and their processed products, geological samples. Ores and their processed products, geological samples. - Determination of S total by Leco analyzer Determination of C total by Leco analyzer Determination of S sulfide by Leco analyzer after preliminary chemical processing SAEL-WA-42 S total 0.01-50% SAEL-WA-42 C total 0.01-50% SAEL-WA-36 S sulfide 0.01-50% 30 Ores and their processed products, geological samples. - Determination of C organic by Leco analyzer after preliminary chemical processing SAEL-WA-38 C organic 0.01-20% 31 Environmental samples (ground waters) - Determination of nitrate, nitrite, fluoride, chloride, sulfate, bromide and phosphate by ion chromatography. SAEL-WA-47 28 29 Managing Director of Stewart Assay and Environmental Laboratories LLC SEAL Schudro V.K. - рН Nitrate Nitrite Fluoride Chloride Sulfate Bromide 6 1-14 единиц рН 0.01-500mg/L 0.01-500mg/L 0.01-500mg/L 0.01-500mg/L 0.01-500mg/L 0.01-500mg/L 0.01-500mg/L Laboratory Manager of Stewart Assay and Environmental Laboratories LLC Imanakunov S.B. page. 6 of 7 Stewart Assay and Environmental Laboratories LLC 32 Biological materials (blood, urine, tissues, plants) Managing Director of Stewart Assay and Environmental Laboratories LLC SEAL Schudro V.K. - Determination of metals by atomicemission method with inductively coupled plasma after premineralization Iron Copper Manganese Cadmium Cobalt Lead Zinc SAEL-WA-46 SAEL-ICP-2 Iron Copper Manganese Cadmium Cobalt Lead Zinc 0.003-10mg/L 0.005-1mg/L 0.001-1mg/L 0.002-1mg/L 0.004-1mg/L 0.005-1mg/L 0.0007-1mg/L Laboratory Manager of Stewart Assay and Environmental Laboratories LLC Imanakunov S.B. page. 7 of 7
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