GEOL 322 – Mineralogy Spring, 2013 Lab 1: Introductory Mineral Identification! Mi ne r a l i de nt i f i c a t i on i s of t e n t he f i r s t s t e p i n unde r s t a ndi ng t he c ompl e x na t ur a l pr oc e s s e s t ha t a n Ea r t h s c i e nt i s t e nc ount e r s . The a na l ys i s a nd i de nt i f i c a t i on of mi ne r a l s c a n t a ke pl a c e a t di f f e r e nt l e ve l s of s ophi s t i c a t i on . For t hi s l a b we wi l l wor k on ha nd s pe c i me n i de nt i f i c a t i on, t he mos t ba s i c of mi ne r a l ogi c a l a na l ys e s . La t e r i n t he c our s e , mor e s ophi s t i c a t e d a na l yt i c a l t e c hni que s wi l l be i nt r oduc e d. As de s c r i be d i n Chapter 6 (all chapter and page numbers are in the Nesse textbook unless otherwise specified), t he r e a r e nume r ous pr ope r t i e s t ha t c a n be e va l ua t e d by vi s ua l i ns pe c t i on of a mi ne r a l s a mpl e , or wi t h t he us e of ve r y s i mpl e t e s t i ng e qui pme nt . The pur pos e of t hi s l a b i s f or you t o be c ome f a mi l i a r wi t h t he t e r mi nol ogy a nd me t hods c ommo nl y us e d i n mi ne r a l ogi c a l i d e nt i f i c a t i on of ha nd s a mpl e s . Some k e y pr ope r t i e s you wi l l be c ha r a c t e r i z i ng i n t hi s l a b i nc l ude : 1. Habit describes the threedimensional aspects of the crystal form. Se e Chapter 2 f or t e r ms us e d t o de s c r i be t he f or m or ha bi t of mi ne r a l s . Te r ms de s c r i bi ng t he c r ys t a l l ogr a phi c f or m s houl d be us e d whe r e a ppr opr i a t e ( e . g. c ube , r hombohe dr on, oc t a he dr on; s e e s e c t i ons on c r ys t a l f or ms , p. 3143) . Ot he r t e r ms us e d t o de s c r i be ha bi t a r e f ound on p. 4445. 1 2 Some t e r ms us e d t o de s c r i be habit a nd e xa mpl e s . Habit Definition Ac i c u l a r ve r y e l ong a t e d a nd needleshaped Bl a de d e l onga t e a n d f l a t t e ne d blades c ol umna r ; pr i s ma t i c columnlike Equa n t box s ha pe d wi t h equal di me ns i ons Fi br ou s a ggr e ga t e of hairlike, t hr e a dl i ke or ne e dl e l i ke c r ys t a l s f ol i a t e d; mi c a c e ous e a s i l y s e pa r a t e d i nt o sheets or l e a ve s Ma s s i v e no di s t i nc t s ha pe t a bul a r ; l a me l l a r tabletlike, one di me ns i on ma r ke dl y s ma l l e r t ha n t he ot he r t wo Example r ut i l e kya ni t e t our ma l i ne ga l e na a nt i gor i t e bi ot i t e c hr ys oc ol l a gyps um 2. Cleavage and fracture Cleavage is the tendency to split or break along planes, whereas Fracture is the irregular breakage of minerals. So me mi ne r a l s onl y ha ve c l e a va ge ( e . g. ha l i t e a nd c a l c i t e ) , s ome o nl y e xhi bi t f r a c t ur e ( e . g. be r yl a nd qua r t z ) , a nd s ome e xhi bi t bot h ( e . g. a mphi bol e s a nd py r oxe ne s ) . ( s e e p. 122) A good de s c r i pt i on of c l e a va ge s h oul d i nc l ude 3 f e a t ur e s : 1) The e a s e wi t h whi c h t he pl a ne c l e a ve s . Thi s c a n of t e n be de duc e d s i mpl y f r om t he s moot hne s s of pr e vi o us e xi s t i ng pl a ne s wi t hout a c t ua l l y de s t r oyi ng t he s a mpl e . ( perfect, good a nd poor c l e a va ge ) . 2) The numbe r of nonparallel c l e a va ge pl a ne s ( c l e a va ge pl a ne s i n di f f e r e nt or i e nt a t i ons ) . I t i s c ommon t o obs e r ve 1 ( basal c l e a va ge , a s i n mi c a s a nd t opa z ) , 2 ( prismatic c l e a va ge , a s i n a mphi bol e s a nd pyr oxe ne s ) , 3 ( cubic or rhombohedral c l e a va ge s e e pa r t 3) , 4 ( octahedral c l e a va ge , a s i n f l uor i t e ) , a nd 6 ( dodecahedral c l e a va ge , r a r e l y s e e n i n s pha l e r i t e ) . 3) The a ngl e be t we e n nonparallel c l e a va ge pl a ne s . 3 c l e a va ge s a l l a t 90 t o e a c h ot he r a r e r e f e r r e d t o a s cubic c l e a va ge ( a s i n ha l i t e ) ; 3 c l e a va ge s not a t 90 ( a s i n c a l c i t e ) a r e c a l l e d rhombohedral c l e a va ge . 3 Fracture is the manner in which the mineral breaks other than along planes of cleavage. ( s e e p. 123) Fracture Description Example c onc h oi da l s moot hl y curved, r i bbe d s ur f a c e obs i di a n Eve n ne a r l y flat s ur f a c e s ga r ne t Ha c kl y r a gge d s ur f a c e wi t h s ha r p e dge s a nd poi nt s na t i ve c oppe r i r r e gu l a r r ough a nd irregular s ur f a c e r hodoni t e s pl i nt e r y f i br ous or splintery f r a c t ur e s ur f a c e ( l i ke wood) pe c t ol i t e 3. Hardness is the resistance of a mineral to scratching and abrasion. Re l a t i ve ha r dne s s i s e xpr e s s e d on t he Mohs Hardness Scale. ( s e e p. 121) 4 Mineral Ta l c Gyps u m Mohs scale 1 2 Comparative Hardness 2. 5 Fi nge r na i l 2. 5 Al umi num Ca l c i t e 3 3. 5 Coppe r pe nny Fl uor i t e 4 4. 5 I r on Apa t i t e 5 5. 5 Kni f e bl a de 5. 5 Wi ndow gl a s s Or t hoc l a s e 6 6. 5 St e e l f i l e 6. 5 Por c e l a i n s t r e a k pl a t e Qua r t z Top a z Cor undu m Di a mo nd 7 8 9 10 4. Tenacity (p. 122) refers to the behavior of minerals when deformed or broken. 5. Luster and opacity (p. 125) Luster is the general appearance of a macroscopic fresh surface in reflected light. Opacity describes whether a mineral is transparent ( c a n s e e t hr ough mi ne r a l ) , translucent ( c a n onl y s e e l i ght t hr ough s a mpl e ) , or opaque ( doe s not t r a ns mi t l i ght ) . Th e l us t e r o f t r a ns pa r e nt mi ne r a l s i s r e l a t e d t o a pr ope r t y c a l l e d t he r e f r a c t i ve i nde x ( RI ) . Some l us t e r t e r ms a l ong wi t h e xa mpl e s : Luster Description Me t a l l i c s hi ny, metallic Nonmetallic Ada ma nt i ne br i l l i a nt a nd di a mond l i ke Vi t r e ous br i ght a nd glassy Gr e a s y a ppe a r s greasy or c oa t e d wi t h oi l Pe a r l y i r i de s c e nt , l i ke mot he r of pe a r l Si l ky l i ke s i l k, s a t i n, or s ome pol ye s t e r Re s i nous l us t e r of a r e s i n Ea r t hy dul l a nd di r t y l ooki ng 5 Mineral Type opa que mi ne r a l s mi ne r a l s wi t h hi gh RI mi ne r a l s wi t h me d. RI mi ne r a l s wi t h l ow/ hi RI l ook on c l e a va ge s ur f a c e f i br ous mi ne r a l s Example ga l e na z i r c on qua r t z , gl a s s ne phe l i ne a na l c i me gyps um s pha l e r i t e r ough or por ous mi ne r a l s ka ol i ni t e 6 6. Color and streak – our perception of the wavelengths of light reflected from or passing through the mineral. (p. 125) Some mi ne r a l s a r e a l wa ys t he s a me color. Ga l e na i s a l wa ys l e a d gr a y; a z ur i t e i s a l wa ys a s ha de of bl ue ( s ome t i me s s o da r k a s t o a l mos t l ook bl a c k) ; ma l a c hi t e i s a l wa ys a pa r t i c u l a r s ha de of gr e e n. I n t he s e mi ne r a l s c ol or c a n be a di a gnos t i c pr ope r t y. Mi ne r a l s s uc h a s qua r t z , c or undum, be r yl , c a l c i t e , a nd f l uor i t e a r e we l l known f or t he va r i e t y of c ol or s t he y di s pl a y. The s e c ol or s a r e of t e n a r e s ul t of t he pr e s e nc e of t r a c e qua nt i t i e s of non s t r uc t ur a l e l e me nt s . I n a ddi t i o n t o c he mi c a l c ompos i t i on, t he na t ur e a nd l oc a t i on of t he t r a c e e l e me nt wi t hi n t he c r ys t a l s t r uc t ur e i nf l ue nc e s t he c ol or of t he mi ne r a l . For i ns t a nc e , i r on oc c upyi ng t he c ha nne l s i n be r yl c r e a t e s t he bl ue c ol or of a qua ma r i ne , but i r on s ubs t i t u t i ng f or a l umi num i n t he be r yl s t r uc t ur e c r e a t e s t he ye l l ow c ol or of he l i odor . I n ma ny c a s e s , c ol or c a n gi ve c l ue s a bout t he c he mi c a l c ompos i t i on of t he mi ne r a l . Some e xa mpl e s of c ol or i ng a ge nt s i n mi n e r a l s i nc l ude : Cr ( gr e e n) i n e me r a l d, uva r ovi t e , t our ma l i ne ; Cr ( r e d) i n r uby; Cr ( pur pl e ) i n c hl or i t e ; Mn ( pi nk a nd r e d) i n pi e mont i t e , r hodoni t e , r hodoc hr os i t e ; Fe ( gr e e n t o br own t o a l mos t bl a c k) i n ol i vi ne , pyr oxe ne , e pi dot e ; Fe ( bl ue ) i n a qua ma r i ne ; Fe ( ye l l ow) i n he l i odo r , c i t r i ne ; Co ( l i l a c ) i n e r yt h r i t e ; Ni ( gr e e n) i n a nna be r gi t e ; Cu ( bl ue a nd gr e e n) i n ma l a c h i t e , a z ur i t e , t ur quoi s e ; U ( f l uor e s c e nt ye l l ows a nd gr e e ns ) i n c a r not i t e , a ut uni t e . Streak is the color of the mineral when it is finely powdered. The s t r e a k of a mi ne r a l ma y be di f f e r e nt f r om i t s c ol or , a nd i s us ua l l y c ons t a nt . 7. Density/Heft – density is mass per unit volume. Heft i s a wa y of e va l ua t i ng de ns i t y by hol di ng t he s a mpl e i n ha nd a nd c o mpa r i ng t he we i ght t o s a mpl e s i z e . ( p. 119120) I n t hi s l a b we wi l l not qua nt i f y t he s pe c i f i c gr a vi t y of mi ne r a l s , but you s houl d t a ke not e of t he he f t of e a c h mi ne r a l – i s i t not i c e a bl y l i ght e r or he a vi e r t ha n i s t ypi c a l ? 8. Other properties: r e a c t i on t o a c i d t a s t e s ome carbonates bubbl e wi t h HCl ; zeolites f or m a ge l halite t a s t e s s a l t y; sylvite t a s t e s bi t t e r ; chalcanthite t a s t e s me t a l l i c ( poi s onous , s o DO NOT TASTE) f e e l talc f e e l s s oa py or gr e a s y ma gne t i s m native iron a nd meteorites, magnetite, we a ke r i n pyrrhotite, e ve n we a ke r i n ilmenite doubl e r e f r a c t i on calcite s me l l sphalerite s t r e a k s me l l s of sulfur; he a t e d arsenic s me l l s l i k e ga r l i c , selenium l i ke hor s e r a di s h ( As a nd Se f ume s a r e poi s onous , s o t hi s t e s t s houl d not be r out i ne l y us e d) r a di oa c t i vi t y uranium and thorium minerals f l uor e s c e nc e scheelite f l uor e s c e s yellow to blue Twins symmetrical intergrowths of 2 or more crystals of the same species. ( p. 102106) Se e t he f i gur e be l ow f or e xa mpl e s of c ont a c t a nd i nt e r pe ne t r a t i on t wi ns . 7 ASSIGNMENT Known Specimens A numbe r of mi ne r a l s ha ve be e n s e t out t ha t pr ovi de e xa mpl e s of s ome of t he a bove p r ope r t i e s . Re f e r e nc e book s wi t h s ome i l l us t r a t i ons a nd phot ogr a phs a r e a l s o a va i l a b l e f or you t o c ons ul t . Your t e xt book wi l l a l s o be us e f ul . Hand in descriptions on separate sheets of paper. 1. De s c r i be t he ha bi t of e a c h mi ne r a l pr ovi de d i n t he Ha bi t s e c t i on i n t he l a b. 2. De s c r i be t he f r a c t ur e a nd/ or c l e a va ge of e a c h mi ne r a l pr ovi de d i n t he Fr a c t ur e & Cl e a va ge s e c t i on. 3. De s c r i be t he l us t e r a nd s t r e a k of e a c h mi ne r a l pr ovi de d i n t he Lus t e r & St r e a k s e c t i on. 4. De s c r i be t he t wi nni ng e xhi bi t e d by e a c h mi ne r a l pr ovi de d i n t he Twi nni ng s e c t i on. 5. Gi ve detailed de s c r i pt i ons f or 8 s pe c i me ns f r om bot h t he Known a nd Unknown s e c t i o ns ( 16 t ot a l ) . Your de s c r i pt i ons s houl d i nc l ude 3 of e a c h of t he c ha r a c t e r i s t i c s de s c r i be d a bove : ha bi t , c l e a va ge / f r a c t ur e , ha r dne s s , t e na c i t y, l us t e r a nd opa c i t y, c ol or , s t r e a k, he f t , a nd ot h e r pr ope r t i e s . 8
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