THE SEPARATION OF A MIXTURE Write on this lab exercise in pencil. Problem Statement How can we use the properties of matter to determine its identity? Purpose This activity allows you to do the following. Apply known physical properties to identify unknown substances. Note the physical nature of a heterogeneous mixture. Perform separatory techniques. Calculate percent by mass. Calculate percent error to demonstrate accuracy. Consult standard reference sources. Develop and practice laboratory techniques and skills. Gain knowledge of laboratory equipment. Background In your text, read about heterogeneous mixtures and how they to separate them. Copy each question onto notebook paper and answer in complete sentences. Staple the answers to the data table. (@ 5 pts.) 1. Examine the mixture without removing it from the vial. What makes this a heterogeneous mixture? 2. List five basic techniques used in separating mixtures. 3. Chemical change is not necessary to separate a mixture. Why is this? Materials You will receive a vial containing a mixture consisting of several parts. Only basic separatory techniques will be required to complete this assignment. Other lab equipment is available as need arises. You will need nothing outside what is available to you in this lab. Procedure You will design and conduct a series of steps to separate the mixture into its parts. Remember to record the mass of all materials or equipment used. During the activity, you must do the following. Clearly describe the parts and properties used. Determine the mass of each identified part. Determine the percent composition by mass for each part. Determine the density of the dull, silvery biscuit-shaped metal to verify its suspected identity. Consult a reference source, CRC Handbook, to determine dull silvery metal’s theoretical density. Determine your percent error in observed vs. theoretical densities of the dull silvery metal. Write a short essay answering the problem statement. Operating Procedures 1. Use no more than two weighing boats. 2. Folder seven or eight paper squares into envelopes to store the separated parts of the mixture. 3. Package each part separately. Label and secure each with tape. Do not recombine separated parts. 4. Place separated parts into a labeled beaker for storage Place this cup in the green tray on the front desk. 5. Return all equipment as instructed. Follow Up Perform the calculations and answer the question posed in the problem statement. You should include as many properties as possible in your answer. Your answer should reflect the scope of the activity. Grade The assignment’s grade counts as a lab grade with a weight of two. SC1. Students will analyze the nature of matter and its classifications. b. Identify substances based on chemical and physical properties. You exceeded the standard(s). You met the standard(s). You did not meet the standard(s). THE SEPARATION OF A MIXTURE 194 Points Group Members: ____________________________________ Date: __________ Data Table: Use Pencil Only Part Brief Description of Part (2 pts.) Suspected Identity (2 pts.) Vial & Sample plastic vial & heterogeneous mixture vial & sample Part 1 Vial plastic vial vial Mass (g) (2 pts.) Percent Mass of Whole (0.1%) (4 pts.) (Show work.) 100.0 % Part 2 Part 2 Properties Used (5 pts.) Part 3 Part 3 Properties Used (5 pts.) Part 4 Part 4 Properties Used (5 pts.) Part 5 Part 5 Properties Used (5 pts.) Part 6 Part 6 Properties Used (5 pts.) Part 7 Part 7 Properties Used (5 pts.) Part 8 Part 8 Properties Used (5 pts.) Totals g SC1. Students will analyze the nature of matter and its classifications. b. Identify substances based on chemical and physical properties. You exceeded the standard(s). You met the standard(s). You did not meet the standard(s). % THE SEPARATION OF A MIXTURE Show all work. (10 pts.) Theoretical Density of Dull Silvery Metal from CRC Handbook = _______________ g/mL Show all work. (10 pts.) Density Calculation for Dull Silvery Matter Percent Error Calculation for Dull Silvery Matter Labeled Miscellaneous Data (10 pts.) Answer to Problem Statement (30 pts.) SC1. Students will analyze the nature of matter and its classifications. b. Identify substances based on chemical and physical properties. You exceeded the standard(s). You met the standard(s). You did not meet the standard(s). THE SEPARATION OF A MIXTURE Group Members: ____________________________________ Date: __________ Grade Feedback Background ( 15 pts.) ⬚ No answered background questions are present. ⬚ ⬚ ⬚ All answers clearly show an understanding of the separation of heterogeneous mixtures. Most answers show an understanding of the separation of heterogeneous mixtures. Answers show little understanding as to how to separate a heterogeneous mixture. Data, Observations, and Calculations ( 149 pts.) ⬚ No data are present. ⬚ ⬚ ⬚ All answers clearly show an understanding of the separation of heterogeneous mixtures. Most answers show an understanding of the separation of heterogeneous mixtures. Answers show little understanding as to how to separate a heterogeneous mixture. 194 Points SC1. Students will analyze the nature of matter and its classifications. b. Identify substances based on chemical and physical properties. You exceeded the standard(s). You met the standard(s). You did not meet the standard(s).
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