Mechanical properties of oil palm trunk fibre reinforced concrete Z Ahmad*, University Technology MARA, Malaysia H M Saman, University Technology MARA, Malaysia F M Tahir, University Putra, Malaysia 26th Conference on OUR WORLD IN CONCRETE & STRUCTURES: 27 - 28 August 2001, Singapore Article Online Id: 100026013 The online version of this article can be found at: http://cipremier.com/100026013 This article is brought to you with the support of Singapore Concrete Institute www.scinst.org.sg All Rights reserved for CI‐Premier PTE LTD You are not Allowed to re‐distribute or re‐sale the article in any format without written approval of CI‐Premier PTE LTD Visit Our Website for more information www.cipremier.com 26th Conference on Our World in Concrete & Structures: 27 - 28 August 2001, Singapore Mechanical properties of oil palm trunk fibre reinforced concrete Z Ahmad*, University Technology MARA, Malaysia H M Saman, University Technology MARA, Malaysia F M Tahir, University Putra, Malaysia Abstract An experimental study was conducted to compare the effectiveness of oil palm trunk fibers used at relatively low volume fractions, in enhancing the mechanical properties of concrete material. Fiber content ranges from zero to 3 percent by volume, fiber length is 25 mm and the concrete matrix compressive strength is about 30 MPa. Flexural and compression tests were conducted according to BS 1881. The influence of fiber content on the compressive strength and modulus of rupture is presented. Keywords: compressive strength, fiber reinforced concrete, modulus of rupture 1. Introduction A variety of fibers type, including man-made fibers or synthetic fibers such as steel, glass, polypropylene and natural cellulose fibers. Investigations have been carried out in many countries on various mechanical properties, physical performance and durability of concrete materials reinforced with natural fibers from coconut husk, palm, bamboo, sugarcane, wood and other vegetable fibers. Trends in the fibrous concrete applications over the last two decades indicate that no one fiber material and fibrous composite material system has emerged to dominate the marketplace [1]. The trunk of oil palm tree can also be processed to form a good source of fiber. The process of attraction of fiber does not require a sophisticated engineering process like the synthetic fiber. With regard to the previous research on oil palm fibers, higher lignin was found in trunk fibers. The higher content of lignin in trunk fiber helps to reduce water absorption in MDF (medium density fiber) board [2]. MDF board from OPTF (oil palm trunk fiber) was stronger and had better fiber-to-fiber strength of with 24.13 MPa of MOE recorded then the frond and EFB MDF [3]. Hopefully similar advantageous will apply to concrete. Important properties of the hardened fiber reinforced concrete composite are strength deformation under load, crack arrest, durability, permeability and shrinkage. In general, the strength is considered to be the most important property and the quality of natural-fiber reinforced concrete is judged mainly by their strength. The ultimate strength depends almost entirely upon the fiber types, length and volume fraction of fibers and also on the properties and proportion of other constituent materials [4]. The critical factors affecting the modulus of rupture for composites in which the fibers pull out, rather than break, are the volume, shape and orientation of the fibers and the bond strength between fiber and matrix [5]. Among the many factors, the two most important .factors, which influence the 139 maximum loads, are the volume percentage of fibers and aspect ratio [6]. As mention by previous researchers [4,5,14,15], very small amounts of fibers have little advantageous effect although in some cases they can modify noticeably the properties of the hardened composite. Higher proportions of fibers have a tendency to prevent complete compaction of the fiber reinforced mixed. The sequence of this can be a substantial loss of compressive strength and poor durability of the hardened product. Therefore based on this report, the main objective of this study is to compare the effectiveness of OPTF in enhancing the mechanical property namely flexural strength and compressive strength of concrete material for different volume percentage of fibers. 2. Research background Economics and other related factors in many developing countries where natural fibers of various origin are abundantly available, demand the construction engineers and builders apply appropriate technology to utilize these natural fibers as effectively and economically as possible to produce goodquality fiber reinforced composite materials for housing and other need. Considerable research has already done in investigating the properties of natural-fiber reinforced cement or concrete products using fibers such as coconut coir, sisal, sugarcane bagasse, bamboo, jute, wood and vegetables in more than 40 countries [7]. Of particular interest has been the use of oil palm trunk fibers in the concrete, being waste material from the clearance of the oil palm plantation. Tremendous amount of trunks is generated during the replanting and not being effectively used. 3. Objective This study is a part of a broad research program on the compatibility study of oil palm trunk fiber as concrete reinforcement. The main objective of this study was to investigate the mechanical properties of OPTF reinforced concrete namely compressive strength and flexural strength. In addition to that is to obtain preliminary information on the relative difference in compressive strength and flexural strength amongst the different percentage of fibers used in the matrix. 4.0 Experimental program 4.1 Materials The oil palm trunk fibers were taken directly from the plantation when the trees newly fell using special excavator machine. After that the fibers were undergone cleaning process to remove the parenchyma. This parenchyma needs to be removed since it contains sugar, which can retard the concrete hardening process. Then the fibers were cut according to specified length (25 mm). According to ACI 544.1 R-60 [6], the length of fibers may vary from 25 to 500mm. For this study the fiber length is fixed at 25mm. OPT fiber is light yellowish when in fresh state as shown in Fig. 1.0. However, the color changes as the fiber tend to become dry, from light yellowish to dark brown. Even though the color changes but the fiber still carries strength. The basic requirements of natural fibers when used as reinforcement in concrete matrices are high tensile strength and elastic modulus. The tensile strength of the fiber was found to be 300 - 600 N/mm 2 . Bulk density of fibers is 1200 kg/m 3 • The diameter of clean fiber is between 0.3 - 0.6 mm. When compared with other natural fibers that have been used, OPTF tensile strength is comparable and in certain fiber types, OPTF is better as shown in Table 1.0. Fig. 1.0 Oil palm trunk fiber 140 Table 1.0 Properties of natural fibers Bulk Density (kglm 3) 1200 145-280 700-800 NA NA NA NA Fiber types Oil palm trunk Coconut Sisal Sugarcane Bamboo Jute Flax (Source: Aziz M.A .et al) [8] Tensile Strength (N/mm2) 300-600 120-200 280-568 170-290 442 250-350 1000 NA- Not available 4.2 Mixes The concrete constituents used were ordinary Portland cement, fine aggregate, coarse aggregate and OPTF. Ordinary Portland cement confirmed the requirements of BS 12:1958. Fine and coarse aggregate confirmed the grading BS 882:1992. Coarse aggregate has maximum size of 20 mm. To compare the properties of fibrous concrete with plain concrete, water-cement ratio was kept constant at 0.5. The proportions of aggregates were kept unchanged for the same reason. Table 1.0 shows the details of concrete mix proportions in kg/m 3 used for this investigation. Table 2.0 : Mix Design [ in kglm1 Mix Fiber By Volume Cement Water 1 0% 360 180 Coarse Aggregate 1075 2 1% 358 179 1061 522 3 2% 355 176 1046 515 4 3% 350 175 1037 511 Fine Aggregate 530 NOTE: Batch quantities: kg/m 3 Assume R.D(relative density) for aggregate =2650 kg/m 3 Cement: Sand: Coarse aggregate (1 :1.5:3) Maximum size: 20mm Water cement ratio: 0.5 (constant) 4.3 Test specimen and test method The test specimen used for flexural strength was 150 x 150 x 750 mm rectangular beam. In total 72 such beams have been cast. The mixing of fiber in concrete was performed according to the ACI 544-1 R57 recommendations. The plain and fiber reinforced concrete mixtures were manufactures in a rotary drum mixer. The mixing procedure is described in the following: 1. Charge the mixer with all the sand and gravel. 2. Start the mixer and add one-third of the water. 3. Add all the cementitious materials together with another one-third of the water over a 4 min. period. 4. Add the fibers to the mix in a gradual manner such that bunching up of fibers on the mix is prevented; the addition of fibers usually takes about 3 mins. 5 Add remaining cementitious materials followed by the remainder water to the mixture over a 3-min period. Fresh plain and fibrous mixes were tested for workability by slump (BS 1881: Part 102: 1983) and VeBe (British Standard 1881: Part 104: 1983) test methods. Specimens for hardened material tests were then manufactured by casting fresh concrete inside molds with compaction achieved through external 141 vibration. All the hardened specimens were cured according to BS 1881: Part 111: 1983 by water immersion. The following tests were performed on hardened concrete specimens; 1. Flexural strength tests were performed for each mix composition on 150 x 150 x 750 mm prismatic specimens in accordance to BS 1881: Part 118: 1983 using third point bending. The tests were carried out for three different days of curing; 3,7 and 28 days. 2. Compressive strength tests were performed for each mix composition according to BS 1881: part 119: 1983 (Method for Determination of compressive strength using portions of beams broken in flexure) also for different curing days; 3,7 and 28 days. 5.0 Experimental result All test results are summarized in Table 3.0, while graphical presentations of the results are displayed in Fig. 2.0, Fig. 3.0 and Fig. 4.0. Each strength value presented in Table 3.0 is the average of 6 specimens. A total of 72 beams for flexural and 72 broken beams for compressions were tested in this investigation. The results of this investigation are applicable to the material and type of fiber used. Table 3.0 Summary statistics for the volume study 0 133 106 2 3 98 65 mean mean 3 11.99 16.2 7 16.43 20.70 28 27.24 31.00 3 19.33 22.7 7 28.1 29.8 28 32.24 35.1 3 14.2 14.9 7 15.63 18.1 28 22.26 25.1 3 11.13 11.2 7 14.38 17.4 28 23.83 20.1 An analysis of variance was performed to determine if there were differences in mean flexural strength (modulus of rupture), and compression strength, among the difference volume of fiber tested. As indicated through ANOVA, there is convincing evidence that fiber volume affects or influence the flexural strength [p-value=0.02] and also affects the compressive strength [p-value = 0.01] at 5% significance level. The result presented in Fig.4.0 indicate that the flexural strength obtained with 1.0 percent volume fraction of OPTF can be reached at 18.35 percent greater or 2.2 times the corresponding properties of plain concrete. Presence of 1.0 percent fiber also increases the compressive strength by 13.22 percent or 1.1 times than the plain concrete as shown in Fig. 4.0. Compressive strength is more dominants compared to flexural strength with the inclusion of OPTF. To determine how the volume of fibers affects the compressive strength, a linear regression was performed. The regression analysis yielded strong evidence that volume percentage affects the compressive strength [p-value =0.005]. However, the relationship between compressive strength and volume of fiber was not very strong [R2 = 0.562] at 28 days. The variation in the compressive strength is 142 explained by 56.2 percent variation in the volume of fiber used. The other 43.8 percent variation can be explained by other factor such as length of fibers, moisture content, absorption capacity of the fiber, mixing method and etc. Previous researches [1] indicate that volume of fiber affect or increase the compressive strength at the 1.0% volume fraction. The addition of 1.0% (volume) of jute fiber gives 13.49% increases in the compressive strength [6]. The same analysis was performed to determine how fiber volume affected the flexural strength. Test results and regression lines (with 95% confidence intervals) representing the effects of OPTF reinforcement on flexural strength and compressive strength of concrete are presented in Fig. 5.0(a), and (b). The flexural and compression strengths are observed to increase with OPTF reinforcement at the lower dosage and tend to decrease as the amount of fiber increases. Fig. 6.0 (a), shows the diameter size of the fiber and the bonding between fiber and the matrix. The loose interface in the bonding may contribute to the strength reduction when further increase in fiber volume. At 1.0 percent, the effect of fiber in transferring (distributing) the stress is dominant. However for more than 1.0 percent, the second effect (loose interface) is dominant. The reduction in strength as the volume of fiber increases may also due to the increase in void content, since the water/cement is maintained. This can reduce the workability as the amount of fiber increases that can be seen from the value of slump as shown in Table.3.0. The use of fibers as reinforcement of concrete and cement therefore requires frequent adjustment of the mix proportions in the process of maximizing the positive contributions of the fibers to chosen properties of hardened concrete [13]. Therefore in this study, the addition of 1.0 percent fiber volume cannot be concluded as the optimum contribution. In this investigation, the mix proportions is fixed, therefore it can only conclude that the addition of OPTF does improve the compressive and flexural strength of the concrete. Further investigation need to be done in order to conclude the optimum amount of OPTF in maximizing the properties of concrete. 6.0 Conclusion The effectiveness of OPTF in enhancing the mechanical properties of concrete materials was compared with plain concrete. All the plain and fibrous concrete mixtures were designed with a fixed proportion. The only variable parameter is the percentage of volume fiber; 0,1,2, and 3. The hardened material mechanical properties were assessed through flexural and compression tests. The following conclusions were derived. 1. Oil palm trunk fibers increased the flexural strengths of concrete material with 1.0 percent volume fraction of OPTF. The average flexural strengths were 18.35 percent higher or 2.2 times the corresponding properties of plain concrete. 2. Oil palm trunk fibers increased the compression strengths of concrete material with 1.0 percent volume fraction of OPTF. The average compression strengths were 13.22 percent higher or 1.1 times, the corresponding properties of plain concrete. 3. OPTF fibers, when used at 1.0 percent volume fraction, produced compressive strength and flexural strength comparable to those obtained with other fibers such as jute. 4. 1.0 percent volume fraction is not the optimum amount of fiber needed to increase the strength. There are other factors need to be studied. 143 Fig.6.0(a): The diameter size of the fiber Fig.6.0(b): The bonding between fiber and matrix ~r------------------------, ~ / \ \ I I J I I I I f / \ '- \ \ '- \ \ a DAYS28 \ VOL a OAY28 ' VOlUME 1I:~'~-'~' __ '_""i:l VOl. ~ DAY7 .. DAVS3 VOLUME VOL a OAY3 VOlUME Percentage 01 Fibers Volume Percentage of Fibers Fig.2.0: Flexural strength (Nlmm2) vs Percentage of fibre (volume) for variation days of curing 3,7 and 28. Strength (Nlmm2) versus Volume Percentage of Fiber J.!. COMF VOL A R.EXI VOL Volume percentage of fiber Fig. 4.0 : Flexural Strength and compression strength (Nlmm 2) vs Percentage of fiber (Volume) for 28 davs 144 Fig.3.0: Compressive strength (N/mm2) vs Percentage of fibre (volume) for variation days of curing 3,7 and 28. 50 ~-------------------------------------------------------, ~ ~ 40 .<:: 'g> ~ ., 30 .~ (J) [l! ~ o 20 U 10 +------,------~------r_----_r----~r-----_r----~,_----~ -.5 0.0 .5 1.0 1.5 2.0 2.5 3.0 3.5 Percentage of Fibers Fig.5.0 (a); Relationship between Compressive Strength and Volume of Fibers at 28 days. 32 30 @' E E % -='"c: ~ e ::> x u.. 28 26 24 .9! 22 20 -.5 0.0 .5 1.0 1.5 2.5 Volume percentage of fiber (%) Fig.5.0 (a): Relationship between Flexural Strength and Volume of Fibers at 28 days 145 3.0 3.5 8.0 Acknowledgments The authors are thankful to the University Technology Mara, Malaysia (Biro Research Center) for providing this project with financial support. Bio-Alam Sdn. Bhd provided the materials used in this investigation. These contributions are gratefully acknowledged. The authors would also like to thank Mr. Saiful and Mr. Mohd Nazir for providing this project with their help in the experimental work. References: [1] Sorovshian, P., and Khan, Hsu, J.w., " Mechanical Properties of Concrete Materials Reinforced with Polypropylene or Polythylene Fibers," ACI Material Journal, V.89, No.6, Nov - dec 1992, pp 535 - 540. [2] Myers, G., and J.D. McNatt (1993) "Selected Properties of Commercial High-Density Hardboards." Forest Products Journal Vol. 43(4) : 59-63 [3] Liew, Lionel (1996) " Properties of Medium Density Fiberboard Made from Oil Palm (Elaeis guineensis) Fibers." Master Forestry (Wood Industry) Project Report. Faculty of Forestry, University Putra Malaysia, Serdang [4] Aziz M.a, Paramasivam P., Lee S.l., " Concrete Reinforced with natural fibers", Proceeding Concrete Technology & Design, Vol. 2, 1984, pp. 106-115 [5] Keer, J.G., "Natural Fiber Reinforced Concrete and Cemenf', Proceedings Concrete Technology & Design, Vol. 1, 1984, pp.65 - 67 [6] ACI Committee 544-1 R " Natural Fiber Reinforced Concrete," ACI Journal Proceedings, V.79, SeptOct 1982, pp.57 - 64 [7] Fordos, Z., " Fiber Reinforced Concrete" ,Proceedings Concrete Technology & Design, Vol. 5, 1984, pp.32- 41 [8] Aziz M.a, Paramasivam P., Lee S.l., " Concrete Reinforced with natural fibers", Proceeding Concrete Technology & Design, Vol. 2,1984, pp.119-120 [9] BS 1881: Part 102 : 1983: Slump Test [10] BS 1881: Part 104: 1983: VeBe Test [11] BS 1881: Part 111 : 1983: Curing Method By Water Immersion [12] BS 1881: Part 118 : 1983: Method for Determination of Flexural Strength [13] BS 1881: Part 119 : 1983: Method for Determination of Compression Strength using Portion of Broken Beams in Flexure (equivalent cube method) [14] P. Bortos, Fresh Concere: Properties and Test, Elsevier Science Publishers B.V., 1992 , pp. 235 236 [15] Faisal F.w., and seminar A.A., "Mechanical properties of High Strength Fiber Reinforced Concrete." ACI Materials Journal, V.89, No.5, Sept-OCT.1992,pp.449-452 146
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