Misc
Inorganics
Organics
Minimum Sample Volumes - Soil/Solid
Analyte
Sample Volume-Minimum*
Sample Volume- Desired
Volatiles (5035), Gasoline Range Organics- MI
Volatiles (5030), Gasoline Range Organics- OH
Semi Volatiles
PCBs
Organochlorine Pesticides
Organochlorine Pesticides/ PCBs
2,4-D, 2,4,5-TP
Organochlorine Herbicides
Diesel Range Organics
Ethylene Glycol
Glycols (ethylene, propylene, triethylene)
Alcohols (n-butanol, ethanol, isobutanol, isopropanol, methanol)
10
10
30
15
15
15
30
30
15
10
10
10
10g
4 oz
4 oz
4 oz
4 oz
4 oz
4 oz
4 oz
4 oz
4 oz
4 oz
4 oz
Analyte
Sample Volume-Minimum*
Sample Volume- Desired
Metals
Mercury
Bromide
Chromium, Hexavalent
Chloride
Corrosivity
Cyanide, Total
Fluoride
Ignitability
Nitrogen, Ammonia
Nitrogen, Total Kjeldahl
Nitrogen, Nitrate
Nitrogen, Nitrite
Nitrate Plus Nitrite
pH
Phosphorus (water soluble)
Sulfate
Sulfide, Total
50 g
50 g
5g
15 g
5g
5g
5g
5g
10 g
5g
10 g
5g
5g
5g
5g
5g
5g
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
Analyte
Sample Volume- Minimum
Sample Volume- Desired
% Moisture
30 g
4 oz
g
g
g
g
g
g
g
g
g
g
g
g
* Bare Minimum sample volumes do not account for the percent moisture sample volume
DCSID: G-526.3 (02/10/16)
oz
oz
oz
oz
oz
oz
oz
oz
oz
oz
oz
oz
oz
oz
oz
oz
oz
oz
Inorganics
Organics
Minimum Sample Volumes - Water
Analyte
Sample Volume- Minimum
Sample Volume- Desired
Volatiles, Gasoline Range Organics
Semi Volatiles
PCBs
Organochlorine Pesticides
Organochlorine Pesticides/ PCBs
2,4-D, 2,4,5-TP
Organochlorine Herbicides
Diesel Range Organics
Ethylene Glycol
Glycols (ethylene, propylene, triethylene)
Alcohols (n-butanol, ethanol, isobutanol, isopropanol, methanol)
40 mL
650 mL
650 mL
650 mL
650 mL
650 mL
650 mL
650 mL
2 mL
2 mL
2 mL
120 mL
1 Liter
1 Liter
1 Liter
1 Liter
1 Liter
1 Liter
1 Liter
40 mL
40 mL
40 mL
Analyte
Sample Volume- Minimum
Sample Volume- Desired
Mercury
Metals Filtering (dissolved metals)
Total Metals
Alkalinity
Biochemical Oxygen Demand
Bromide
Carbon, Total Organic
Chemical Oxygen Demand
Chromium, Hexavalent
Chloride
Chlorine Demand
Chlorine, Total Residual
Cyanide, Amenable
Cyanide, Available
Cyanide, Total
Dissolved Oxygen
Fats, Oils, & Grease
Fluoride
Hardness
Ignitability
Low Level Mercury
Nitrogen, Ammonia
Nitrogen, Total Kjeldahl
Nitrogen, Nitrate
Nitrogen, Nitrite
Nitrate Plus Nitrite
pH
Phenolics, Total
Phosphorus, Ortho (dissolved)*
Phosphorus, Total
Reactivity
Solids, Total
Solids, Total Dissolved
Solids, Total Suspended
Solids, Total Volatile
Specific Conductance
Sulfate
Sulfide, Total
Turbidity
100 mL
100 mL
100 mL
50 mL
300 mL
10 mL
10 mL
5 mL
50 mL
10 mL
2 Liters
25 mL
50 mL
20 mL
50 mL
50 mL
100 mL
10 mL
100 mL
50 mL
40 mL
100 mL
50 mL
10 mL
10 mL
10 mL
10 mL
100 mL
100 mL
100 mL
25 mL
50 mL
50 mL
50 mL
50 mL
25 mL
10 mL
50 mL
100 mL
250 mL
250 mL
250 mL
250 mL
500 mL
50 mL
40 mL VOA
10 mL
125 mL
50 mL
2 Liters
50 mL
250 mL
40 mL
250 mL
125 mL
500 mL
50 mL
250 mL
125 mL
120 mL
250 mL
250 mL
50 mL
50 mL
50 mL
25 mL
250 mL
250 mL
250 mL
125 mL
250 mL
250 mL
250 mL
250 mL
50 mL
50 mL
250 mL
250 mL
DCSID: G-526.3 (02/10/16)