Creating a balanced mix design for highstrength concrete By Bryce Simons igh-strength concrete is used more widely with each passing year. But what is highstrength concrete? According to ACI 363 “High Strength Concrete,” any concrete with a specified compressive strength of 6000 psi or greater is highstrength concrete. When this definition was written, it was highly appropriate. However, in the years since, a significant amount of experience has been gained for concrete mixes with compressive strengths far exceeding 6000 psi. I have personally designed many mixes with compressive strengths exceeding 15,000 psi and several exceeding 20,000 psi. So much experience has been gained, in fact, that the Canadian code currently defines highstrength concrete as any concrete with a compressive strength exceeding 10,000 psi. It is important to remember several things about high-strength concrete. Initially, it is just one of many types of concrete mixes that have been adjusted to deliver a specific property or properties. In this case, it is compressive strength. The same understanding which made it possible to develop high-strength concrete is also applied when developing concrete mixes with high flexural strengths, high durability benefits, high skid resistance, high abrasion resistance, and super-flat characteristics. In other words, high-strength concrete is just one type of high-performance concrete. Secondarily, high-strength concrete is not a large part of the production output of any ready mix plant. However, the ability to produce this type of concrete without difficulty requires a higher level of sophistication and skill than is considered necessary for more conventional 3000-psi and 4000-psi concrete mixes. Having access to this level of sophistication automatically precludes many of the problems that plague other facilities where these skills are missing. H Defining high-strength concrete My personal definition of high-strength concrete is somewhat different than the formal definitions described earlier. For the purposes of my clients, I normally define high-strength concrete as any mix with a compressive strength requirement at least 2000 psi higher than what they are accustomed to dealing with. Based on this definition, there are many parts of the country where 6000 psi is highstrength concrete. However, in those markets where 8000-psi to 10,000-psi concrete has been available for many years, it takes compressive strength requirements of 10,000 psi to 12,000 psi to be classified as high-strength concrete. It is also possible for two producers in the same geographic region to have different definitions of high-strength concrete. A well-established central mix plant may have been producing 10,000 psi concrete for years. However, a few miles away, another well-established truck mix plant may have experience with concrete to only 5000 psi. For them, 7000 psi becomes high-strength concrete. Why does a minor difference of only 2000 psi shift a concrete mix into the highstrength category? Keep in mind that to comply with ACI 318 Chapter 5, a new mix (one without any historical backup information) needs to have an average compressive strength 1200 psi greater than specified for strengths between 3000 psi and 5000 psi, and 1400 psi greater than specified for strengths greater than 5000 psi. These overdesign factors are normally used for high-strength concrete because it is not often that a ready mix plant can show historical data. This means that the specified strength is not just 2000 psi greater than what the supplier is accustomed to, but that the supplier must deliver a mix that is 3400 psi (2000 psi plus 1400 psi) greater than what the supplier is accustomed to. Making the necessary revisions to the mix proportions will significantly affect the fresh and hardened properties of the concrete. Knowing what to expect when these changes are made and how to react to unforeseen circumstances can make the difference between a successful program and an unsuccessful program. The sledgehammer method I have had many people tell me that they produced 8000-psi concrete simply by adding two or three bags of cement to an already existing mix, cutting back some of the sand (or cutting back on the sand and gravel) and adding superplasticizer (sometimes adding a lot of superplasticizer) to create the mix. Unfortunately, there are a lot of problems with this method. This is typically what I refer to as the sledgehammer approach. This approach ignores the individual characteristics of the mix constituents and forces the mix to achieve a certain fluidity without regard to the other properties which are also being affected. Of course, this approach works. There have been far too many examples of this type of high-strength concrete to ignore reality. However, these mixes tend to have difficult handling characteristics, or they may be harder to batch, or they may be harder to place or pump, or they may be more difficult to finish. Shrinkage and retardation also may be issues. A reduction in the amount of bleedwater may make it much more difficult to finish. In short, there are a number of inherent difficulties with this approach. Water-cement ratios The key to properly designing highstrength concrete mixes is successfully lowering the water-cement ratio while still maintaining workable, placeable concrete. Most high-strength concrete mixes have water-cement ratios substantially below 0.40, while many that I have worked on have gone as low as 0.20. Clearly, there are only two ways to lower the water-cement ratio: 1) reduce the amount of water or 2) increase the amount of cementitious material. Depending on the magnitude of strength being called for, it is often necessary to do both. Lowering the water content can be ac- complished by two primary techniques: 1) reducing the inherent water demand of the mix and 2) replacing some of the water with water reducers and superplasticizer. Water demand The water demand of the mix is a natural property of any concrete mix. Essentially, it is the amount of water required for the individual mix constituents to achieve the desired degree of workability. The total surface area of the constituents and particle shape have a profound effect on the water demand. The sand has the greatest impact on the water demand of a concrete mix. This is because the total surface area of the sand particles is substantially greater than the T he use of highstrength concrete allows for the construction of modern-day, high-rise buildings such as 311 South Wacker Drive in Chicago. This 70-story building completed in 1991 used concrete with compressive strengths to 12,000 psi. other mix constituents (except for the cementitious products which go into solution). Additionally, a sand with more fine particles will have substantially more total surface area than will a coarser sand. A sand with a fineness modulus of 2.6 will have a significantly greater water demand than a similar sand with a fineness modulus of 3.2 Particle shape also plays a significant role in water demand. A crushed material has much sharper edges than a rounded material. Consequently, the crushed aggregate particles will require more water to float them past adjacent particles than will the rounded aggregate. Crushed aggregates are also normally covered with residue from the crushing process (crusher dust). This dust has a tendency to increase water demand and impairs the ultimate bonding between the cement paste and the aggregate particle. Gravel size and type The type of gravel available must be assessed. My experience has shown that for high-strength concretes, well-washed, rounded gravels tend to work better than crushed coarse aggregates. I believe this is due to the fact that most crushed aggregates are stockpiled without being thoroughly washed. As discussed earlier, the crusher dust that coats each rock particle provides a bond breaker between the resultant cement paste and the rock itself. The proper sized gravel needs to be adjusted to the application. It is a published fact that in order to reduce shrinkage and increase the modulus of elasticity of a mix, a larger sized gravel should be used. However, much of the work which was done in Seattle in the mid1980s showed that the workability and the resulting strength of the mixes actually increased when 3⁄8inch minus gravel was used instead of a 7⁄8-inch minus. Although the total surface area of the gravel will increase as the maximum sized particle is reduced from 3⁄4 inch to 3⁄8 inch, the magnitude of the change is relatively small and, therefore, is typically not a major concern. The cleanliness of the gravel is probably the single most important factor in a successful high-strength concrete program. It has been proclaimed repeatedly throughout the country that the reason the Seattle area could produce such highstrength concrete was because the aggregate was so hard. In reality, the aggregates used for the mixes in Seattle were almost identical in hardness and strength to many of the aggregates in other parts of the country where the perception is that the gravel is not so good. The primary reason the Seattle aggregates worked so well is because they came from a glacial outwash source that naturally washed the aggregates so thoroughly that there was virtually no minus 200 material in the pits. There was no need to wash the aggregates because they were already clean. It is typically necessary to adjust the sand-gravel content to accommodate the higher cementitious contents of a high-strength concrete mix. Obviously, there are going to be more fines in the mix from the cementitious materials than is ordinary. It is not uncommon to have mixes with seven to 10 bags of cement, 15% fly ash, and 5% to 10% silica fume. The total cementitious content of these mixes is unusually high. Consequently, the need for the fines from the sand contribution is not as significant. By using a coarser sand and allowing the fines to come from the cementitious materials, high-strength mixes can be very effectively balanced. In addition to using a coarser sand, it is important to use as little sand as possible. Often, the sand portion of the total aggregate fraction is several percentage points lower than is typically used. In many areas, it is not uncommon to find balanced highstrength concrete mix designs with sand comprising only 39% of the total aggregate volume. In some paving mixes, it has been as low as 34%. However, in other locations, where the coarser aggregate is the only kind available, or for several other reasons, the balanced sand content may be as high as 48%. Cement type and source Cement type and source is a concern. As the strength of the concrete mix increases, the number of factors which influence the ultimate strength begin to have more impact. Cements from the same source have a certain amount of day-to-day variation. However, using cements from different sources will provide a level of variation far in excess of that which would come from a single source. That variation can create major difficulties during the course of a project. The chemistry of the cement is important. The heat of hydration in high-strength concrete mixes can be quite high. Therefore, a consistent Type II cement with a lower C3A content is a good cement for most high-strength concrete applications. On some projects where variation was a concern and storage space was not a problem, the total amount of cement required for the entire project was stored from a single day’s run from the cement plant. The same cement was then used to develop the mix designs and for all of the field testing. Fly ash Fly ash is a major component of any high-strength concrete mix. Fly ash works as a water reducer. It also works to keep the ultimate heat of hydration down. Finally, fly ash works to make the overall mix easier to batch, discharge, pump, and place. Normally, fly ash which is not interground with the cement works better than that which is. It is important to use a good quality fly ash. This is important to reduce mix variability and to ensure that the fresh properties of the concrete remain constant. One index of fly ash is loss on ignition, or LOI. This is a measure of the carbon content in the ash. This value should be quite low. If the carbon content gets too high, then water demand of the mix can get large, superplasticizer dosages will vary significantly, and problems with false setting and air entrainments can become an issue. Silica fume In many instances, silica fume may also be used in the mix. Typically, mixes that have strengths in excess of 15,000 psi will have silica fume. The type of silica fume used will make a difference. I have had direct experience which indicates that the silica fume which comes in the form of a slurry works more efficiently than does that which comes in a dry, densified form. Typically, this does not become a major concern until the water-cement ratio drops below 0.30. For high-strength concrete, typical dosage rates for the slurry-type silica fume range between 7% and 10%, by weight of cement. Typical dosage rates for the densified silica fume range between 10% and 14%, by weight of cement. However, if the slurry form is used, the water contained in that slurry should be included when calculating the water-cement ratio of the mix. Chemical admixtures Finally, the chemical admixtures need to be considered. It is typically customary for a given operation to use admixtures from a single supplier. Most often, as the admixtures come from the same supplier, there will not be significant compatibility problems. However, the compatibility of the chemical admixtures used should be checked regardless of where they come from. Occasionally, setting or shrinkage problems, or other problems, may be encountered due to the larger quantities of admixtures being used, even when using products from the same supplier. Mixing can be a problem as the water-cement ratio drops. Although many literature sources prescribe designing the mix to a 1-inch slump before adding superplasticizer, this simply is not possible with some of the higher-strength mixes. It is not uncommon to run a laboratory program in which there is so little water that the mix looks like so many marbles, then baseballs, and finally concrete. By changing the order of addition of the ingredients, so the sand is held out until all else has been added, and then added last, this problem can be reduced. In the larger commercial size mixers, this tends to be less of a problem than in smaller laboratory mixers. To create the properly balanced high-strength concrete mix design, it will be necessary to work with the changing parameters listed previously. Don’t be afraid to experiment. The higher the strength, the more this mix is not going to look, act, or feel like ordinary concrete. Instead, as the water-cement ratio goes down, it will begin to look more like peanut butter than concrete. Don’t be afraid to exceed the maximum allowable mixing times prescribed in ASTM. Finally, don’t be in a rush to add more water just because it looks like there is a chance the mix will not come out. Give it time. Don’t be afraid of slumps in excess of 4 inches. High-strength concrete typically has slumps as high as 91⁄2 or 10 inches. This is allowable because the slump is created with the admixtures—not water. When the mix is finally balanced, there will be no doubt about it. A vibrator will be able to immediately effect a very large radius, the mix will batch with relative ease, and the fresh and hardened properties will meet or exceed all expectations. ✥ Bryce Simons P.E. is manager of special materials testing, AGRA Earth & Environmental, Albuquerque, N.M. PUBLICATION # J950788 Copyright © 1995, The Aberdeen Group All rights reserved
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