Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 Performance of ACCOS, an Automatic Crystal quality Control System for the PWO crystals of the CMS calorimeter E. Au!ray *, G. Chevenier , M. Freire , P. Lecoq , J.M. Le Go! , R. Marcos , G. Drobychev, O. MisseH vitch, A. Oskine, R. Zouevsky, J.P. Peigneux, M. Schneegans CERN, DIV.PPE/130, Bat. 27, CH-1211 Geneva 23, Switzerland INP, Minsk, Belarus LAPP, Annecy, France Received 15 December 1999; accepted 11 March 2000 Abstract Nearly 80 000 PWO crystals for the CMS electromagnetic calorimeter will arrive at CERN/Geneva and INFNENEA/Rome between now and year 2004. The stringent speci"cations on their dimensions and optical quality have to be veri"ed prior to their formal acceptation. Automatic systems for measuring the critical parameters of each crystal and recording them in a database have been designed and constructed. The "rst machine is now in stable operation at CERN. In this note, the performance of each instrument, based on the measurements on &1000 pre-production crystals, is analysed in terms of stability and compared to the results of conventional benches. 2001 Elsevier Science B.V. All rights reserved. 1. Introduction The CMS collaboration [1] plans to use 76 200 tapered lead tungstate crystals (PWO) for its highresolution electromagnetic calorimeter [2]. These crystals, produced in Russia (Bogoroditsk) and in China (BGRI and SIC) will be delivered to two CMS Regional Centres: CERN/Geneva and INFN-ENEA/Rome, where the calorimeter will be assembled. In order to guarantee that all the delivered crystals meet the speci"cations [3] on the * Corresponding author. Tel.: #41-22-767-58-44; fax: #4122-7678930. E-mail address: [email protected] (E. Au!ray). parameters considered as crucial for the calorimeter performance, several measurements must be performed. First, the dimensions of each crystal must be measured to a precision of &10 lm, in order to guarantee that the crystal can be mounted in its individual glass "ber alveolus with the necessary clearance. Then, the optical quality of the crystals must be checked, namely its optical transmission. The transversal transmission allows to check the homogeneity of the transmission along the crystal, whereas the longitudinal transmission guarantees a long absorption length and reveals possible absorption bands or poor radiation resistance [3]. The light yield of the crystals, in fact the light collected on a photodetector seeing their largest 0168-9002/01/$ - see front matter 2001 Elsevier Science B.V. All rights reserved. PII: S 0 1 6 8 - 9 0 0 2 ( 0 0 ) 0 0 6 6 5 - 3 326 E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 section, is an essential parameter for the energy resolution (stochastic term) of the future calorimeter, as well as the uniformity of the light collection along the crystal (constant term of the resolution). Moreover, this light must be collected in a short time (in 4100 ns), with absence of slow components (in the range of a few 100 ns) which can a!ect the pulse shape, and as little as possible contribution of longer components (afterglow) to avoid pile-up e!ects. All these parameters are measured currently on classical benches (Light Yield benches, spectrometers), but the duration of the measurements and of their analysis, as well as all the crystal manipulations needed, would make the control of several ten-thousands of crystals fastidious, costly in manpower and risky for the crystals. This is why systems of benches (named ACCoS, Automatic Crystal Control System) were designed [4}6] allowing measurement of these parameters by appropriate methods in a fully automatic mode, including transfer of all the data to a database. The "rst machine was built in LAPP/Annecy in collaboration with INP/ Minsk, and installed at CERN (ACCoCE1, Fig. 1) in summer 1998 and extensively tested since. It is now in steady production mode: in fact, more than 1000 pre-production PWO crystals from Bogoroditsk Technical Chemical Plant in Russia were recently measured. In this note, based on these measurements, the level of stability reached by each instrument and its performance compared to classical benches are shown and discussed after a brief description of the system and its operation. Fig. 1. Photograph of ACCoCE 1. Fig. 2. ACCoCE 1 design. E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 327 Fig. 3. View of the 3D machine (Johansson Topaz 7). 2. Main features of ACCoCE1 The machine is composed of a circular server presenting the crystals in turn to a dimension measuring machine and to optical benches, either "xed or mounted on a linear movement bolted to a rectangular table (see Fig. 2). The 110 cm diameter server for 20 crystals arranged radially is bolted on a turntable driven by a step by step motor yielding a crystal positioning precision of a few tenths of mm. The crystals have their section tilted by 60 and are supported horizontally by two thin vertical pillars allowing all measurements with minimum limitations. The small section is always placed facing the centre of the circle and carries a label with barcode. A "xed barcode reader identi"es each crystal as it stops facing it during an initial turn of the server. Each crystal number is then associated to a position on the server in a look-up table. Hanni"n, Motion & Control, Digiplan, Poole, Dorset, UK; or Groupe Jeambrun, Lyon, France. Barcode reader Symbol LS 1220. To measure the dimensions of the crystals, a classical three-dimensional (3D) machine, capable of a precision of &5 lm per point and with an open geometry (Fig. 3) for easy crystal presentation by a circular server, was chosen. Each crystal in turn is presented to the dimension measurement with end-faces vertical or nearly and side faces at 30 or 603 from vertical. Fifteen points are measured on each lateral face of the crystals and nine points on the two end faces, allowing precise reconstruction of the six planes. In order not to lose precision by probing slanting faces, the 2 mm diameter balls, ending the "ve stylets of the star-shaped probe, approach the crystal surface slowly and perpendicularly on the last millimetres. A calibration on a reference ball (&30 mm diameter) allows to rede"ne the origin of the coordinate system and to recalibrate the diameter of the probe balls for corrections. The geometry of the crystals for each of the di!erent types is determined by a set of seven variables (Fig. 4) for left and right parity (mirror symmetry). Side P is always placed on the support Johansson Topaz 7, Eskilstuna, Sweden; or Marne-laValleH e, France. 328 E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 pillars with the same orientation (at 60 from vertical, whether left or right). Side D is depolished by the producer to a speci"ed [3] degree of roughness, in order to obtain light collection uniformity. Two compact (7;8;22 cm) spectrometers measure the optical transmission through the crystal length or width of a light beam produced by a 20 W halogen lamp. The eleven discrete wavelength values are de"ned by interference "lters chosen for best determination of the band edge slope and of possible absorption bands. A large area UV-extended pin photodiode (PD) [4] detects the transmitted light. For Transversal Transmission Optics (TTO), the light beam always passes through the optically polished sides N and W and the PD is located at &5 cm from the light emitting optics. The spectrometer, "xed on a chariot mounted on a linear motorised movement , (see foot note 1) moves along the crystal and stops every 2 cm in 11 points start- ing at 1.5 cm from the small end. The diameter of the light beam is adjusted to &10 mm. A calibration measurement in air is taken at a position outside of the crystal. For Longitudinal Transmission Optics (LTO), the PD is located at &27 cm from the light emitting optics which was optimised for such a distance: quasi-parallel beam of &7 mm diameter entering the crystal and &9 mm exiting. This diameter provides adequate sensitivity to clouds of scatter points sometimes present near the central axis of the crystal. The Longitudinal Transmission (LT) optics and its PD are in a "xed position and the light beam is centred on the crystal when it stops in its measuring place. A calibration measurement is performed in air between each crystal. To measure kinetic parameters, Light Yield (LY) and LY Non-Uniformity (NU), a method allowing to derive the three parameters from a single time spectrum was chosen. One reason for preferring a time measurement is the relatively low light yield of PWO crystals, which makes direct light yield measurement with a source and PM di$cult unless good optical contact is performed, which is rather unpractical for a fully automatic measuring device. The decay time of the PWO crystal's scintillation light is measured using the detection by photomultipliers (PMT) of the two collinear 511 keV gamma-rays from a Na source. In fact, c detec ted in a small BaF crystal produces the Start signal and the detection of c in the PWO yields the Stop signal. The time di!erences are analysed in a TDC, capable of multi-hit event rejection [7]. For the time spectrum shape and the LY measurement to be correct, the detected light of PWO must not be larger than a few tenths of photoelectrons per Na event, which is readily obtained with a PM (square 3;3 cm) seeing the crystal through its largest section at a distance of 1}2 cm. The BaF /Na/PWO geometry is very compact in or der to maximise the c solid angles and thus the rates. The Start telescope, comprising PM with divider, small crystal and source, is moved along the PWO crystal on the same chariot as the TTO Radiation Instruments & New Components Ltd., (RI&NC), Minsk, Belarus. PMTs for Kinetics 5900U, Hamatmatsu UV-extended photomultipliers (28;28;20 mm). Fig. 4. Crystal geometry. E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 spectrometer, with 21 positions of measurement, each cm, starting at 1.5 cm from small end. Normally, the crystals are "rst measured in dimensions, then LT followed by decay time and "nally TT is measured on each crystal. The sequence is fully automatic with always indication of what is being measured and online presentation of the measured spectra. For each crystal number, ACCoCE communicates with the C.R.I.S.T.A.L. [8] system and its &Objectivity' database, in order to know what has to be measured next. After each type of measurement, some calculations take place and all the data are transferred to the database. The present total time is about 7 h for 20 crystals. One crystal is in fact a reference crystal, which is never moved and allows to check all the measurements stability. 3. Dimension measurement For each face of a measured crystal, a plane is "tted to the measured points. The planarity of this face is de"ned as the distance between the two planes parallel to the "tted plane and passing by the points most distant from it, outside and inside. With these planes, three volumes can be de"ned: the average volume corresponding to the "tted planes, the outside volume and the inside volume. The corners are then de"ned as intersection of three planes and the dimensions are derived according to their de"nition (see Fig. 4). The average, outside and inside volumes yield respectively the average, the maximum (relevant for penetration in alveolus) and minimum dimensions. Four values of the length are de"ned: one is along the side line perpendicular to the end faces (PW intersect); the three others are de"ned as the length between the three other small section corners and their projections on the large section, parallel to the PW intersect line. Four length values can also be de"ned for the outer and inner crystal volume. For fast comparisons or for physics, the average of the four average length values can be taken. A steel standard (SSD) was manufactured to the dimensions of a type six left crystal to a precision of the order of 10 lm. The SSD was measured three times in each of the 19 server positions, i.e. 57 times with SSD removed and repositionned each time. The 329 Table 1 Planarities and dimensions of the Steel Standard measured by ACCoCE1 and CERN Metrology Planarities Nominal *Accos 57 *MetroCERN F R P D N W 0 0 0 0 0 0 3 2.5 4.5 7 5 12 3 5 4 2 5 9 Dimensions Nominal *Accos 57 *MetroCERN AF BF CF AR BR CR L 21.831 22.601 21.999 25.435 26.182 25.630 230 !20 #15 !17 !7 !17 !3 !9 !7 #6 #1 #8 !12 #16 #10 distributions of front and rear dimensions (Fig. 5) show a very good reproducibility (p"0.8}1.3 lm). The planarity of each of the 6 faces is rather small and in good agreement with SSD measurements at the CERN metrology service (Table 1). The dimensions, compared to CERN metrology and to the nominal values for Type 6, show agreement well within 20 lm (Table 1). More precise knowledge of the SSD's e!ective dimensions is needed to establish the absolute precision of ACCoCe1. Long-term stability of dimension measurements can be seen (Figs. 6 and 7) on 61 measurements of the Reference crystal: R0488 (Type 6L), spread over a period of 6 months. A small shift can be observed on L2, L3 (&6 lm) and B (&12 lm) dimensions after February 20, which came back to the previous level after a calibration on March 5 and stayed very stable ever since. In fact, after March 5, a 3D calibration is systematically performed at the beginning of each run. The dispersions of all dimensions show sigmas below 4 lm. 4. Transmission measurements The transversal transmission (TT) spectrum was measured many times along the reference crystal 330 E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 Fig. 5. Distribution of the 57 steel standard measurements for dimensions front and rear, respectively. E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 Fig. 6. Stability of length (a), front (b), and rear dimensions (c) for the reference crystal measured from February to July 1999 (61 measurements). (R0488). Fig. 8 shows the very good superposition observed for sampled transmission curves measured from April to July at positions D"15, 115, 210 mm from the crystal small end. Fig. 9 presents the distribution at three wavelengths of the 62 measured TT values at the three positions along the crystals. The observed stability: p/mean &0.2% (&1% at 350 nm) is excellent. TT measurements on ACCoCE1 of &20 crystals were compared to measurements on the 331 CERN/Lab27 Reference spectrometer [9]. Fig. 10 shows correlation and di!erence in transmission between the two instruments at three wavelengths, using the measurements at all positions along the 20 crystals. The observed correlation is restricted by the small variation in transmission values from crystal to crystal. The larger dispersion and the shift of &2% observed for transmissions at 350 nm can be attributed to uncertainties in the wavelength de"nition in a spectrum region where the wavelength dependence of the transmission is very large. Longitudinal transmission was measured 76 times on crystal R0488, from April to July 99. Fig. 11 illustrates the very good superposition of some sampled curves. Fig. 12 shows the distributions at three wavelengths of the 76 LT measurements. A very small dispersion of the order of 0.5% is observed. At 350 nm, the e!ect of a temporary "lter drift, later cured, can be observed. Fig. 13 represents the correlation and di!erence at three wavelengths between LT measured on the reference spectrophotometer and ACCoCE1 for 104 crystals. The observed dispersions are small with again a &3% systematic shift for 350 nm. Similar to our reference spectrophotometer in B27, the ACCoCE1 spectrophotometer has been designed to provide adequate sensitivity to the possible presence of cloudy cores of bubbles or impurities along the axis of the crystal on part or totality of its length. When the density of such a core is high enough, it may a!ect the light yield of the crystal and in particular the uniformity of light collection, thus making the uniformisation process hazardous. High densities of scatters in crystals also a!ect the response of the monitoring system in uncontrolled ways and must therefore be avoided. For spectrophotometers not using integration spheres, the level of the longitudinal transmission is a!ected, which in principle permits rejection of the crystal. But the diameter of the light beam must be optimised for a moderate sensitivity to these clouds but not to miss them if they are o!-axis. We found that a diameter of 7 mm at crystal entrance resulting in 9 mm at crystal exit was optimum. Fig. 14 illustrates the very good agreement observed between ACCoCE1 and B27 reference spectrometer for LT measurements of two good crystals and a still satisfactory 332 E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 Fig. 7. (a) Histogram of the length dimensions for the reference crystal measured from February to July 1999. Histogram of the (b) front and (c) rear dimensions for the reference crystal measured from February to July 1999. E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 Fig. 8. Superposition of TT spectra measured at three positions along the reference crystal from April to July. 333 334 E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 Fig. 9. Distribution of the 62 TT measurements at three positions along the reference crystal for 350, 420 and 620 nm. Fig. 10. Correlation & di!erence between TT at three wavelengths values for each position of 20 crystals measured on ACCOS & B27 Reference spectrophotometer. E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 335 Fig. 11. Superposition of LT spectra measured from April to July on the reference crystal. agreement when the LT level is near or below speci"cation. A good stability of the band-edge slope, as de"ned by a linear "t to three points on transmission rise, can be observed in Fig. 15(a). Good correlation and small di!erences between slopes measured on our reference spectrophotometer in B27 and on ACCoCE1 spectrophotometer can be seen in Fig. 15(b and c). 336 E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 the parameters of the exponential "tting of the decay time spectrum. In fact, for all pre-production crystals measured, the ratio LY(100)/LY(1000) was found to be above 99%. The relative LY value (in % of e$ciency) in each position along a crystal is derived from the Poissonian probability of detecting zero light photon produced in PWO by c from a Na source event, when c is detected at 1803 in the Start telescope. This probability is proportional to the crystal light yield. To obtain absolute LY values in photoelectrons/MeV, average normalisation coe$cients were determined for typically 10 crystals measured both on ACCoCE1 and on the CERN/B27 pulse height analysis bench: B3. For LY pro"les and NU Factors, corrections for several di!erences in measuring conditions should be applied: E Di!erent geometry causing di!erent Compton contributions, E For ACCoCE1: absence of wrapping, of optical contact; distance to PM of &1 cm, E Di!erent PM quantum e$ciency spectra causing di!erent sensitivity to the emitted light, waveshifting along the crystals due to light absorption. Fig. 12. Distribution of the transmission values for 76 measurements from April to July 1999 at three wavelengths on the Reference crystal. 5. Decay time, light and uniformity measurements On ACCoCE1, a full crystal decay time spectrum in the range 0}1000 ns is recorded in 21 points along the crystal, allowing an e$cient detection of possible slow and medium-slow (the most dangerous for pulse shape determination) components. For a quick check of the crystals kinetic parameters, the LY fraction collected in the "rst 100 ns of the spectrum relative to the light in 1000 ns is derived from the recorded time spectra, as well as These corrections being relatively small and di$cult to calculate with su$cient accuracy, it was preferred to include an empirical correction in the normalisation coe$cients 1C 2 of the ACCoCE1 G LY, for each position i along crystals. For all crystals, each position on the ACCoCE1 LY curves was then multiplied by the relevant coe$cient LY (pe/MeV)"(C ';LY (ACCoCe1). G G G Typical values of these coe$cients are shown in Table 2. This set of coe$cients is checked for each batch and for each type of crystals. A good stability of the normalised and corrected LY curves, measured 43 times on the reference crystal R0488 from April to July 99 is observed on 17 sampled curves in Fig. 16(a). The distribution of the LY measured at 8X depth in the crystal (shower maximum) can be seen on Fig. 16(b) for the 43 measurements on crystal R0488. Fig. 16(c) shows the distribution of the NU E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 337 Fig. 13. Correlation and di!erence between LT values at three wavelength of 104 crystals measured on ACCoCE1 and B27 Reference spectrophotometer. Fig. 14. LT spectra for two good clear crystals and for two crystals near speci"cation limit due to cloudy cores. 338 E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 Fig. 15. (a) Distribution of the band edge slope on 76 measurements of the reference crystal from April to July 99. (b) Correlation and di!erence between band-edge slope values of 104 crystals measured on ACCOS and (c) B27 Reference spectrophotometer. Factor (NUF "relative slope of the linear "t to the LY values in "rst half of crystal) for the 43 measurements of the reference crystal. Fig. 16. (a) Superposition of the LY non-uniformity curvesmeasured from April to July on the reference crystal. (b) Distribution of respectively the normalised LY at 8X values and (c) FNUF for 43 measurements from April to July 1999 of the reference crystal. Fig. 17 shows the correlations and di!erences between B3 and normalised ACCoCE1 measurements for LY and NUF for 54 crystals not used in E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 339 Table 2 Normalisation coe$cients (including corrections) for 21 positions along crystals Pos. 15 (mm) Ci 25 35 45 36.6 34.4 33.9 33.5 55 65 33.3 33.1 75 85 33.1 32.9 95 105 115 125 135 145 155 165 175 185 195 205 215 32.8 32.9 32.9 33.0 32.8 33.1 33.1 33.4 33.8 34.6 35.4 36.2 37.0 Fig. 17. Correlation and di!erence between the LY and NUF values of 54 crystals measured on ACCoCE1 and B27 Reference LY Bench (B3). Fig. 18. Photograph of ACCoCE machine for Bogoroditsk. 340 E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 the normalisation procedure. The observed LY correlation is good with a dispersion: p&7% and no signi"cant residual di!erence, taking into account that crystals of four types are normalised using the same coe$cients. The observed NUF correlation is excellent with a dispersion: p&0.12%/X and no signi"cant residual di!erence showing that 10 crystals for determining the normalisation coe$cients are su$cient in statistics. for the delivery of 11 000 BGO crystals, has never been used at a scale as large as for CMS: 80 000 PWO crystals. Moreover, the installation of similar machines at the producer plants will mean double control of each crystal, not only reducing the percentage of rejected crystals at reception, but also giving best chance of high-quality crystals with well-known and recorded characteristics. Acknowledgements 6. Conclusion The reproducibility and long-term stability of ACCoCE1 measurements having been established and con"rmed by the measurement since April 99 of more than 1000 pre-production crystals, we can state that the machine is now ready to face control of the crystal production at a rate of currently 2;20 crystals/day (&60 in 3 shifts, if necessary). ACCoR (Rome) will soon be operating at a similar capacity. To reduce the fraction of crystals to be rejected because they do not satisfy to speci"cations (at present ranging from 16% to 20%), it was agreed to equip the producers with similar systems. A second ACCoCE machine, with increased capacity (30 crystals) and assisted loading (no manual handling of the crystals) (Fig 18), was constructed and commissioned at CERN, before being transported and installed in Bogoroditsk (Russia) end of July. To face deliveries at CERN, which will constantly be near the 1000/month level in years 2000}2005, means to be capable of controlling up to 100 crystals/day during peak periods, if one takes into account remeasurements, maintenance, special tests and breakdowns. This is why a third machine with same capacity and loading as ACCoCE2 will be assembled in fall at CERN and should be in operation beginning of year 2000. ACCoCE1 will later be upgraded, so that CERN Regional Centre will have a capacity of &120 crystals/day in two shifts. The successful start of ACCoS machines also highlights the success of a concept: the full characterisation of each delivered crystal. This concept, already applied with success in L3 experiment We are deeply indebted to A. Federov and M. Korjic (INP Minsk) for their essential contribution to ACCoS conceptual studies and for their constant support. We are very grateful to G. Dromby, P. Letournel and A. Oriboni for their excellent work on the prototype construction at LAPP and also to B. Buisson, H. Cabel, A. Conde-Garcia, A. Deforni, R. Morino and V. Panov for their invaluable help in installing, tuning and running ACCoCE1 at CERN. We are also indebted to our Software team for providing the very powerful C.R.I.S.T.A.L system, particularly to Z. Kovacs and M. Zsenei. We would like to thank warmly all our collaborators of the CMS/ECAL community and in particular the ECAL/Rome group for many illuminating and stimulating discussions. References [1] The Compact Muon Solenoid, CMS Technical Proposal, CERN/LHCC 94-38, LHCC/P1, December 15, 1994. [2] The Electromagnetic Calorimeter Project, Technical Design Report, CERN/LHCC 97-33, CMS TDR 4, December 15, 1997. [3] E. Au!ray, M. Lebeau, P. Lecoq, M. Schneegans, Speci"cations for lead tungstate crystals preproduction, CMS-Note 98/038, May 19, 1998. [4] G. Drobychev, et al., Studies and proposals for an automatic crystal Control system (ACCOS), CMS-Note 1997/036. [5] E. Au!ray, et al., Certifying procedures for lead tungstate crystal parameters during mass production for the CMS ECAL, Proceedings of the 1998 IEEE Nuclear Science Symposium Conference Record. Toronto, Canada, November, 1998, Vol.1, pp. 508}13 [6] G. Basti, et al., A proposal for an automatic crystal control system, CMS-IN 97/033, 1997. E. Auwray et al. / Nuclear Instruments and Methods in Physics Research A 456 (2001) 325}341 [7] W.W. Moses, A method to increase optical timing spectra measurement rates using a multi-hit TDC, Nucl. Instr. and Meth. A 336 (1993) 253. [8] J.-M. Le Go! et al., C. R. I. S. T. A. L./ concurrent repository and information system for tracking assembly and 341 production lifecycles } a data capture and production management tool for the assembly and construction of the CMS ECAL detector, CMS Note/1996 } 003. [9] C. Laviron, P. Lecoq, private communication.
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