Test Report No. CANEC1305830001 Date: 08 May 2013 HANGZHOU SILAN INTEGRATED CIRCUIT CO., LTD. NO 308,NO.10 ROAD,EAST ZONE,ECONOMY&TECHNOLOGY DEVELOPMENT AREA,XIASHA,HANGZHOU CHINA The following sample(s) was/were submitted and identified on behalf of the applicant as DICE SGS Job No. Date of sample received Testing Period Test Requested Test Method Test Results : CP13-020202 - GZ : 24 Apr 2013 : 24 Apr 2013 - 03 May 2013 : Selected test (s) as requested by client. : Please refer to next page(s). : Please refer to next page(s). Signed for and on behalf of SGS-CSTC Ltd Signed for and on behalf of SGS-CSTC Ltd. ______________________ Kenny Wang Approved Signatory ______________________ Michelle Song Approved Signatory Page 1 of 26 Test Report No. CANEC1305830001 Date: 08 May 2013 Page 2 of 26 Test Results: Test Part Description: Specimen No. SGS Sample ID 1 CAN13-058300.001 Description Silvery"chip" Remarks: (1) (2) (3) (4) 1 mg/kg = 1 ppm = 0.0001% MDL = Method Detection Limit ND = Not Detected (<MDL) “-“ = Not Regulated Diarsenic pentaoxide, Diarsenic trioxide, Boric acid, Disodium tetraborate, anhydrous Tetraboron disodium heptaoxide, hydrate Test Result: (Substances in the Candidate List of SVHC) Test Method : SGS In-House method-GZTC CHEM-TOP-092-01, Analyzed by ICP-OES. Test Item(s) Diarsenic pentaoxide Diarsenic trioxide Boric acid Disodium tetraborate, anhydrous Tetraboron disodium heptaoxide, hydrate CAS_NO 1303-28-2 1327-53-3 10043-35-3 11113-50-1 1303-96-4 1330-43-4 12179-04-3 12267-73-1 Unit % (w/w) % (w/w) % (w/w) MDL 0.005 0.005 0.005 001 0.093 0.080 ND % (w/w) 0.005 ND % (w/w) 0.005 ND Notes : 1. * Calculated concentration of Diarsenic pentaoxide,Diarsenic trioxide are based on the arsenic by ICP-OES.Calculated concentration of boric acid, disodium tetraborate, anhydrous and tetraboron disodium heptaoxide, hydrate are based on the total/water extractive boron and sodium by ICP-OES. Test Report No. CANEC1305830001 Date: 08 May 2013 Page 3 of 26 4-(1,1,3,3-tetramethylbutyl)phenol, Bis(2-methoxyethyl) ether, N,N-dimethylacetamide; , 1,2-dimethoxyethane; ethylene glycol dimethyl ether (EGDME) Test Method : SGS In-House method- GZTC CHEM-TOP-092-02, Analyzed by GC-MS. Test Item(s) 4(1,1,3,3-tetramethylbutyl)phen ol Bis(2-methoxyethyl) ether N,N-dimethylacetamide EGDME CAS_N 140-66-9 111-96-6 127-19-5 110-71-4% Unit % (w/w) MDL 0.050 001 ND % (w/w) % (w/w) % (w/w) 0.050 0.050 0.005 ND ND ND SS- -00259 Test Method: (1) (2) (3) (4) With reference to IEC 62321:2008(Section 8/9/10) Determination of Cadmium by ICP-OES. With reference to IEC 62321:2008(Section 8/9/10) Determination of Lead by ICP-OES. With reference to IEC 62321:2008(Section 7) Determination of Mercury by ICP-OES. With reference to IEC 62321:2008(Annex C) Determination of Hexavalent Chromium by Colorimetric Method using UV-Vis. (5) With reference to IEC 62321:2008(Annex A) Determination of PBBs and PBDEs by GC-MS. Test Item(s): Cadmium(Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium (Cr(VI)) Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Unit mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg MDL 2 2 2 2 5 5 5 5 5 5 5 5 5 001 ND ND ND ND ND ND ND ND ND ND ND ND ND ND Test Report No. CANEC1305830001 Decabromobiphenyl Sum of PBDEs Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether Octabromodiphenyl ether Nonabromodiphenyl ether Decabromodiphenyl ether mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Date: 08 May 2013 5 5 5 5 5 5 5 5 5 5 5 Page 4 of 26 ND ND ND ND ND ND ND ND ND ND ND ND Hexabromocyclododecane (HBCDD) Test method: Determination of HBCDD by GC-MS based EPA 3550C:2007. Test Item(s): Hexabromocyclododecane (HBCDD) Unit mg/kg MDL 10 001 ND Note: (1) Reference Information: Directive 2011/65/EU recasting RoHS directive 2002/95/EC: Hexabromocyclododecane (HBCDD) is considered as a priority for risk evaluation and substance restriction. Phthalates Test Method: Determination of phthalates by GC-MS based on EN 14372:2004. Test Item(s): Dibutyl phthalate (DBP) Butyl benzyl phthalate (BBP) Bis (2-ethylhexyl) phthalate (DEHP) Unit MDL 001 %(w/w) %(w/w) %(w/w) 0.003 0.003 0.003 ND ND ND Note: (1) Reference Information: Directive 2011/65/EU recasting RoHS directive 2002/95/EC: Bis (2-ethylhexyl) phthalate (DEHP), Butyl benzyl phthalate (BBP) and Dibutyl phthalate (DBP) are considered as a priority for risk evaluation and substance restriction. Test Report No. CANEC1305830001 Date: 08 May 2013 Page 5 of 26 Polychlorinated Biphenyls (PCBs) Test Method: With reference to US EPA Method 8082A:2007, analysis was performed by GC-MS. Test Item(s): 2.4.4’-Trichlorobiphenyl (PCB 28) 2.2’.5.5’-Tetrachloro-biphenyl (PCB 52) 2.2’.4.5.5’-Pentachloro-biphenyl (PCB 101) 2.3’.4.4’.5-Pentachlorobiphenyl (PCB 118) 2.2’3.4.4’.5’-Hexachloro-biphenyl (PCB 138) 2.2’.4.4’.5.5’-Hexachloro-biphenyl (PCB 153) 2.2’.3.4.4’.5.5’- Heptachlorobiphenyl (PCB 180) CAS No. 7012-37-5 35693-99-3 37680-73-2 31508-00-6 35065-28-2 35065-27-1 35065-29-3 Unit mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg MDL 0.5 0.5 0.5 0.5 0.5 0.5 0.5 001 ND ND ND ND ND ND ND Polychlorinated Naphthalenes (PCNs) Test Method: With reference to US EPA Method 8081B:2007, analysis was performed by GC-MS. Test Item(s): 1-Chlorinated Naphthalene 2-Chlorinated Naphthalene 1,4-Dichlorinated Naphthalene 1,5-Dichlorinated Naphthalene 1,2-Dichlorinated Naphthalene 1,8-Dichlorinated Naphthalene 1,2,3-Trichlorinated Naphthalene 1,2,3,4-Tetrachlorinated Naphthalene 1,2,3,4,6-Pentachlorinated Naphthalene Octa-chlorinaed Naphthalene Unit mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg MDL 5 5 5 5 5 5 5 5 5 5 001 ND ND ND ND ND ND ND ND ND ND Test Report No. CANEC1305830001 Date: 08 May 2013 Page 6 of 26 Polychlorinated Terphenyls (PCTs) Test Method: With reference to US EPA Method 8082A:2007, analysis was performed by GC-ECD/MS. Test Item(s): Aroclor5432 Aroclor5442 Aroclor5460 Unit mg/kg mg/kg mg/kg MDL 5 5 5 001 ND ND ND Note: (1) PCTs Reference Information: Entry 1 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006 (previously restricted under Directive 89/677/EC) Shall not be placed on the market, or used: — as substances, — In mixtures, including waste oils, or in equipment, in concentrations greater than 50 mg/kg (0,005 % by weight). Please refer to Regulation (EC) No 552/2009 to get more detail information. SCCP (Short chained chlorinated paraffins) Test Method: With reference to US EPA 3550C:2007, analysis was performed by GC-ECD. Test Item(s) Short Chained Chlorinated Paraffins (C10-C13) Unit MDL 001 mg/kg 50 ND Organic-Tin compounds Test Method: With reference to ISO 17353:2004, analysis was performed by GC-MS. Test Item(s): Dibutyltin (DBT) Tributyltin (TBT) Triphenyltin (TPhT) Dioctyltin (DOT) Unit mg/kg mg/kg mg/kg mg/kg MDL 0.02 0.02 0.02 0.02 001 ND ND ND ND PFOS (Perfluorooctane sulfonates) Test Method: With reference to US EPA Method 3550C:2007, analysis was performed by LC-MS. Test Item(s) Perfluorooctane sulfonates (PFOS) PFOS – Acid PFOS – Metal Salt PFOS – Amide Unit MDL 001 mg/kg 10 ND Test Report No. CANEC1305830001 Date: 08 May 2013 Page 7 of 26 For reference: commission regulation (EU) No 757/2010 amending regulation (EC) No 850/2004: (1) For the purposes of this entry, Article 4(1) (b) shall apply to concentrations of PFOS equal to or below 10 mg/kg (0,001 % by weight) when it occurs in substances or in preparations. (2) For the purposes of this entry, Article 4(1) (b) shall apply to concentrations of PFOS in semi-finished products or articles, or parts thereof, if the concentration of PFOS is lower than 0,1 % by weight calculated with reference to the mass of structurally or micro-structurally distinct parts that contain PFOS or, for textiles or other coated materials, if the amount of PFOS is lower than 1µg /m 2 of the coated material. Benzotriazole UV absorbent Test Method: With reference to US EPA Method 3550C:2007, analysis was performed by GC-MS. Test Item(s): 2-(3,5-Di-tert-butyl-2-hydroxyphenyl) benzotriazole(UV-320) CAS No. 3846-71-7 Unit mg/kg MDL 5 001 ND Commission Decision 2011/135/EU (previously restricted under 2010/153/EU and 2009/251/EC) – Dimethyl fumarate(DMF) Test Method: SGS Inhouse method (GZTC CHEM-TOP-095), analysis was performed by GC-MS. Test Item(s): Recommended Max. Limit Unit MDL 001 0.1 mg/kg 0.1 ND - - - PASS Dimethyl fumarate(DMF) Conclusion Note: (1) The maximum permissible limit is quoted from the document EU Directive 2011/135/EU (previously restricted under 2010/153/EU and 2009/251/EC) Phthalates Content Test Method: With reference to EN 14372:2004, analysis was performed by GC-MS. Test Item(s): Dibutyl Phthalate (DBP) Content Benzylbutyl Phthalate (BBP) Content Bis-(2-ethylhexyl) Phthalate (DEHP) Content Diisononyl Phthalate (DINP) Content Di-n-octyl Phthalate (DNOP) Content Diisodecyl Phthalate (DIDP) Content Unit %(w/w) %(w/w) %(w/w) %(w/w) %(w/w) %(w/w) MDL 0.003 0.003 0.003 0.010 0.003 0.010 001 ND ND ND ND ND ND Test Report No. CANEC1305830001 Diisobutyl Phthalate (DIBP) Content Di-n-hexyl Phthalate (DnHP) Content 1,2-Benzenedicarboxylic acid, di-C6-8branched alkyl esters, C7-rich (DIHP) Content 1,2-Benzenedicarboxylic acid, di-C7-11branched and linear alkyl esters (DHNUP) Content Di-methoxyethyl Phthalate (DMEP) Content Diisopentyl Phthalate(DIPP) Content n-pentyl-Isopentyl Phthalate(nPiPP) Content 1,2-Benzenedicarboxylic acid, dipentyl ester, branched and linear(C5-PHTH) Notes: Date: 08 May 2013 %(w/w) %(w/w) 0.003 0.003 ND ND %(w/w) 0.010 ND %(w/w) 0.010 ND %(w/w) %(w/w) %(w/w) 0.003 0.003 0.003 ND ND ND %(w/w) 0.010 ND Page 8 of 26 (1) C5-PHTH=DPP+DIPP+nPiPP Polyvinyl chloride (PVC) Test Method: SGS in house method (GZTC CHEM-TOP-066), analysis was performed by FTIR. Test Item(s): Polyvinyl chloride (PVC) CAS No. 9002-86-2 001 Negative Note: (1) Negative = Undetectable, Positive = Detectable. Ozone Depleting Substances (ODS) No. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 Test Item(s) CFC CFC-11 CFC-12 CFC-13 CFC-111 CFC-112 CFC-112 CFC-113 CFC-113 CFC-114 CFC-114 CFC-115 CFC-211 CFC-212 CFC-213 CFC-214 CFC-215 CFC-215 CAS No. 75-69-4 75-71-8 75-72-9 354-56-3 76-11-9 76-12-0 354-58-5 76-13-1 374-07-2 76-14-2 76-15-3 422-78-6 661-96-1 1652-89-7 677-68-9 1599-41-3 76-17-5 Unit - mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Test Method (Reference) - EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS Result N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. MDL - 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 Test Report 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 CFC-216 CFC-216 CFC-217 HCFC HCFC-21 HCFC-22 HCFC-31 HCFC-121 HCFC-122 HCFC-123 HCFC-123a HCFC-124 HCFC-124a HCFC-131 HCFC-131a HCFC-132a HCFC-132b HCFC-133a HCFC-141b HCFC-142b HCFC-221 HCFC-222 HCFC-223 HCFC-225ca HCFC-225cb HCFC-226 HCFC-231 HCFC-232 HCFC-233 HCFC-234 HCFC-235 HCFC-241 HCFC-242 HCFC-243 HCFC-244 HCFC-251 HCFC-252 HCFC-253 HCFC-261 HCFC-261 HCFC-271 HCFC-262 HCFC-262 HBFC CHF2Br CH 2FBr C 2HFBr4 C2HF2Br3 C2HF3Br2 C 2HF4Br No. CANEC1305830001 661-97-2 1652-80-8 422-86-6 CAS No. 75-43-4 75-45-6 593-70-4 354-14-3 354-21-2 306-83-2 354-23-4 2837-89-0 354-25-6 359-28-4 811-95-0 471-43-2 1649-08-7 75-88-7 1717-00-6 75-68-3 422-26-4 422-30-0 422-52-6 422-56-0 507-55-1 431-87-8 421-94-3 460-89-9 7125-84-0 425-94-5 460-92-4 666-27-3 460-63-9 338-75-0 679-85-6 421-41-0 819-00-1 460-35-5 7799-56-6 420-97-3 430-55-7 102738-79-4 420-99-5 CAS No. 1511-62-2 373-52-4 354-04-1 - mg/kg mg/kg mg/kg - mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg - mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Date: 08 May 2013 EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS - EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS - EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS Page 9 of 26 N.D. N.D. N.D. - N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 - 0.1 0.1 0.1 0.1 0.1 0.1 Test Report 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 111 112 C2H 2FBr3 C2H2F2Br2 C2H 2F3Br C2H 3FBr2 C2H 3F2Br C 2H4FBr C 3HFBr6 C3HF2Br5 C3HF3Br4 C3HF4Br3 C3HF5Br2 C 3HF6Br C3H 2FBr5 C3H2F2Br4 C3H2F3Br3 C3H2F4Br2 C3H 2F5Br C3H 3FBr4 C3H3F2Br3 C3H3F3Br2 C3H 3F4Br C3H 4FBr3 C3H4F2Br2 C3H 4F3Br C3H 5FBr2 C3H 5F2Br C 3H6FBr HALON Halon 1211 Halon 1301 Halon 2402 OTHERS Dibromofluoromethane Methyl bromide Bromochloromethane HFC HFC-23 HFC-32 HFC-41 HFC-43-10mee HFC-125 HFC-134 HFC-134a HFC-152a HFC-143 HFC-143a HFC-227ea HFC-236 cb HFC-236ea HFC-236fa No. CANEC1305830001 75-82-1 421-06-7 359-07-9 762-49-2 CAS No. 353-59-3 75-63-8 124-73-2 CAS No. 1868-53-7 74-83-9 74-97-5 CAS No. 75-46-7 75-10-5 593-53-3 354-33-6 359-35-3. 811-97-2 75-37-6 420-46-2 430-66-0 431-63-0 690-39-1 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg - mg/kg mg/kg mg/kg - mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Date: 08 May 2013 EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS - EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS - EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS Page 10 of 26 N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. - N.D. N.D. N.D. - N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 - 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 Test Report 113 114 115 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 HFC-245ca HFC-245fa HFC-365mfc PFC Perfluoromethane Perfluoroethane Perfluoropropane Perfluorobutane Perfluoropentane Perfluorohexane Perfluorocyclobutane CHC 1,3-dichloropropane 2,2-dichloropropane Carbon tetrachloride Chloroethane Chloroform Chloromethane Cis-1,2-dichloroethene Cis-1,3-dichloropropene Hexachlorobutadiene Methylene chloride Tetrachloroethylene Trans-1,2-dichloroethene Trans-1,3dichloropropene Trichloroethylene 1,1,1,2-tetrachloroethane 1,1,1-trichloroethane 1,1,2,2-tetrachloroethane 1,1,2-trichloroethane 1,1-dichloroethane 1,1-dichloroethene 1,1-dichloropropene 1,2,3-trichloropropane 1,2-dichloroethane 1,2-dichloropropane Note: 1. N.D. = Not Detected (<MDL) 2. MDL = Method Detection Limit No. CANEC1305830001 Date: 08 May 2013 Page 11 of 26 679-86-7 CAS No. 75-73-0 76-16-4 76-19-7 355-25-9 678-26-2 355-42-0 115-25-3 CAS No. 142-28-9 594-20-7 56-23-5 75-00-3 67-66-3 74-87-3 156-59-2 10061-01-5 87-68-3 75-09-2 127-18-4 156-60-5 mg/kg mg/kg mg/kg - mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg - mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS - EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS - EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS N.D. N.D. N.D. - N.D. N.D. N.D. N.D. N.D. N.D. N.D. - N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. 0.1 0.1 0.1 - 0.1 0.1 0.1 0.1 0.1 0.1 0.1 - 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 10061-02-6 mg/kg EPA 5021A:2003, HS-GC-MS N.D. 0.1 79-01-6 630-20-6 71-55-6 79-34-5 79-00-5 75-34-3 75-35-4 563-58-6 96-18-4 107-06-2 78-87-5 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS EPA 5021A:2003, HS-GC-MS N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 Test Report No. CANEC1305830001 Date: 08 May 2013 Page 12 of 26 Formaldehyde Test Method: With reference to ISO 17226-1:2008, analysis was preformed by HPLC-DAD. Test Item(s): Formaldehyde Unit mg/kg MDL 16 001 ND Halogen Test Method: With reference to EN 14582:2007, analysis was performed by IC. Test Item(s): Chlorine (Cl) Unit mg/kg MDL 50 001 ND Bromine (Br) mg/kg 50 ND Asbestos Test Method: With reference to NIOSH 9000:1994& NIOSH 9002:1994, analysis was performed by XRD&PLM. Test Item (s) Chrysotile Amosite Crocidolite Anthophyllite Tremolite Actinolite CAS NO 012001-29-5 012172-73-5 012001-28-4 077536-67-5 077536-68-6 077536-66-4 Note: (1) Negative < 0.1%(w/w), Positive ≥0.1%(w/w) Unit %(w/w) %(w/w) %(w/w) %(w/w) %(w/w) %(w/w) MDL 0.1 0.1 0.1 0.1 0.1 0.1 001 Negative Negative Negative Negative Negative Negative Test Report No. CANEC1305830001 Date: 08 May 2013 Page 13 of 26 Azo Dyes Test Method: Textile: According to BS EN 14362-1:2012 – Analysis was conducted with GC-MS/HPLC-DAD. Determination of 4-aminoazobenzene (CAS No.:60-09-3) –EN14362-3:2012; with the use of Gas Chromatography – Mass Spectrometry (GC-MS) Test Item(s) 4-Aminobiphenyl Benzidine 4-Chlor-o-toluidine 2-Naphthylamine o-Aminoazotoluene 5-nitro-o-toluidine / 2-Amino-4-nitrotoluene 4-Chloroaniline 4-methoxy-m-phenylenediamine /2,4-Diaminoanisole 4,4'-Diaminodiphenylmethane 3,3'-Dichlorobenzidine 3,3'-Dimethoxybenzidine 3,3'-Dimethybenzidine 4,4'-methylenedi-o-toluidine / 3,3'-Dimethyl-4,4'-diaminodiphenyl methane p-Cresidine 4,4'-Methylene-bis-(2-chloroaniline) 4,4'-Oxydianiline 4,4'-Thiodianiline o-Toluidine 4-methyl-m-phenylenediamine / 2,4-Toluylendiamine 2,4,5-Trimethylaniline 4-aminoazobenzene O-Anisidine 2,4-Xylidine 2,6-Xylidine CAS No. Unit MDL 001 92-67-1 92-87-5 95-69-2 91-59-8 97-56-3 mg/kg mg/kg mg/kg mg/kg mg/kg 5 5 5 5 5 ND ND ND ND ND 99-55-8 mg/kg 5 ND 106-47-8 mg/kg 5 ND 615-05-4 mg/kg 5 ND 101-77-9 91-94-1 119-90-4 119-93-7 mg/kg mg/kg mg/kg mg/kg 5 5 5 5 ND ND ND ND 838-88-0 mg/kg 5 ND 120-71-8 101-14-4 101-80-4 139-65-1 95-53-4 mg/kg mg/kg mg/kg mg/kg mg/kg 5 5 5 5 5 ND ND ND ND ND 95-80-7 mg/kg 5 ND 137-17-7 60-09-3 90-04-0 95-68-1 87-62-7 mg/kg mg/kg mg/kg mg/kg mg/kg 5 5 5 5 5 ND ND ND ND ND Notes : (1)The BS EN 14362-1/2 and ISO 17234-1 methods will enable further cleavage of 4-aminoazobenzene to non-forbidden amines: aniline and 1,4-phenylenediamine, therefore, the test method of § 64 LFGB, BVL, B 82.02.9 was employed to verify the presence of 4-aminoazobenzene. Test Report No. CANEC1305830001 Date: 08 May 2013 Page 14 of 26 Tris(2-chloroethyl) phosphate Test Method: With reference to EN71-11, analysis was performed by LC-MS. Test Item(s) Tris(2-chloroethyl) phosphate Unit MDL 001 mg/kg 5.0 ND Element(s) Test Method: With reference to US EPA Method 3052:1996, analysis was performed by ICP-OES. Unit mg/kg Test Item(s): Beryllium (Be) MDL 001 5 ND Beryllium oxide (BeO) Test Method: With reference to US EPA Method 3052:1996, analysis was performed by ICP-OES. Test Item(s): Beryllium oxide (BeO) ◆ Unit mg/kg MDL 15 001 ND Note: (1) ◆BeO: Calculate from Beryllium content CoCl2 (Cobalt dichloride) Test Method: With reference to SGS In House Method(GZRD-R&D-TOP-104) & EPA 3052:1996, analysis was performed by IC & ICP-OES. Test Item(s): CoCl2 Note: Unit mg/kg MDL 100 001 ND CoCl2: Result is calculated based on the results of Cobalt and Chloride contents. Test Report No. CANEC1305830001 Date: 08 May 2013 Page 15 of 26 Perchlorate Test Method: With reference to SGS In-house method (GZTC-R&D-TOP-287), analysis was performed by LC-MSMS. Test Item(s) Perchlorate Unit µg/kg MDL 5 001 ND Test Report No. CANEC1305830001 Date: 08 May 2013 ATTACHMENTS SVHC Testing Flow Chart 1) Name of the person who made testing: Michael Tso / Liu Qiong 2) Name of the person in charge of testing: Adams Yu / Yolanda Wei Sample cutting/preparation Sample measurement Sample Pretreatment Instrumental Analysis DATA Page 16 of 26 Test Report No. CANEC1305830001 Date: 08 May 2013 Page 17 of 26 ATTACHMENTS RoHS Testing Flow Chart 1) Name of the person who made testing: Michael Tso / Cutey Yu 2) Name of the person in charge of testing: Adams Yu / Yolanda Wei 3) These samples were dissolved totally by pre-conditioning method according to below flow chart (Cr6+ and PBBs/PBDEs test method excluded). Sample Preparation Sample Measurement Pb/Cd/Hg Acid digestion with microwave/ hotplate Sample solvent extraction Filtration Concentration/ Dilution of extraction solution Solution Residue Filtration 1) Alkali Fusion / Dry Ashing 2) Acid to dissolve ICP-OES/AAS DATA Cr6+ PBBs/PBDEs GC-MS DATA Nonmetallic material Adding digestion reagent Heating to 90~95℃ for extraction Filtration and pH adjustment Adding 1,5diphenylcarbazide for color development Metallic material Positive Spot test Negative Boiling water extraction Adding 1,5diphenylcarbazide for color development UV-Vis A red color indicates the presence of Cr6+. If necessary, confirm with UV-Vis. DATA DATA Test Report No. CANEC1305830001 ATTACHMENTS HBCDD Testing Flow Chart 1) Name of the person who made testing: Cutey Yu 2) Name of the person in charge of testing: Yolanda Wei Sample cutting / preparation Sample Measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Date: 08 May 2013 Page 18 of 26 Test Report No. CANEC1305830001 ATTACHMENTS Phthalates Testing Flow Chart 1) Name of the person who made testing: Liu Qiong 2) Name of the person in charge of testing: Yolanda Wei Sample cutting / preparation Sample Measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Date: 08 May 2013 Page 19 of 26 Test Report No. CANEC1305830001 ATTACHMENTS SCCP/MCCP Testing Flow Chart 1) Name of the person who made testing: Liu Qiong 2) Name of the person in charge of testing: Yolanda Wei Sample cutting / preparation Sample Measurement Solvent extraction Concentration Clean-Up Filtration GC-ECD DATA Date: 08 May 2013 Page 20 of 26 Test Report No. CANEC1305830001 Date: 08 May 2013 ATTACHMENTS PFOA / PFOS Testing Flow Chart 1) Name of the person who made testing: Tina Zhao 2) Name of the person in charge of testing: Yolanda Wei Sample cutting / preparation Sample Measurement Solvent extraction Concentration/Dilution Filtration LC-MS DATA Page 21 of 26 Test Report No. CANEC1305830001 ATTACHMENTS Dimethyl Fumarate Testing Testing Flow Chart 1) Name of the person who made testing: Liu Qiong 2) Name of the person in charge of testing: Yolanda Wei Sample cutting / preparation Sample Measurement Solvent extraction Concentration/Dilution Filtration GC-MS DATA Date: 08 May 2013 Page 22 of 26 Test Report No. CANEC1305830001 ATTACHMENTS PVC Testing Flow Chart 1) Name of the person who made testing: Cutey Yu 2) Name of the person in charge of testing: Yolanda Wei Sample cutting/preparation FTIR Check wave-number of C-Cl bonding DATA Date: 08 May 2013 Page 23 of 26 Test Report ATTACHMENTS No. CANEC1305830001 Date: 08 May 2013 Halogen Testing Flow Chart 1) Name of the person who made testing: Bella Wang 2) Name of the person in charge of testing: Adams Yu Sample cutting / preparation Sample Measurement Combustion in oxygen bomb Dissolved in an absorption solution Filtration Analyzed by ion chromatography. Double confirm by other instruments, if necessary DATA Page 24 of 26 Test Report ATTACHMENTS No. CANEC1305830001 Elementary Testing Flow Chart 1) Name of the person who made testing: Bella Wang 2) Name of the person in charge of testing: Adams Yu Sample cutting / preparation Sample Measurement Acid digestion Filtration Solution ICP-OES/AAS DATA Date: 08 May 2013 Page 25 of 26 Test Report No. CANEC1305830001 Date: 08 May 2013 Sample photo : CANEC1305830001 CANEC1305830001 CAN13-058300.001 SGS authenticate the photo on original report only *** End of Report *** Page 26 of 26
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