Test Report

Test Report
No. CANEC1305830001
Date: 08 May 2013
HANGZHOU SILAN INTEGRATED CIRCUIT CO., LTD.
NO 308,NO.10 ROAD,EAST ZONE,ECONOMY&TECHNOLOGY DEVELOPMENT
AREA,XIASHA,HANGZHOU CHINA
The following sample(s) was/were submitted and identified on behalf of the applicant as DICE
SGS Job No.
Date of sample received
Testing Period
Test Requested
Test Method
Test Results
: CP13-020202 - GZ
: 24 Apr 2013
: 24 Apr 2013 - 03 May 2013
: Selected test (s) as requested by client.
: Please refer to next page(s).
: Please refer to next page(s).
Signed for and on behalf of
SGS-CSTC Ltd
Signed for and on behalf of
SGS-CSTC Ltd.
______________________
Kenny Wang
Approved Signatory
______________________
Michelle Song
Approved Signatory
Page 1 of 26
Test Report
No. CANEC1305830001
Date: 08 May 2013
Page 2 of 26
Test Results:
Test Part Description:
Specimen No.
SGS Sample ID
1
CAN13-058300.001
Description
Silvery"chip"
Remarks:
(1)
(2)
(3)
(4)
1 mg/kg = 1 ppm = 0.0001%
MDL = Method Detection Limit
ND = Not Detected (<MDL)
“-“ = Not Regulated
Diarsenic pentaoxide, Diarsenic trioxide, Boric acid, Disodium tetraborate, anhydrous Tetraboron disodium
heptaoxide, hydrate
Test Result: (Substances in the Candidate List of SVHC)
Test Method : SGS In-House method-GZTC CHEM-TOP-092-01, Analyzed by ICP-OES.
Test Item(s)
Diarsenic pentaoxide
Diarsenic trioxide
Boric acid
Disodium tetraborate,
anhydrous
Tetraboron disodium
heptaoxide, hydrate
CAS_NO
1303-28-2
1327-53-3
10043-35-3
11113-50-1
1303-96-4
1330-43-4
12179-04-3
12267-73-1
Unit
% (w/w)
% (w/w)
% (w/w)
MDL
0.005
0.005
0.005
001
0.093
0.080
ND
% (w/w)
0.005
ND
% (w/w)
0.005
ND
Notes :
1. * Calculated concentration of Diarsenic pentaoxide,Diarsenic trioxide are based on the arsenic by
ICP-OES.Calculated concentration of boric acid, disodium tetraborate, anhydrous and tetraboron
disodium heptaoxide, hydrate are based on the total/water extractive boron and sodium by ICP-OES.
Test Report
No. CANEC1305830001
Date: 08 May 2013
Page 3 of 26
4-(1,1,3,3-tetramethylbutyl)phenol, Bis(2-methoxyethyl) ether, N,N-dimethylacetamide; , 1,2-dimethoxyethane;
ethylene glycol dimethyl ether (EGDME)
Test Method : SGS In-House method- GZTC CHEM-TOP-092-02, Analyzed by GC-MS.
Test Item(s)
4(1,1,3,3-tetramethylbutyl)phen
ol
Bis(2-methoxyethyl) ether
N,N-dimethylacetamide
EGDME
CAS_N
140-66-9
111-96-6
127-19-5
110-71-4%
Unit
% (w/w)
MDL
0.050
001
ND
% (w/w)
% (w/w)
% (w/w)
0.050
0.050
0.005
ND
ND
ND
SS-
-00259
Test Method:
(1)
(2)
(3)
(4)
With reference to IEC 62321:2008(Section 8/9/10) Determination of Cadmium by ICP-OES.
With reference to IEC 62321:2008(Section 8/9/10) Determination of Lead by ICP-OES.
With reference to IEC 62321:2008(Section 7) Determination of Mercury by ICP-OES.
With reference to IEC 62321:2008(Annex C) Determination of Hexavalent Chromium by Colorimetric
Method using UV-Vis.
(5) With reference to IEC 62321:2008(Annex A) Determination of PBBs and PBDEs by GC-MS.
Test Item(s):
Cadmium(Cd)
Lead (Pb)
Mercury (Hg)
Hexavalent Chromium (Cr(VI))
Sum of PBBs
Monobromobiphenyl
Dibromobiphenyl
Tribromobiphenyl
Tetrabromobiphenyl
Pentabromobiphenyl
Hexabromobiphenyl
Heptabromobiphenyl
Octabromobiphenyl
Nonabromobiphenyl
Unit
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
MDL
2
2
2
2
5
5
5
5
5
5
5
5
5
001
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Test Report
No. CANEC1305830001
Decabromobiphenyl
Sum of PBDEs
Monobromodiphenyl ether
Dibromodiphenyl ether
Tribromodiphenyl ether
Tetrabromodiphenyl ether
Pentabromodiphenyl ether
Hexabromodiphenyl ether
Heptabromodiphenyl ether
Octabromodiphenyl ether
Nonabromodiphenyl ether
Decabromodiphenyl ether
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Date: 08 May 2013
5
5
5
5
5
5
5
5
5
5
5
Page 4 of 26
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Hexabromocyclododecane (HBCDD)
Test method: Determination of HBCDD by GC-MS based EPA 3550C:2007.
Test Item(s):
Hexabromocyclododecane (HBCDD)
Unit
mg/kg
MDL
10
001
ND
Note:
(1) Reference Information: Directive 2011/65/EU recasting RoHS directive 2002/95/EC:
Hexabromocyclododecane (HBCDD) is considered as a priority for risk evaluation and substance restriction.
Phthalates
Test Method: Determination of phthalates by GC-MS based on EN 14372:2004.
Test Item(s):
Dibutyl phthalate (DBP)
Butyl benzyl phthalate (BBP)
Bis (2-ethylhexyl) phthalate (DEHP)
Unit
MDL
001
%(w/w)
%(w/w)
%(w/w)
0.003
0.003
0.003
ND
ND
ND
Note:
(1) Reference Information: Directive 2011/65/EU recasting RoHS directive 2002/95/EC:
Bis (2-ethylhexyl) phthalate (DEHP), Butyl benzyl phthalate (BBP) and Dibutyl phthalate (DBP) are considered
as a priority for risk evaluation and substance restriction.
Test Report
No. CANEC1305830001
Date: 08 May 2013
Page 5 of 26
Polychlorinated Biphenyls (PCBs)
Test Method: With reference to US EPA Method 8082A:2007, analysis was performed by GC-MS.
Test Item(s):
2.4.4’-Trichlorobiphenyl (PCB 28)
2.2’.5.5’-Tetrachloro-biphenyl (PCB 52)
2.2’.4.5.5’-Pentachloro-biphenyl (PCB 101)
2.3’.4.4’.5-Pentachlorobiphenyl (PCB 118)
2.2’3.4.4’.5’-Hexachloro-biphenyl (PCB 138)
2.2’.4.4’.5.5’-Hexachloro-biphenyl (PCB 153)
2.2’.3.4.4’.5.5’- Heptachlorobiphenyl (PCB 180)
CAS No.
7012-37-5
35693-99-3
37680-73-2
31508-00-6
35065-28-2
35065-27-1
35065-29-3
Unit
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
MDL
0.5
0.5
0.5
0.5
0.5
0.5
0.5
001
ND
ND
ND
ND
ND
ND
ND
Polychlorinated Naphthalenes (PCNs)
Test Method: With reference to US EPA Method 8081B:2007, analysis was performed by GC-MS.
Test Item(s):
1-Chlorinated Naphthalene
2-Chlorinated Naphthalene
1,4-Dichlorinated Naphthalene
1,5-Dichlorinated Naphthalene
1,2-Dichlorinated Naphthalene
1,8-Dichlorinated Naphthalene
1,2,3-Trichlorinated Naphthalene
1,2,3,4-Tetrachlorinated Naphthalene
1,2,3,4,6-Pentachlorinated Naphthalene
Octa-chlorinaed Naphthalene
Unit
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
MDL
5
5
5
5
5
5
5
5
5
5
001
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Test Report
No. CANEC1305830001
Date: 08 May 2013
Page 6 of 26
Polychlorinated Terphenyls (PCTs)
Test Method: With reference to US EPA Method 8082A:2007, analysis was performed by GC-ECD/MS.
Test Item(s):
Aroclor5432
Aroclor5442
Aroclor5460
Unit
mg/kg
mg/kg
mg/kg
MDL
5
5
5
001
ND
ND
ND
Note:
(1) PCTs Reference Information: Entry 1 of Regulation (EC) No 552/2009 amending Annex XVII of REACH
Regulation (EC) No 1907/2006 (previously restricted under Directive 89/677/EC)
Shall not be placed on the market, or used:
— as substances,
— In mixtures, including waste oils, or in equipment, in concentrations greater than 50 mg/kg (0,005 % by
weight).
Please refer to Regulation (EC) No 552/2009 to get more detail information.
SCCP (Short chained chlorinated paraffins)
Test Method: With reference to US EPA 3550C:2007, analysis was performed by GC-ECD.
Test Item(s)
Short Chained Chlorinated Paraffins
(C10-C13)
Unit
MDL
001
mg/kg
50
ND
Organic-Tin compounds
Test Method: With reference to ISO 17353:2004, analysis was performed by GC-MS.
Test Item(s):
Dibutyltin (DBT)
Tributyltin (TBT)
Triphenyltin (TPhT)
Dioctyltin (DOT)
Unit
mg/kg
mg/kg
mg/kg
mg/kg
MDL
0.02
0.02
0.02
0.02
001
ND
ND
ND
ND
PFOS (Perfluorooctane sulfonates)
Test Method: With reference to US EPA Method 3550C:2007, analysis was performed by LC-MS.
Test Item(s)
Perfluorooctane sulfonates (PFOS)
PFOS – Acid
PFOS – Metal Salt
PFOS – Amide
Unit
MDL
001
mg/kg
10
ND
Test Report
No. CANEC1305830001
Date: 08 May 2013
Page 7 of 26
For reference: commission regulation (EU) No 757/2010 amending regulation (EC) No 850/2004:
(1) For the purposes of this entry, Article 4(1) (b) shall apply to concentrations of PFOS equal to or below 10 mg/kg
(0,001 % by weight) when it occurs in substances or in preparations.
(2) For the purposes of this entry, Article 4(1) (b) shall apply to concentrations of PFOS in semi-finished products or
articles, or parts thereof, if the concentration of PFOS is lower than 0,1 % by weight calculated with reference to the
mass of structurally or micro-structurally distinct parts that contain PFOS or, for textiles or other coated materials, if the
amount of PFOS is lower than 1µg /m 2 of the coated material.
Benzotriazole UV absorbent
Test Method: With reference to US EPA Method 3550C:2007, analysis was performed by GC-MS.
Test Item(s):
2-(3,5-Di-tert-butyl-2-hydroxyphenyl)
benzotriazole(UV-320)
CAS No.
3846-71-7
Unit
mg/kg
MDL
5
001
ND
Commission Decision 2011/135/EU (previously restricted under 2010/153/EU and 2009/251/EC) –
Dimethyl fumarate(DMF)
Test Method: SGS Inhouse method (GZTC CHEM-TOP-095), analysis was performed by GC-MS.
Test Item(s):
Recommended
Max. Limit
Unit
MDL
001
0.1
mg/kg
0.1
ND
-
-
-
PASS
Dimethyl fumarate(DMF)
Conclusion
Note:
(1) The maximum permissible limit is quoted from the document EU Directive 2011/135/EU (previously restricted under
2010/153/EU and 2009/251/EC)
Phthalates Content
Test Method: With reference to EN 14372:2004, analysis was performed by GC-MS.
Test Item(s):
Dibutyl Phthalate (DBP) Content
Benzylbutyl Phthalate (BBP) Content
Bis-(2-ethylhexyl) Phthalate (DEHP) Content
Diisononyl Phthalate (DINP) Content
Di-n-octyl Phthalate (DNOP) Content
Diisodecyl Phthalate (DIDP) Content
Unit
%(w/w)
%(w/w)
%(w/w)
%(w/w)
%(w/w)
%(w/w)
MDL
0.003
0.003
0.003
0.010
0.003
0.010
001
ND
ND
ND
ND
ND
ND
Test Report
No. CANEC1305830001
Diisobutyl Phthalate (DIBP) Content
Di-n-hexyl Phthalate (DnHP) Content
1,2-Benzenedicarboxylic acid, di-C6-8branched alkyl esters, C7-rich (DIHP) Content
1,2-Benzenedicarboxylic acid, di-C7-11branched and linear alkyl esters (DHNUP)
Content
Di-methoxyethyl Phthalate (DMEP) Content
Diisopentyl Phthalate(DIPP) Content
n-pentyl-Isopentyl Phthalate(nPiPP) Content
1,2-Benzenedicarboxylic acid, dipentyl ester,
branched and linear(C5-PHTH)
Notes:
Date: 08 May 2013
%(w/w)
%(w/w)
0.003
0.003
ND
ND
%(w/w)
0.010
ND
%(w/w)
0.010
ND
%(w/w)
%(w/w)
%(w/w)
0.003
0.003
0.003
ND
ND
ND
%(w/w)
0.010
ND
Page 8 of 26
(1) C5-PHTH=DPP+DIPP+nPiPP
Polyvinyl chloride (PVC)
Test Method: SGS in house method (GZTC CHEM-TOP-066), analysis was performed by FTIR.
Test Item(s):
Polyvinyl chloride (PVC)
CAS No.
9002-86-2
001
Negative
Note:
(1) Negative = Undetectable, Positive = Detectable.
Ozone Depleting Substances (ODS)
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
Test Item(s)
CFC
CFC-11
CFC-12
CFC-13
CFC-111
CFC-112
CFC-112
CFC-113
CFC-113
CFC-114
CFC-114
CFC-115
CFC-211
CFC-212
CFC-213
CFC-214
CFC-215
CFC-215
CAS No.
75-69-4
75-71-8
75-72-9
354-56-3
76-11-9
76-12-0
354-58-5
76-13-1
374-07-2
76-14-2
76-15-3
422-78-6
661-96-1
1652-89-7
677-68-9
1599-41-3
76-17-5
Unit
-
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Test Method (Reference)
-
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
Result
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
MDL
-
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
Test Report
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
CFC-216
CFC-216
CFC-217
HCFC
HCFC-21
HCFC-22
HCFC-31
HCFC-121
HCFC-122
HCFC-123
HCFC-123a
HCFC-124
HCFC-124a
HCFC-131
HCFC-131a
HCFC-132a
HCFC-132b
HCFC-133a
HCFC-141b
HCFC-142b
HCFC-221
HCFC-222
HCFC-223
HCFC-225ca
HCFC-225cb
HCFC-226
HCFC-231
HCFC-232
HCFC-233
HCFC-234
HCFC-235
HCFC-241
HCFC-242
HCFC-243
HCFC-244
HCFC-251
HCFC-252
HCFC-253
HCFC-261
HCFC-261
HCFC-271
HCFC-262
HCFC-262
HBFC
CHF2Br
CH 2FBr
C 2HFBr4
C2HF2Br3
C2HF3Br2
C 2HF4Br
No. CANEC1305830001
661-97-2
1652-80-8
422-86-6
CAS No.
75-43-4
75-45-6
593-70-4
354-14-3
354-21-2
306-83-2
354-23-4
2837-89-0
354-25-6
359-28-4
811-95-0
471-43-2
1649-08-7
75-88-7
1717-00-6
75-68-3
422-26-4
422-30-0
422-52-6
422-56-0
507-55-1
431-87-8
421-94-3
460-89-9
7125-84-0
425-94-5
460-92-4
666-27-3
460-63-9
338-75-0
679-85-6
421-41-0
819-00-1
460-35-5
7799-56-6
420-97-3
430-55-7
102738-79-4
420-99-5
CAS No.
1511-62-2
373-52-4
354-04-1
-
mg/kg
mg/kg
mg/kg
-
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
-
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Date: 08 May 2013
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
-
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
-
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
Page 9 of 26
N.D.
N.D.
N.D.
-
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
-
0.1
0.1
0.1
0.1
0.1
0.1
Test Report
66
67
68
69
70
71
72
73
74
75
76
77
78
79
80
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
98
99
100
101
102
103
104
105
106
107
108
109
110
111
112
C2H 2FBr3
C2H2F2Br2
C2H 2F3Br
C2H 3FBr2
C2H 3F2Br
C 2H4FBr
C 3HFBr6
C3HF2Br5
C3HF3Br4
C3HF4Br3
C3HF5Br2
C 3HF6Br
C3H 2FBr5
C3H2F2Br4
C3H2F3Br3
C3H2F4Br2
C3H 2F5Br
C3H 3FBr4
C3H3F2Br3
C3H3F3Br2
C3H 3F4Br
C3H 4FBr3
C3H4F2Br2
C3H 4F3Br
C3H 5FBr2
C3H 5F2Br
C 3H6FBr
HALON
Halon 1211
Halon 1301
Halon 2402
OTHERS
Dibromofluoromethane
Methyl bromide
Bromochloromethane
HFC
HFC-23
HFC-32
HFC-41
HFC-43-10mee
HFC-125
HFC-134
HFC-134a
HFC-152a
HFC-143
HFC-143a
HFC-227ea
HFC-236 cb
HFC-236ea
HFC-236fa
No. CANEC1305830001
75-82-1
421-06-7
359-07-9
762-49-2
CAS No.
353-59-3
75-63-8
124-73-2
CAS No.
1868-53-7
74-83-9
74-97-5
CAS No.
75-46-7
75-10-5
593-53-3
354-33-6
359-35-3.
811-97-2
75-37-6
420-46-2
430-66-0
431-63-0
690-39-1
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
-
mg/kg
mg/kg
mg/kg
-
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Date: 08 May 2013
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
-
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
-
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
Page 10 of 26
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
-
N.D.
N.D.
N.D.
-
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
-
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
Test Report
113
114
115
116
117
118
119
120
121
122
123
124
125
126
127
128
129
130
131
132
133
134
135
136
137
138
139
140
141
142
143
144
145
146
HFC-245ca
HFC-245fa
HFC-365mfc
PFC
Perfluoromethane
Perfluoroethane
Perfluoropropane
Perfluorobutane
Perfluoropentane
Perfluorohexane
Perfluorocyclobutane
CHC
1,3-dichloropropane
2,2-dichloropropane
Carbon tetrachloride
Chloroethane
Chloroform
Chloromethane
Cis-1,2-dichloroethene
Cis-1,3-dichloropropene
Hexachlorobutadiene
Methylene chloride
Tetrachloroethylene
Trans-1,2-dichloroethene
Trans-1,3dichloropropene
Trichloroethylene
1,1,1,2-tetrachloroethane
1,1,1-trichloroethane
1,1,2,2-tetrachloroethane
1,1,2-trichloroethane
1,1-dichloroethane
1,1-dichloroethene
1,1-dichloropropene
1,2,3-trichloropropane
1,2-dichloroethane
1,2-dichloropropane
Note:
1. N.D. = Not Detected (<MDL)
2. MDL = Method Detection Limit
No. CANEC1305830001
Date: 08 May 2013
Page 11 of 26
679-86-7
CAS No.
75-73-0
76-16-4
76-19-7
355-25-9
678-26-2
355-42-0
115-25-3
CAS No.
142-28-9
594-20-7
56-23-5
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
87-68-3
75-09-2
127-18-4
156-60-5
mg/kg
mg/kg
mg/kg
-
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
-
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
-
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
-
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
N.D.
N.D.
N.D.
-
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
-
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
0.1
0.1
0.1
-
0.1
0.1
0.1
0.1
0.1
0.1
0.1
-
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
10061-02-6
mg/kg
EPA 5021A:2003, HS-GC-MS
N.D.
0.1
79-01-6
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
96-18-4
107-06-2
78-87-5
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
EPA 5021A:2003, HS-GC-MS
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
Test Report
No. CANEC1305830001
Date: 08 May 2013
Page 12 of 26
Formaldehyde
Test Method: With reference to ISO 17226-1:2008, analysis was preformed by HPLC-DAD.
Test Item(s):
Formaldehyde
Unit
mg/kg
MDL
16
001
ND
Halogen
Test Method: With reference to EN 14582:2007, analysis was performed by IC.
Test Item(s):
Chlorine (Cl)
Unit
mg/kg
MDL
50
001
ND
Bromine (Br)
mg/kg
50
ND
Asbestos
Test Method: With reference to NIOSH 9000:1994& NIOSH 9002:1994, analysis was performed by XRD&PLM.
Test Item (s)
Chrysotile
Amosite
Crocidolite
Anthophyllite
Tremolite
Actinolite
CAS NO
012001-29-5
012172-73-5
012001-28-4
077536-67-5
077536-68-6
077536-66-4
Note:
(1) Negative < 0.1%(w/w), Positive ≥0.1%(w/w)
Unit
%(w/w)
%(w/w)
%(w/w)
%(w/w)
%(w/w)
%(w/w)
MDL
0.1
0.1
0.1
0.1
0.1
0.1
001
Negative
Negative
Negative
Negative
Negative
Negative
Test Report
No. CANEC1305830001
Date: 08 May 2013
Page 13 of 26
Azo Dyes
Test Method:
Textile:
According to BS EN 14362-1:2012 – Analysis was conducted with GC-MS/HPLC-DAD.
Determination of 4-aminoazobenzene (CAS No.:60-09-3) –EN14362-3:2012; with the use of Gas
Chromatography – Mass Spectrometry (GC-MS)
Test Item(s)
4-Aminobiphenyl
Benzidine
4-Chlor-o-toluidine
2-Naphthylamine
o-Aminoazotoluene
5-nitro-o-toluidine /
2-Amino-4-nitrotoluene
4-Chloroaniline
4-methoxy-m-phenylenediamine
/2,4-Diaminoanisole
4,4'-Diaminodiphenylmethane
3,3'-Dichlorobenzidine
3,3'-Dimethoxybenzidine
3,3'-Dimethybenzidine
4,4'-methylenedi-o-toluidine /
3,3'-Dimethyl-4,4'-diaminodiphenyl
methane
p-Cresidine
4,4'-Methylene-bis-(2-chloroaniline)
4,4'-Oxydianiline
4,4'-Thiodianiline
o-Toluidine
4-methyl-m-phenylenediamine /
2,4-Toluylendiamine
2,4,5-Trimethylaniline
4-aminoazobenzene
O-Anisidine
2,4-Xylidine
2,6-Xylidine
CAS No.
Unit
MDL
001
92-67-1
92-87-5
95-69-2
91-59-8
97-56-3
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
5
5
5
5
5
ND
ND
ND
ND
ND
99-55-8
mg/kg
5
ND
106-47-8
mg/kg
5
ND
615-05-4
mg/kg
5
ND
101-77-9
91-94-1
119-90-4
119-93-7
mg/kg
mg/kg
mg/kg
mg/kg
5
5
5
5
ND
ND
ND
ND
838-88-0
mg/kg
5
ND
120-71-8
101-14-4
101-80-4
139-65-1
95-53-4
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
5
5
5
5
5
ND
ND
ND
ND
ND
95-80-7
mg/kg
5
ND
137-17-7
60-09-3
90-04-0
95-68-1
87-62-7
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
5
5
5
5
5
ND
ND
ND
ND
ND
Notes :
(1)The BS EN 14362-1/2 and ISO 17234-1 methods will enable further cleavage of 4-aminoazobenzene to
non-forbidden amines: aniline and 1,4-phenylenediamine, therefore, the test method of § 64 LFGB, BVL, B
82.02.9 was employed to verify the presence of 4-aminoazobenzene.
Test Report
No. CANEC1305830001
Date: 08 May 2013
Page 14 of 26
Tris(2-chloroethyl) phosphate
Test Method: With reference to EN71-11, analysis was performed by LC-MS.
Test Item(s)
Tris(2-chloroethyl) phosphate
Unit
MDL
001
mg/kg
5.0
ND
Element(s)
Test Method: With reference to US EPA Method 3052:1996, analysis was performed by ICP-OES.
Unit
mg/kg
Test Item(s):
Beryllium (Be)
MDL
001
5
ND
Beryllium oxide (BeO)
Test Method: With reference to US EPA Method 3052:1996, analysis was performed by ICP-OES.
Test Item(s):
Beryllium oxide (BeO) ◆
Unit
mg/kg
MDL
15
001
ND
Note:
(1) ◆BeO: Calculate from Beryllium content
CoCl2 (Cobalt dichloride)
Test Method: With reference to SGS In House Method(GZRD-R&D-TOP-104) & EPA 3052:1996, analysis was
performed by IC & ICP-OES.
Test Item(s):
CoCl2
Note:
Unit
mg/kg
MDL
100
001
ND
CoCl2: Result is calculated based on the results of Cobalt and Chloride contents.
Test Report
No. CANEC1305830001
Date: 08 May 2013
Page 15 of 26
Perchlorate
Test Method: With reference to SGS In-house method (GZTC-R&D-TOP-287), analysis was performed by LC-MSMS.
Test Item(s)
Perchlorate
Unit
µg/kg
MDL
5
001
ND
Test Report
No. CANEC1305830001
Date: 08 May 2013
ATTACHMENTS
SVHC Testing Flow Chart
1) Name of the person who made testing: Michael Tso / Liu Qiong
2) Name of the person in charge of testing: Adams Yu / Yolanda Wei
Sample cutting/preparation
Sample measurement
Sample Pretreatment
Instrumental Analysis
DATA
Page 16 of 26
Test Report
No. CANEC1305830001
Date: 08 May 2013
Page 17 of 26
ATTACHMENTS
RoHS Testing Flow Chart
1) Name of the person who made testing: Michael Tso / Cutey Yu
2) Name of the person in charge of testing: Adams Yu / Yolanda Wei
3) These samples were dissolved totally by pre-conditioning method according to below flow chart
(Cr6+ and PBBs/PBDEs test method excluded).
Sample Preparation
Sample Measurement
Pb/Cd/Hg
Acid digestion with
microwave/ hotplate
Sample solvent
extraction
Filtration
Concentration/
Dilution of extraction
solution
Solution
Residue
Filtration
1) Alkali Fusion /
Dry Ashing
2) Acid to
dissolve
ICP-OES/AAS
DATA
Cr6+
PBBs/PBDEs
GC-MS
DATA
Nonmetallic
material
Adding digestion
reagent
Heating to
90~95℃ for
extraction
Filtration and
pH adjustment
Adding 1,5diphenylcarbazide
for color
development
Metallic
material
Positive
Spot test
Negative
Boiling water
extraction
Adding 1,5diphenylcarbazide
for color
development
UV-Vis
A red color
indicates the
presence of Cr6+. If
necessary, confirm
with UV-Vis.
DATA
DATA
Test Report
No. CANEC1305830001
ATTACHMENTS
HBCDD Testing Flow Chart
1) Name of the person who made testing: Cutey Yu
2) Name of the person in charge of testing: Yolanda Wei
Sample cutting / preparation
Sample Measurement
Solvent extraction
Concentration/Dilution
Filtration
GC-MS
DATA
Date: 08 May 2013
Page 18 of 26
Test Report
No. CANEC1305830001
ATTACHMENTS
Phthalates Testing Flow Chart
1) Name of the person who made testing: Liu Qiong
2) Name of the person in charge of testing: Yolanda Wei
Sample cutting / preparation
Sample Measurement
Solvent extraction
Concentration/Dilution
Filtration
GC-MS
DATA
Date: 08 May 2013
Page 19 of 26
Test Report
No. CANEC1305830001
ATTACHMENTS
SCCP/MCCP Testing Flow Chart
1) Name of the person who made testing: Liu Qiong
2) Name of the person in charge of testing: Yolanda Wei
Sample cutting / preparation
Sample Measurement
Solvent extraction
Concentration
Clean-Up
Filtration
GC-ECD
DATA
Date: 08 May 2013
Page 20 of 26
Test Report
No. CANEC1305830001
Date: 08 May 2013
ATTACHMENTS
PFOA / PFOS Testing Flow Chart
1) Name of the person who made testing: Tina Zhao
2) Name of the person in charge of testing: Yolanda Wei
Sample cutting / preparation
Sample Measurement
Solvent extraction
Concentration/Dilution
Filtration
LC-MS
DATA
Page 21 of 26
Test Report
No. CANEC1305830001
ATTACHMENTS
Dimethyl Fumarate Testing
Testing Flow Chart
1) Name of the person who made testing: Liu Qiong
2) Name of the person in charge of testing: Yolanda Wei
Sample cutting / preparation
Sample Measurement
Solvent extraction
Concentration/Dilution
Filtration
GC-MS
DATA
Date: 08 May 2013
Page 22 of 26
Test Report
No. CANEC1305830001
ATTACHMENTS
PVC Testing Flow Chart
1) Name of the person who made testing: Cutey Yu
2) Name of the person in charge of testing: Yolanda Wei
Sample cutting/preparation
FTIR
Check wave-number of C-Cl bonding
DATA
Date: 08 May 2013
Page 23 of 26
Test Report
ATTACHMENTS
No. CANEC1305830001
Date: 08 May 2013
Halogen Testing Flow Chart
1) Name of the person who made testing: Bella Wang
2) Name of the person in charge of testing: Adams Yu
Sample cutting / preparation
Sample Measurement
Combustion in oxygen bomb
Dissolved in an absorption solution
Filtration
Analyzed by ion chromatography. Double confirm by other
instruments, if necessary
DATA
Page 24 of 26
Test Report
ATTACHMENTS
No. CANEC1305830001
Elementary Testing Flow Chart
1) Name of the person who made testing: Bella Wang
2) Name of the person in charge of testing: Adams Yu
Sample cutting / preparation
Sample Measurement
Acid digestion
Filtration
Solution
ICP-OES/AAS
DATA
Date: 08 May 2013
Page 25 of 26
Test Report
No. CANEC1305830001
Date: 08 May 2013
Sample photo :
CANEC1305830001
CANEC1305830001
CAN13-058300.001
SGS authenticate the photo on original report only
*** End of Report ***
Page 26 of 26