Assessment of Coatings for Friction-Type Connections Mohamed Anzar1, Howard Morris1, and Thomas Smith1 1 Roads and Traffic Authority of NSW Abstract Friction-type connections are widely used to connect steel members where slipping is not permitted under serviceability loads. The friction developed between the faying surfaces transfers the design shear forces at the serviceability limit states. The bolts act in tension and are not subject to shear.As a rule, faying surfaces are coated with inorganic zinc silicate coatings and a slip factor for these coatings is specified in AS 5100.6. For other applied coatings and surface conditions, AS 5100.6 specifies testing in accordance with AS 4100 Appendix J.Epoxy zinc rich primers are generally not used for friction-type connections. This testing program was prompted when an epoxy zinc rich primer was proposed for friction-type connection during the course of a contract. Epoxy zinc rich primers have some operational advantages over zinc silicate primers and a testing program to assess the suitability of a range of zinc rich coatings for faying surfaces was initiated. Nine different zinc rich coatings and bare metal samples were tested in accordance with AS 4100 Appendix J and the results are presented in this paper. The effects of variations in bolt quality and the measures taken to modify the testing parameters to suit the bolts used for the test samples are discussed. The effects of coating dry film thickness (DFT) on the friction coefficient are also discussed. Introduction Faying surfaces of bolted connections must be either painted or galvanized to prevent crevice corrosion developing between surfaces in contact. For faying surfaces of painted members in friction-type bolted connections, current RTA QA Specification B220 specifies one coat of a zinc rich primer having dry film thickness of 75 microns and stipulates that the zinc paint coating applied to faying surfaces of friction-type connections designed to AS 4100 must have a minimum coefficient of friction of 0.35 measured according to AS 4100 Appendix J. V. Ponnampalam, H. Madrio and E. Ancich Sustainable Bridges: The Thread of Society AP-G90/11_096© ABC 2011 255 256 Mohamed Anzar, Howard Morris and Thomas Smith Inorganic zinc silicate primers have been used for steelwork and their use at friction-type connections has posed no real issue as AS 5100.6 specifies that the slip factor (µ) may also be taken as 0.35 for abrasive blast cleaned steel surfaces coated with zinc silicate coatings. If any other applied finish or surface condition, including a machined surface is desired, the slip factor needs to be evaluated based upon adequate test evidence. According to AS 5100.6, tests performed in accordance with the procedure specified in AS 4100 Appendix J are deemed to provide satisfactory test evidence. However, there has been an increasing trend over recent years for epoxy zinc rich (also known as organic zinc) primers to be used for the priming of new steelwork in lieu of inorganic zinc silicate primers. This is primarily the result of the generally superior curing and over-coating times associated with epoxy coatings compared to inorganic zinc silicate coatings particularly when ambient conditions are cool and dry. The greater ease of mixing and applying epoxy zinc primers is also understood to be a key reason for preferring epoxy zinc primers over inorganic zinc silicates, particularly for on-site works. For structures with friction-type connections, one option is to use an inorganic zinc silicate primer for all of the steelwork. Alternatively, an epoxy zinc primer can be used for all steelwork except at the faying surfaces of connections where an inorganic zinc silicate is used. If epoxy zinc rich primers can be satisfactorily used for the faying surfaces of friction-type connections, it will permit the use of one primer only throughout the structure making the painting work simpler and more efficient than having to use two primers. However, the slip-factors of the epoxy coatings need to be evaluated before using them for friction-type connections. At present, certain epoxy zinc coatings have been proposed for friction-type connections for RTA bridgeworks, on the basis of testing commissioned by coating manufacturers. Initially, it was thought that the epoxy zinc primers that are certified suitable for friction-type connections achieve this by virtue of high zinc content. However, there have been a number of instances over the years of coating failures on RTA bridges, involving delamination of topcoats as a result of cohesive failures through a zinc primer coating, where a zinc primer with high zinc content has been used for the repair of an inorganic zinc silicate primer coating or a thermal applied zinc coating. It is believed that the risk of such cohesive failures can be reduced by using zinc primers with a lower zinc content where to have a higher percentage of binder in the film. The friction characteristics of epoxy zinc primers with slightly lower zinc contents are of interest even though the lower zinc content product appeared less likely to satisfy the current slip-factor requirements of slip factor 0.35. Assessment of Coatings for Friction-Type Connections 257 Test Program As part of an RTA internal evaluation program, a testing program was initiated and three different products from each of three manufacturers were included. One inorganic zinc silicate product and two epoxy zinc rich coatings with low and high zinc contents were selected from each manufacturer for testing. RTA provided the steel coupons and manufacturers applied the coatings on the samples for testing under their supervision. The names of the manufacturers and products are considered commercial-in-confidence and not disclosed here. Five samples of each coating were tested. The total number of samples tested in this program was 50 comprising 5 samples each of 9 different coatings and 5 bare metal samples. Test Method Testing was conducted by the RTA Materials Technology Section, Auburn, to AS 4100 Appendix J: Standard Test for evaluation of slip factor. The test consists of bolting together a set of four painted plates as shown in Fig.1and Fig.2 then loading this setup in tension to induce a small amount of slip. 22 dia 12 22 dia 27 dia 25 23 dia 27 dia 23 dia 12 200 250 60 120 60 250 8 74 80 40 56 56 40 80 74 Fig. 1. Dimension of samples used The bolts compressing the plates were torqued to a range as described by the method. Four dial gauges as in Fig.3 were placed on the setup to indicate the plate movement (slip). The output of these gauges was recorded via a computer program. The setup was placed in a Universal Testing Machine and tension was 258 Mohamed Anzar, Howard Morris and Thomas Smith applied to induce slippage. The point at which the plates slipped is known as the slip load. Fig. 2. Assembled sample for testing Fig. 3. Sample mounted for testing Testing Details • Samples were blasted and painted by the respective manufacturers, prior to arriving at the laboratory with the coating type marked. • The only surface preparation carried out by the Auburn laboratory was on the bare steel samples which were washed with a liquid alkaline solution (Gamlen CA1) to remove traces of oils and greases that may have been present. Flaky mill-scale was not removed. • Samples were tightened by the laboratory by a pneumatic Norbar high–torque tool. • A specially made jig shown in Fig.4 was used to hold and align the samples while being tightened. • A Boltstress G5 Ultrasonic Direct Tension Monitor shown in Fig.5 was used to measure the tension induced in the bolt while it was tightened. A probe is placed on the end of the bolt and ultrasonic measurements are taken of the bolt elongation. This is then instantaneously converted to a tensile load via linear stress-strain calculations. Assessment of Coatings for Friction-Type Connections 259 • The Monitor is calibrated using a NATA certified jack and gauge combination with a sample bolt. Fig. 4. Jig used while tightening Fig. 5. Boltstress tension monitor • The M20 bolts used in the assembly required end preparation. The probe end (bolt head) required a suitably flat surface to allow transmittance of the vibrations. A high speed rotary tool was used to grind the surface. • The induced tension was measured by the monitor. • The induced tension in the supplied bolts is lower than the minimum proof load specified in AS5100.6. The AS 4100 Appendix J method states that the induced tension should be at least 80% but no more than 100% of the specified proof load. It was found with these particular bolts, non-recoverable elongation was occurring before the minimum proof load specified in AS 5100.6 for M20 bolts was achieved. The bolt tension induced for the series of tests was reduced to 120kN to be within the elastic limit while being more than 80% of the specified proof load. • Tensile load was applied to the bolted sample stepwise at a rate of 20kN/min. The sample was tensioned at this rate for 30 seconds, then held at the load achieved for a further 30 seconds to allow for any creep to cease (i.e. effectively loading the sample 10kN in total per minute). This cycle was repeated until slip of plates occurred. Test Results Dry Film Thickness (DFT) readings of the coated samples were taken at twenty four locations comprising 4 readings on each face in contact before assembly around the bolt holes of contact surfaces. The mean value of these 24 readings was taken as the representative DFT reading of the sample and the slip factor was compared to it. 260 Mohamed Anzar, Howard Morris and Thomas Smith The failure mode refers to the way (speed and noise) in which the samples failed, i.e. the slipping of the painted plate surfaces. Sample graphs of a slow slip and fast slip are provided in Fig.7 and Fig.8, respectively. Samples that underwent a slow failure, required the slip load to be defined at a corresponding slip of 0.13mm (refer to AS 4100 Appendix J). For those that failed suddenly, the slip load was easily distinguishable. Fig. 7. Loading graph for a slow slip test Fig. 8. Loading graph for a sudden slip test Test results for bare metal samples are given in Table.1. The coated samples were also tested and results were calculated. The results obtained for samples of bare metal and 9 coatings are summarized in Table.2. Assessment of Coatings for Friction-Type Connections 261 Table I. Test results for bare steel samples Sample Bolt Tension (T) Measured Slip Load (P) kN kN Slip Factor (=(P/2)/T) BS-1a 120.8 84.1 0.35 BS-1b 122.0 84.1 0.34 BS-2a 124.3 72.8 0.29 BS-2b 122.8 72.8 0.30 BS-3a 119.9 63.2 0.26 BS-3b 121.9 63.2 0.26 BS-4a 120.6 112.4 0.47 BS-4b 121.7 112.4 0.46 BS-5a 123.2 59.7 0.24 BS-5b 121.3 59.7 0.25 Average slip factor 0.32 Minimum slip factor 0.24 Calculated slip factor as per AS 4100 Appendix J for five samples 0.17 The slip factor to be used in design as per AS 4100 Appendix J 0.24 (Higher of above two values) Table II. Summary test results for bare steel and coated samples Type BS Slip Factor Nature of slip Maximum Minimum Average Calculated Design 0.47 0.24 0.32 0.17 0.24 Loud, sudden Inorganic zinc silicate A1 0.59 0.37 0.53 0.36 0.37 Loud, sudden B1 0.50 0.38 0.44 0.36 0.38 Loud, sudden C1 0.56 0.48 0.52 0.42 0.48 Loud, sudden Epoxy zinc rich coatings (high zinc content) A2 0.41 0.26 0.34 0.21 0.26 Loud, sudden B2 0.40 0.28 0.35 0.25 0.28 No audible, slow C2 0.36 0.26 0.31 0.23 0.26 No audible, slow Epoxy zinc rich coatings (low zinc content) A3 0.58 0.31 0.45 0.30 0.31 No audible, slow B3 0.23 0.11 0.17 0.10 0.11 Not loud, sudden C3* 0.20 0.14 0.16 0.11 0.14 No audible, slow *The sample C3 originally had 5 samples but one of the test results could not be captured. Therefore, the calculated result for this coating type was based on 4 test samples and the statistical factor for 3 samples was used to calculate the design value for this coating shown in Table.II. 262 Mohamed Anzar, Howard Morris and Thomas Smith 160 DFT Reading 140 DFT(microns) 120 100 80 60 Inorganic zinc 40 Bare Steel 20 Epoxy low Zn Epoxy high Zn 0 0 5 10 15 20 25 30 35 40 45 50 Sample Number Fig. 9. DFT Readings of Coated Samples Fig. 9 shows the mean DFT readings from 24 readings for each sample included in the testing program. Samples 1 to five are bare steel samples with no DFT readings involved. Each set of five samples between two vertical lines represent different coatings. Samples 6 to 20 are coated with inorganic zinc silicate coatings and 21 to 50 are coated with epoxy zinc rich coatings. Coatings 21 to 35 have high zinc contents and coatings 36 to 50 have low zinc contents. 0.7 Slip Factor 0.6 Slip Factor 0.5 0.4 0.3 Epoxy low Zn 0.2 Inorganic zinc Bare Steel 0.1 Epoxy high Zn 0.0 0 5 10 15 20 25 30 35 40 45 50 Sample Number Fig. 10. Slip Factors of Coated Samples Fig.10 shows the slip factors obtained based on slip load for each sample. The test samples have two bolted connections and two very close slip factors for each sample. The average of these two values is shown against each sample number in Fig.10. The sample numbers in Fig.9 and Fig.10 correspond to identical samples. Assessment of Coatings for Friction-Type Connections 263 The comparison of slip factors obtained for Samples 7, 17 and 37 and their DFT readings in relation to other samples in their respective coating types between vertical lines indicates that the slip factors do not appear to be influenced by the variation in average DFT readings for the range of DFT thicknesses involved. The design slip factor of 0.24 obtained for bare metal surfaces is less than the value of 0.35 allowed by AS 5100.6. The slip factors for three out of five samples were below 0.3 and were highly variable. The low values obtained cannot be attributed to surface preparation which did not include blast cleaning as a previous similar RTA testing program included three bare metal samples of blast cleaned surfaces also showed lower than the AS 5100.6 design slip factor of 0.35. This indicates that caution should be exercised before using 0.35 for bare metal surfaces in design. Slip factors obtained for three inorganic zinc silicate coatings represented by samples 6 to 20 in Fig.10 satisfy the slip factor 0.35 allowed in AS 5100.6. The slip factors for epoxy zinc rich samples, numbers 21 to 50, are highly variable. For manufacturers B and C, higher zinc content values gave greater slip factors than lower zinc content values. For manufacturer A, the opposite is the case. From these results, no general rule can be drawn regarding slip factor versus zinc content. Comparison of Australian and RCSC Approaches This project to assess the slip factors of coatings was initiated after a number of paint manufacturers produced test certificates for various epoxy zinc rich coatings indicating slip factors of the order of 0.50 when tested according to Specification for Structural Joints Using ASTM A325 or A490 Bolt[3]. This specification is issued by the United States based, Research Council for Structural Connections (RCSC). The slip factor values reported are high compared to the values prescribed in AS 5100.6. The key difference is that the RCSC approach utilizes mean values of slip factor whereas the AS 5100.6 approach uses minimum values with a statistical adjustment. AS 5100.6 specifies a factor kh for different type holes taking 1.0 for standard holes, 0.85 for short slotted and oversize holes and 0.70 for long slotted holes. The RCSC specification also specifies similar factors in its equations deviating slightly only for long slotted holes. A case of a single bolt connection with single sliding surface and a standard hole is used for comparison of the approaches and discussion below. 264 Mohamed Anzar, Howard Morris and Thomas Smith RCSC Approach Specification for Structural Joints Using High-Strength Bolts[4] or its predecessor Specification for Structural Joints Using ASTM A325 or A490 Bolts[3] is used for testing slip coefficients. This specification defines faying surfaces into three different classes, Class A, B or C and specifies applicable different mean slip coefficients as follows. 0.33 for Class A faying surfaces (uncoated clean mill-scale steel surfaces or surfaces with Class A coatings on blast-cleaned steel); 0.50 for Class B surfaces (uncoated blast-cleaned steel surfaces or surfaces with Class B coatings on blast-cleaned steel); and 0.35 for Class C surfaces (roughened hot-dip galvanized surfaces). The RCSC specification uses mean slip coefficient obtained from five individual tests and specifies equations based on mean coefficient. The tests conducted according to the specification use samples with a single bolt connection. The RCSC specification specifies equations for design slip resistance at the factored-load level and at the service load level. According to the commentary, these equations are calibrated to produce essentially the same results. The factored load equation to calculate the slip resistance for a single bolt connection with single sliding interface subjected to shear only becomes as below: Rn = μDuTm where Tm is the specified minimum bolt pretension and Du is a multiplier used to convert the specified minimum tension to the mean tension in the bolt with a specified default value of 1.13. The equation for the same situation at the service-load level is as follows: Rn = μDTm where D is a slip probability factor with the default value of 0.80 that reflects the distribution of actual slip coefficient values about the mean installed pretension to the specified minimum bolt pretension Tm and slip probability level. The RCSC uses the average slip factor obtained from 5 tests and effectively increases the specified minimum tension by 1.13 to derive the average pretension in the bolts for factored load level designs. The slip resistance ratio obtained between factored load case and service load case given by the ratio of the above two equations becomes Du/D = 1.13/0.80 = 1.41, using the default values specified in the specification. The calibration of equations may have aimed for this ratio. Assessment of Coatings for Friction-Type Connections 265 Australian approach The design shear capacity for a single bolt connection with single sliding interface subjected to shear only becomes: φVsf = φμNti Nti is equal to Tm in RCSC. However, μ is evaluated according to AS 4100 Appendix J and is a minimum value and not a mean value as discussed above. The design shear capacity φVsf for bolt serviceability limit state is thus obtained by multiplying nominal shear capacity Vsf of a bolt by the capacity factor φ = 0.70 in AS 5100.6. The sample as per AS 4100 Appendix J has 2 bolted connections in each sample giving two slip factors from each test. AS 4100 calculates the minimum possible slip factor with 90% confidence level based on the test results obtained and uses a factor of 0.90 or 0.85 depending on the number of samples to include effects of small sample size used in the tests for evaluating the slip factor. The factor calculated in this way is then used with the minimum tension specified as above. AS 5100.6 specifies slip factor µ = 0.35 for clean steel surfaces and abrasive blast cleaned steel surfaces coated with zinc silicate (inorganic) coatings. Discussion of RCSC and Australian approaches A comparison of the two approaches can be illustrated by considering the serviceability resistances determined according to these methods for the following example. For a friction-type connection comprising uncoated blast-cleaned steel surfaces, RCSC specifies a slip factor, μRCSC of 0.50 whilst AS 5100.6 specifies a slip factor, μAS of 0.35. AS 5100.6 specifies a capacity reduction factor φ = 0.70. RCSC does not specify a corresponding reduction. The RCSC slip resistance for service-load level, Rn=μ RCSC DTm. The AS 5100.6 serviceability limit state design shear capacity, φVsf = φμ AS Nti. Noting that D = 0.80 from above and that Tm and Nti are the minimum specified bolt tensions and are equal, the ratio of the RCSC slip resistance to the AS 5100.6 design shear capacity equals, μ RCSC D / φμ AS = 0.50*0.80/(0.70*0.35) =1.63. 266 Mohamed Anzar, Howard Morris and Thomas Smith Thus, the RCSC’s value is about 63% more than the AS 5100.6 design shear capacity. Conversely, the AS 5100.6 design shear capacity is approximately 61% of the RCSC slip resistance. If a φ value of 1.0 were used instead of 0.7 in AS 5100.6 to calculate the design shear capacity, then the above values of 63% and 61% become 14% and 88% respectively. Thus even without a capacity reduction factor, AS 5100.6 gives conservative values compared to the RCSC approach. Conclusion Nine different zinc rich coatings from three manufacturers and bare metal samples were tested in accordance with AS 4100 Appendix J and the results are presented. A slip factor of 0.35 or more was obtained for inorganic zinc silicate surfaces and this validates the values specified in AS 5100.6. No firm conclusion can be reached on the effects of high zinc content on slip factors in view of the limited number of samples tested. However, the slip factors for high zinc content epoxy coatings were found to be less variable than those for low zinc content epoxy coatings. The design factor of 0.24 was obtained for bare metal samples instead of 0.35 specified in AS 5100.6. The values from the testing are appeared to be closer to the values expected for samples made with uncoated clean mill-scale steel surfaces. Further studies are required to ascertain the reason for lower value than specified including the effect of surface profile in the performance of blast clean surfaces. The slip factors do not appear to be influenced by the variation in average DFT readings at least for the range of DFT thicknesses expected in practice. It appears that AS 5100.6 can consider allowing slightly increased capacity for friction-type bolted connections. The capacity reduction factor used in AS 5100.6 for calculating the design shear capacity may possibly be increased if the slip factor is evaluated in accordance with AS 4100 Appendix J. The friction coefficient tests conducted by other organizations may report mean friction coefficients instead of the statistically adjusted values reported from tests conducted according to AS 4100 Appendix J. These results should not be treated equivalent. Assessment of Coatings for Friction-Type Connections 267 Disclaimer The opinions expressed in this paper are entirely those of the authors, and do not necessarily represent the policy of the Roads and Traffic Authority of NSW (RTA). References [1] AS 4100 – 1998: Steel Structures [2] AS 5100.6 – 2004: Bridge design, Part 6: Steel and composite construction [3] Specification for Structural Joints Using ASTM A325 or A490 Bolts9, Prepared by RCSC Committee A.1—Specifications and approved by the Research Council on Structural Connections, June 30, 2004 [4] Specification for Structural Joints Using High-Strength Bolts, Prepared by RCSC Committee A.1—Specifications and approved by the Research Council on Structural Connections, December 31, 2009 [5] RTA QA Specification B220, Protective Treatment of Bridge Steel Work, Edition 3 Revision 1, October 2008
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