History of MEMS at RIT ROCHESTER INSTITUTE OF TECHNOLOGY MICROELECTRONIC ENGINEERING History of MEMS at RIT Dr. Lynn Fuller Webpage: http://people.rit.edu/lffeee Microelectronic Engineering Rochester Institute of Technology 82 Lomb Memorial Drive Rochester, NY 14623-5604 Tel (585) 475-2035 Email: [email protected] Department webpage: http://www.rit.edu/kgcoe/microelectronic Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller 1-23-2017 history of MEMS.ppt Page 1 History of MEMS at RIT OUTLINE MEMS Time Line at RIT MEMS Technology Time Line at RIT Examples of Research Projects in MEMS Examples of Senior Project in MEMS Examples of Masters Thesis Projects in MEMS Examples of Course Projects in MEMS Lots of Pictures and Movies of MEMS Devices The examples in this presentation represents only a few of the many achievements in MEMS at RIT over the past 20 years Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 2 History of MEMS at RIT MEMS TIME LINE 1982 Microelectronic Engineering Program Starts 1986 RIT Dedicates Microelectronic Engineering Cleanroom 1987 First Graduates of MicroE and Start of RIT’s First Full Time Masters Program in Engineering (ME MME) 1989 First MEMS Research Project – Industry Sponsor 1990 First Federally Funded MEMS Research Project 1991 First Senior Project on MEMS 1994 First MEMS Patent Issued to RIT 1995 Student Run Factory to Manufacture CMOS Devices 1996 First Masters Thesis on MEMS Devices 1997 Incubator to Provide Lab Access for Start Up Companies 1999 First MEMS Courses Taught at RIT 2000 First Short Course on MEMS for Industry People 2001 First MEMS Courses Taught in Mechanical Engineering 2002 Start of the Ph.D. Program in Microsystems Engineering 2003 First NSF Funded MEMS Curriculum Development Project and First MEMS Course Taught by EE 2011 First MEMS Ph.D. Student, Journal Publication, 2nd MEMS Patent Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 3 History of MEMS at RIT MEMS TECHNOLOGY TIME LINE 2”& 3” Wafer Fab – Metal Gate PMOS Optical Pattern Generator and Maskmaking Contact Lithography Wafer Saw and Wire Bonder 1986 4” Wafer Fab – Metal Gate PMOS Stepper Lithography 1987 E-Beam Maskmaking 1989 LPCVD Poly, Nitride, LTO Reactive Ion Etch Ion Implant 1991 CMOS Capability 1995 MESA Work-in-Process Tracking System 1999 6” Wafer Fab – CMOS Capability CMP Tools 2002 Deep Trench Etch Tool Rochester Institute of Technology PE CVD Tool Microelectronic Engineering 2010 ASML Stepper 1982 © January 23, 2017 Dr. Lynn Fuller Page 4 History of MEMS at RIT FIRST MEMS RESEARCH PROJECT - MICRO GAS CHROMATOGRAPHY 1989 Dr. Lane, Dr. Fuller, David Price and Perkin Elmer Co Research Project to make gas chromatograph channels in silicon wafers. Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 5 History of MEMS at RIT RIT’S FIRST MEMS PATENT – DR. LANE, 1994 Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 6 History of MEMS at RIT FORCE BALANCE ACCELEROMETER MICRO SYSTEM Feedback If Vo positive Cc C2 Measure C2 V2 + Mass C1 Cc Measure C1 Feedback If Vo negative Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Vo V1 Dr. Lane, 1992 Bell Aerospace, Inc. Page 7 History of MEMS at RIT RIT’S FIRST MICRO MOTORS – SENIOR PROJECT 100 µm Matt Matessa, 1991, BSµE, Joined Cypress Semiconductor San Jose, CA Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 8 History of MEMS at RIT RIT’S FIRST PHOTONIC DEVICES – SENIOR PROJECT Dave Borkholder, 1994, after graduation from RIT joined Ph.D. program in EE at Stanford University Palo Alto, CA HOT FILAMENT LIGHT SOURCES 600 µm GaP wafers with n-type epilayer, add gold metal, dice and wire bond to RIT thick film ceramic package. 100 µm Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 9 History of MEMS at RIT CAPACITOR MICROPHONE – SENIOR PROJECT 1 µm Aluminum Jon Stephan, 1995, joined Intel Corporation Folsom, CA 2.0 µm Gap Rochester Institute of Technology Microelectronic Engineering ALUMINUM DIAPHRAGM CAPACITIVE MICROPHONE © January 23, 2017 Dr. Lynn Fuller Page 10 History of MEMS at RIT MICROPHONE SIGNAL CONDITIONING i R 9V i Vo TL081 V + C -9 V Co = Average value of C Cm = amplitude of C change C = Co +Cm sin (2pft) V is constant across C Vo = - i R i = d (CV)/dt i = V Cm 2 p f cos (2pft) Vo = - 2pf V R Cm cos (2pft) Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller amplitude of Vo Page 11 History of MEMS at RIT CMOS OPERATIONAL AMPLIFIER – MASTERS THESIS +V 10 M11 M3 L/W 80/20 8 2 M4 20/40 M10 M6 20/40 3 80/20 7 5 M9 80/20 20/30 M1 Vin- M2 20/30 20/30 4 9 Vin+ 1 M7 6 M5 20/40 Vout 20/40 20/40 M8 -V p-well CMOS Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller 20 dimensions L/W (µm/µm) Page 12 History of MEMS at RIT CMOS OPERATIONAL AMPLIFIER – MASTERS THESIS ROCHESTER INSTITUTE OF TECHNOLOGY MICROELECTRONIC ENGINEERING LFF OPAMP.XLS FILE3B LOT F960319 OPAMP TEST RESULTS - 1-29-97 Gain dB 73.9794 73.53387 73.33036 70.31748 67.53154 65.48316 63.97314 62.41148 61.51094 60.34067 59.46256 58.68997 58.0618 57.50123 57.14665 56.5215 56.1236 55.56303 20 0 -20 Vout V 10 9.5 9.28 6.56 4.76 3.76 3.16 2.64 2.38 2.08 1.88 1.72 1.6 1.5 1.44 1.34 1.28 1.2 0.02 0.002 0.0002 Vin mV 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 Op Amp Frequency Response 80 70 60 50 Ga in dB Frequency hZ 1 5 100 200 300 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 50000 500000 10000000 40 30 20 10 0 -10 -20 1 10 100 1000 10000 100000 1000000 10000000 Frequency Hz Ed Sayer, MSEE 1991, joined Digital Equipment Corp., Hudson, MA Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 13 History of MEMS at RIT TOP SIDE BULK MICROMACHINED PRESSURE SENSORS – SENIOR PROJECT Pressure Sensor with Nitride Diaphragm and Poly Piezo Resistors over Bulk Etched Cavity 300 µm Jason Trost, 1995 BSµE, joined Harris Semiconductor Mountaintop, PA Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 14 History of MEMS at RIT NIH FUNDED RESEARCH ON PRESSURE SENSORS Source Gate Drain Diaphragm Insulator Contact Si Wafer Air Gap (~1 atm) Kerstin Babbitt, 1997 BSEE U of Rochester, joined Motorola, Austin, TX Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 15 Bottom Plate History of MEMS at RIT FINITE ELEMENT ANALYSIS 2mm x 2mm Crystalline Silicon Diaphragms 30μm thick 50psi Circular Diaphragm Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 16 History of MEMS at RIT 2000 µm NIH FUNDED RESEARCH ON PRESSURE SENSORS FIRST MEMS DEVICE WITH INTEGRATED ELECTRONICS Sensor Oscillator 20/100 20/100 20/100 C sensor 5 to 25 pF VDD= -10V 40/20 VO 600/20 100/20 100/20 100/20 C parasitic = 10pF 0 to 5 mm Hg Pressure Range Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 17 GND R load 1 Meg C load 20 pF History of MEMS at RIT NIH FUNDED RESEARCH ON PRESSURE SENSORS Vgate Vsource 15 µm Vdrain 75 µm Poly Diaphragm 5x Vgate 2 µm n+ Poly Aluminum Plug Vdrain Vsource Etch Holes Contact Cut to Poly Gate Rochester Institute of Technology Microelectronic Engineering P+ 1 µm space (vacuum) P+ 1000 Å Oxide © January 23, 2017 Dr. Lynn Fuller n-type silicon Page 18 History of MEMS at RIT NIH FUNDED RESEARCH ON PRESSURE SENSORS Kerstin Babbitt 1997, Motorola Stephanie Bennett 1997, ASML Sheila Kawati 1998, Syracuse Medical School An Pham 1999, Integrated NanoTechnology Dr. Lynn Fuller 500 µm Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 19 History of MEMS at RIT INCUBATOR - ADVANCED VISION TECHNOLOGY INC. Transparent Si 2 Window O Seal/Plug Vacuum Chamber Control Gate Emitter Insulator Low Voltage Phosphor Substrate Micro-encapsulated Chamber Integrated Phosphor Field Emission Device .900 Color Chart of AVT Phoshors .800 .700 .600 YELLOWISH GREEN GREEN .500 .400 BLUISH GREEN BLUE .300 GREEN .200 Rochester Institute of Technology Microelectronic Engineering GREENISH BLUE BLUE .100 000 © January 23, 2017 Dr. Lynn Fuller PINK RED PURPLISH RED REDDISH PURPLE .100 .200 .300 .400 .500 .600 .700 .800 Page 20 History of MEMS at RIT INCUBATOR – INTEGRATED NANO-TECHNOLOGIES, LLC Hybridization Courtesy of T A GC A T C G A T AT Gold INT Bio-Detect Card 65°C 1 µm A T CG T A G AC T T A Gold Dr. David Chafin and Dr. Rick Murante Because the DNA is hybridized to a probe DNA with 15 matching base pairs, the probability that the attached DNA is the desired DNA is one billion to one or better. (i.e. 415 ) Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 21 History of MEMS at RIT FIRST MEMS PROJECT BETWEEN COE AND COS CHEMIRESISTOR Simple inter-digitated electrodes coated with a chemically sensitive layer that changes the resistance in response to a few ppm of some (or many) chemicals Copper-substituted Phthalcyanine conductive polymer is sensitive to CCl4, NH3 and N2O or Carbon Nano-Tubes and various polymers Dr. Lynn Fuller Dr. KSV Santhanam Yatin Prayag 1999 Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Resistor with 25µm gaps 25µm length 7250µm width Page 22 History of MEMS at RIT CHEMICAL SENSORS Upper Left: Finished Sensor with chip pins Upper Right: Close up of interdigitated gold fingers Elizabeth Gregg 2005 Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 23 History of MEMS at RIT CHEMICAL SENSORS Mix a polymer with Carbon Black and apply a thin coat over interdigitated gold fingers Testing 30s off, 120s on, 60s off, 120s on, 30s off 0.1 ml Acetone/ 125 ml bottle = 800 ppm Resistance goes from ~100 ohms (no vapor) to ~ 4,000 ohms (with vapor) Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 24 History of MEMS at RIT FIRST MECHANICAL ENGINEERING MEMS RESEARCH PROJECT FLOW PLATES FOR FUEL INJECTION Variety of different size and shape holes etched through 500 µm thick silicon wafer Dr. Risa Robinson Delphi Products, Inc. Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 25 History of MEMS at RIT BULK MICROMACHINED ATOMIZER FOR DRUG DELIVERY n-type Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 26 History of MEMS at RIT MEMS THERMAL ACTUATOR MASTERS THESIS Current Flow = zero Current Flow = 10 mA Skinny arm is hotter and expands causing bending motion Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 27 History of MEMS at RIT FINITE ELEMENT ANALYSIS OF THERMAL BENDING ANSYS Small arm 300 C, 10um X 100 um Large arm 0 C, 30 um x 100 um Maximum Displacement = 6 um Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Andrew Randles Page 28 History of MEMS at RIT INTEGRATION OF PHOTODIODE AND MEMS December 2001 Kevin Munger. joined IBM Burlington, VT Thermal Actuator with Integrated Photodiode Rochester Institute of Technology Microelectronic Engineering Maximum Deflection 9 µm at 30 µw 162,000 cycles, 6 msec., © January 23, 2017 Dr. Lynn Fuller Page 29 History of MEMS at RIT SHORT COURSE JULY 2000 EXAMPLE Cantilevers Springs Accelerometer Electrostatic Comb Drive Mirrors Optical Modulators Optical Arrays Tweezers Inductors Contactors Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 30 History of MEMS at RIT APRIL 1999 CLASS PROJECT Cantilevers Springs Accelerometer Electrostatic Comb Drive Mirrors Optical Modulators Optical Arrays Tweezers Inductors Contactors Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 31 History of MEMS at RIT CANTILEVERS AND COMB DRIVES Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 32 History of MEMS at RIT OTHER STRUCTURES Mirror Gears Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 33 History of MEMS at RIT SEM PICTURES Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 34 History of MEMS at RIT VERIFICATION OF RELEASE Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 35 History of MEMS at RIT ELECTRICAL RESULTS Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 36 History of MEMS at RIT ELECTROSTATIC ACTUATION OF CANTILEVER 1 µm Movement Rochester Institute 10of Technology Volt Electrostatic Actuation Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 37 History of MEMS at RIT 2003 CLASS PROJECT - GAS FLOW DETECTOR Heater GAS Flow Upstream Temp Sensor Downstream Temp Sensor No Voltage to Heater Resistance of Heater 1000 ohms Resistance of Resistor 4800 ohms Polysilicon Al SacOx Rochester Institute of Technology Microelectronic Engineering Si3N4 Silicon Substrate © January 23, 2017 Dr. Lynn Fuller Page 38 History of MEMS at RIT SURFACE MICROMACHINED GAS FLOW SENSOR Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Vee Chee Hwang, 2004 Page 39 History of MEMS at RIT PHOTOGRAPHS/SEMS/ELECTRICAL Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 40 History of MEMS at RIT HEATER TESTING Movie 20 Volts applied to Heater Resistor changed by 100 ohms Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 41 History of MEMS at RIT MOVIE OF HEATER Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 42 History of MEMS at RIT 2002 CLASS PROJECT – PRESSURE SENSOR Polysilicon Resistors Aluminum Metal Silicon Nitride Insulator R1 Si 500 µm R3 R2 Silicon Diaphragm Silicon Nitride Etch Mask Package Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 43 R4 History of MEMS at RIT FINITE ELEMENT ANALYSIS Points of Maximum Stress Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 44 History of MEMS at RIT FINITE ELEMENT ANALYSIS 2mm x 2mm Crystalline Silicon Diaphragms 30μm thick 50psi Regular Si Diaphragm Corrugated Diaphragm Layer 2: 1.5mm x 1.5mm Polysilicon 1μm thick Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller By Rob Manley Page 45 History of MEMS at RIT DIAPHRAGM DEFORMATION MOVIE Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 46 History of MEMS at RIT DIAPHRAGM STRESS MOVIE Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 47 History of MEMS at RIT DIAPHRAGM FABRICATION 20 µM 20% KOH Etch, @ 72 C, 10 Hrs. Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 48 History of MEMS at RIT MOVIE OF DIAPHRAGM MOVING R3 R1 R4 R2 Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 49 History of MEMS at RIT TESTING 5 Volts Vo2=2.5035v R1 R3 R2 Vo1=2.4965v R4 Gnd Rochester Institute of Technology Microelectronic Engineering Apply and release chuck vacuum to observe change in output voltage © January 23, 2017 Dr. Lynn Fuller Page 50 History of MEMS at RIT WIRE BONDING AND PACKAGING Fixture to hold TO-8 and TO-39 packages for wire bonding. Rob Manley Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller K&S WAFER SAW Page 51 History of MEMS at RIT TESTING OF PACKAGED PRESSURE SENSORS 0 5 10 15 20 25 30 35 40 45 60.6 63.84 66.32 68.95 72.28 75.62 78.68 81.25 84.39 87.21 Output Voltage (mV) MEMS Pressure Sensor Output Rochester Institute of Technology Microelectronic Engineering 5-15-02 © January 23, 2017 Dr. Lynn Fuller 100 90 80 70 60 50 40 30 20 10 0 y = 0.0002x2 + 0.586x + 60.593 0 10 20 30 Pressure (psi) Page 52 40 50 History of MEMS at RIT SURFACE MICROMACHINED GAS FLOW SENSOR L of heater & resistor = 1mm W (heater) = 50um W (resistors) = 20um Gap = 10um V applied = 27V to 30.5V Temp ~600 °C at 26 volts Lifetime > 10 min at 27 volts (possibly longer, did not test) Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Vee Chee Hwang, 2004 Page 53 History of MEMS at RIT BULK MICROMACHINED GAS FLOW SENSOR Measured Resistance, V/I=1.2Kohms Theoretical Resistance, L*Rhos/W= 400µm*60/20µm = 1.2Kohms Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Raunak Mann, 2004 Page 54 History of MEMS at RIT THERMIONIC GAS DETECTOR Polysilicon Micro-filament heater Make hot Thermionic emission occurs causing ionization Force ions to a collection plate Measure resulting current or voltage Resistive Heater Collection Plate Amplified Current + Biasing Plate Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Ionic current Robert Manley, 2004 Page 55 History of MEMS at RIT THERMIONIC GAS DETECTOR Polysilicon Un-etched Sacox Silicon Nitride Si Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Robert Manley, 2004 Page 56 History of MEMS at RIT THERMIONIC GAS DETECTOR Cold Hot Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Robert Manley, 2004 Page 57 History of MEMS at RIT MODIFIED BULK PROCESS FOR MEMS CLASS 2004-06 Metal PE CVD Nitride Poly Diffusion Diaphragm Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 58 History of MEMS at RIT MODIFIED BULK PROCESS FOR MEMS CLASS 2004-06 Pressure Sensor, diffused resistors or poly resistors Microphone- more sensitive pressure sensor Speaker – diaphragm with coil on it, magnet below Accelerometer – diaphragm with mass in center from back etch donut Diaphragm Actuator with coil and resistors for sensing and feedback Optical pyrometer with thermocouples on diaphragm Heater on diaphragm either poly or diffused resistor heater Heater plus temperature sensor (diffused heater, poly resistor sensor) Heater plus interdigitated chemical sensor Cantilever accelerometer with piezoresistors either poly or diffusion, mass from back etch donut Cantilever accelerometer with magnetic coil for sensor, mass from back etch donut Gas flow sensor single resistor anemometer Gas flow sensor with heater and two resistors Torsional mirror with coil actuators Gyroscope with piezoresistor sensors or coil and magnet sensors, with mass from back etch donut for each ½ of torsion bar Transistors and logic, RF Inductors Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 59 History of MEMS at RIT MODIFIED BULK PROCESS FOR MEMS CLASS 2004-06 Torisonal Mirror Class Project Chip Rochester Institute of Technology Microelectronic Engineering Gas Flow Sensor © January 23, 2017 Dr. Lynn Fuller Page 60 History of MEMS at RIT MODIFIED BULK PROCESS FOR MEMS CLASS 200406 Movie Thermopile Speaker Rochester Institute of Technology Microelectronic Engineering Accelerometer Inductor © January 23, 2017 Dr. Lynn Fuller Pressure Sensor Page 61 History of MEMS at RIT MEMS ACTUATOR AND POSITION SENSOR Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 62 History of MEMS at RIT VISCOCITY SENSOR JOURNAL PUBLICATION AND PATENT Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 63 History of MEMS at RIT MODIFIED BULK PROCESS FOR MEMS CLASS 2004-06 Wafer Inspection Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Backside of Wafer Page 64 History of MEMS at RIT BIO PROBES Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 65 History of MEMS at RIT SECOND VERSION COMPLETED DEVICES W3 W1 L1 L2 W2 Rochester Institute of Technology Microelectronic Engineering W1 = 300 µm W2 = 1100 W3 = 450 L1 = 1400 L2 = 1250 © January 23, 2017 Dr. Lynn Fuller Page 66 History of MEMS at RIT THERMALLY ACTUATED MEMS MICRO MIRROR Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 67 History of MEMS at RIT DEVICE CROSS SECTION Mechanical Poly Layer Metal Sacrificial Oxide Field Oxide Bottom Poly Starting Wafer Bottom Poly 1 (Red) Layer 1 Sacrificial Oxide (Blue Outline) Layer 2 Anchor (Green) Layer 3 Mechanical Poly 2 (Purple) Layer 4 Contact Cut (White) Layer 6 Metal (Blue) Layer 7 Outline (Yellow Outline) Layer 9 No Implant Yellow Layer 15 Rochester Institute of Technology Microelectronic Engineering Holes Layer 16 (combined with Poly 2) © January 23, 2017 Dr. Lynn Fuller Page 68 History of MEMS at RIT LIST OF MEMS DEVICES MADE WITH THIS PROCESS Resistors – Micro Bolometer Heaters – Chemical Sensors Micro Mirror - Two Axis Mirror Thermally Actuated Two Arm Cantilever Chevron Actuators Electrostatic Comb Drive MEMS Switch Accelerometer Gas Flow Sensor, Anemometer, Thermionic Light Modulator Bio Probes Speaker Humidity Sensors Pressure Sensors - Microphone Temperature Sensors – Thermopile, Resistor Inductors, Capacitors – Humidity Sensor Rochester Institute of Technology Hall Effect Sensors – other Magnetic Field Sensors Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 69 History of MEMS at RIT 2014 MEMS MULTICHIP PROJECT DESIGN Total 15 mm by 15 mm plus 500 um for sawing into 9 chips for overall 16.5mm by 16.5mm size. Wafer sawing is easier if all chips are the same size 5mm by 5mm design space for each project Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 70 History of MEMS at RIT MEMS CLASS PROJECT FALL 2014 Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 71 History of MEMS at RIT 2015 PROCESS DESCRIPTION Mechanical Poly2 Layer Metal Sacrificial Oxide Field Oxide Bottom Poly1 Starting Wafer This is a surface micromachine process with two layers of polysilicon and one layer of metal. Poly2 can be suspended above the wafer allowing for structures that can move. The two poly layers can cross without connection or can be connected through anchor holes. The metal layer can connect to Poly2 through a via or to Poly1 through via and anchor holes. The yellow layers are silicon nitride. Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 72 History of MEMS at RIT MENTOR GRAPHICS LAYOUT OF CANTILEVER The cantilever shown is anchored on the left and free to move on the right. The design includes resistive and capacitive position sensors and electrostatic actuation. The device can be used as an accelerometer. Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 73 History of MEMS at RIT 2015 MEMS MULTICHIP PROJECT DESIGN Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 74 History of MEMS at RIT CLEAR FIELD RETICLE FOR ASML Poly One Non-Chrome Side Metal Chrome Side Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 75 History of MEMS at RIT SURFACE MEMS 2015 PROCESS 1. Starting wafer 2. PH03 – level 0, Marks 3. ET29 – Zero Etch 4. ID01-Scribe Wafer ID, D1… 5. ET07 – Resist Strip, Recipe FF 6. CL01 – RCA clean 7. OX04 – 6500Å Oxide Tube 1 8. CV01 – LPCVD Poly 5000Å 9. IM01 – Implant P31, 2E16, 60KeV 10. PH03 – level 1 Poly-1 11. ET08 – Poly Etch 12. ET07 – Resist Strip, Recipe FF 13. CL01- RCA Clean 14. OX05 – 700Å Dry Oxide 15. CV02- LPCVD Nitride 4000Å 16. PH03 – level 2 Anchor 17. ET29 – Etch Nitride 18. ET07 - Resist Strip, Recipe FF 19. CL01 – RCA Clean 20. CV03-TEOS SacOx Dep 1.75um 21. PH03 – level 3 SacOx Define 22. ET06 - wet etch SacOx Define Etch 23. ET07- Resist Strip, Recipe FF 24. CL01 – RCA Clean 25. CV01-LPCVD Poly 2um, 140 min 26. PH03 - level 4 No Implant 27. IM01-P31 2E16 100KeV 28. ET07 Resist Strip, Recipe FF 29. CL01 – RCA Clean 30. OX05- 500Å pad oxide 31. CV02 – 2000Å nitride 32. PH03 - level 5 Poly2 33. ET29 – Plasma Etch Nitride 34. ET06 – Wet Etch pad oxide 35. ET68 - STS Etch Poly2 36. ET07 - Resist Strip, Recipe FF 37. PH03 – level 6 Contact Cut 38. ET29 – Etch Nitride Contact Cut 39. ET06 – Etch Oxide Contact Cut 40. ET07 – Resist Strip, Recipe FF 41. 39. CL01 – RCA Clean two HF 42. ME01 – Metal Deposition - Al 43. PH03 – level 7 Metal 44. ET55 – Metal Etch - wet 45. ET07 – Resist Strip 46. PH03 – level 8 – Release 47. SA01 – Saw Wafer ½ Way 48. Special Soap Clean 49. ET66 – Final SacOx Etch 50. ET07 - Resist Strip with Acetone 51. Rinse and Dry w Isopropyl Pull 52. TE01 – wafer level testing 53. SEM1 – Pictures 54. Packaging and Testing 12-8-15 Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 76 History of MEMS at RIT BLOG - ZERO ETCH AND PHOTORESIST STRIP Today’s Goal: Coat the wafers with photoresist, expose with ASML stepper, develop and plasma etch ASML alignment marks on six wafers. Step 2: Etch Silicon using Drytek Quad 482 Etcher – Cleaning of chamber for 5 min. in 02 plasma Etching the device wafer for 2 min. in CF4, CHF3 and O2 plasma Inspection of alignment marks on wafer Removal of Photoresist using GaSonics - (recipe FF) Microscope images of alignment marks before and after P.R. removal Before P.R. removal After P.R. removal Rochester Institute of Technology Drytek Quad Microelectronic Engineering GaSonics PR Asher Authors: Abhinav, Nikhil, Ranjana, Shruthi, Yamini © January 23, 2017 Dr. Lynn Fuller Page 77 October 19, 2015 History of MEMS at RIT BLOG - RCA CLEAN AND OXIDE GROWTH Today’s Goal: Remove organic and metallic contaminants from wafers with RCA clean, steam oxide growth of 6500Å of oxide in Bruce Tube 1. • Performed step 6: CL01 (RCA clean) Cleaned four wafers from lot Processed through SRD afterwards • Adam developed and etched the other two wafers in the lot • Performed step 7: OX04 (oxide growth) Procedure used to grow 6500A of oxide • Measured Oxide Thickness: Mean : 6597.7 Å Std Dev. = 0.38% OX04 – oxide growth CL01 – RCA Clean Rochester Institute of Technology Microelectronic Engineering Authors: Mattias Herrfurth, Corey Shay © January 23, 2017 Dr. Lynn Fuller Page 78 October 20, 2015 History of MEMS at RIT BLOG - POLYSILICON2 ETCHING Today’s Goal: To etch Polysilicon2 on remaining wafers • Using the dry tech quad tool, Recipe FACPOLY • Chamber 2, Time= 18 minutes Adam at Dry Tech Quad Wafer Bfore Poly Etch Wafer After Poly Etch Rochester Institute of Technology Microelectronic Engineering Authors: Ankur © January 23, 2017 Dr. Lynn Fuller Page 79 December 5, 2015 History of MEMS at RIT BLOG - CONTACT LITHO, NITRIDE & OXIDE ETCH Today’s Goal: To perform Level 6, Contact cut lithography and Nitride and Oxide etch on wafers D2, D4, D6. • Manual coating of PR S1827 • Contact cut lithography with Dose- 400 mj/cm2 Focus offset – 0.5 micro σ = 0.7 • Post bake at 140 °C • Nitride Etch – Recipe – Factory Nitride Etch, Lam 490 Gas used – SF6 Time – (3 minutes for etch + 1 minute over etch)/wafer • Buffered Oxide Etch – BOE 5.2:1 - for 2 minutes Deionized water - for 5 minutes, SRD Wafer after Oxide etch Rochester Institute of Technology Microelectronic Engineering Authors: Abhinav, Nikhil, Ranjana, Shruthi, Yamini © January 23, 2017 Dr. Lynn Fuller Page 80 December 07, 2015 History of MEMS at RIT BLOG - ALUMINUM METAL DEPOSITION Today’s Goal: Deposit Al using CVC601 Sputter tool for a target thickness of 10,000Å. • • Step 42: ME01 – Metal Deposition – Al 4 device wafers (D2, D3, D4, D6 ) + 1 control wafer with tape for measurement Time ~ 34 min 2000 Watts for ~300 Å/min ( Sputtering power ) Pressure 5 mT ( Sputtering Pressure ) Argon Flow 28 sccm ( to set the Sputtering Pressure ) Arc detect count -> 40 Pre-sputtering: 5 min same power - Arc detect count -> 3 Remove contaminants from target expose to atmosphere (Al 2O3, AlN, etc.). Target Wafer after Sputtering Inside the Vacuum Chamber Inside the Vacuum Chamber Rochester Institute of Technology with theMicroelectronic Platen Engineering without the Platen Authors: Miaotian Wang © January 23, 2017 Dr. Lynn Fuller Page 81 December 9, 2015 History of MEMS at RIT OIL QUALITY MEMS MULTI-SENSOR Photo Diode 5mm x 5mm Diffused Heater Actuator Viscosity Sensor Water in Oil EIS Diode Temperature Sensor Picture of MEMS Multisensor Device 2H 30V-30us pulse v. SAE 60 temperature SAE60_35_Y 4.00E-07 SAE60_43_Y SAE60_54_Y 2.00E-07 Displacement (m) SAE60_75_Y 0.00E+00 -5.00E-04 0.00E+00 5.00E-04 1.00E-03 -2.00E-07 -4.00E-07 -6.00E-07 -8.00E-07 -1.00E-06 Rochester Institute of Technology Microelectronic Engineering Time (s) Temp Sensor Test Viscosity Oil with 1% Soot © January 23, 2017 Dr. Lynn Fuller Page 82 1.50E-03 2.00E-03 History of MEMS at RIT MICROSYSTEM Battery USB Power Energy Harvester Power Management other . . . . µP Rochester Institute of Technology Microelectronic Engineering . . . . Communication MEMS Signal Conditioning Team Galt’s definition for Microsystems is the integration of MEMS sensors and actuators with CMOS electronics to provide solutions for a wide variety of applications including automotive, military, aerospace, consumer and biomedical. USB, WiFi CAN (other) Wireless World Wide Web © January 23, 2017 Dr. Lynn Fuller Page 83 History of MEMS at RIT MULTISENSOR MICROSYSTEM Back µP Rochester Institute of Technology MEMS Multisensor Chip Acceleration (shock) Temperature, Humidity Front Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 84 History of MEMS at RIT OTHER PROJECTS Dr. David Borkholder – PI Blast Dosimeter / DARPA Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 85 History of MEMS at RIT OTHER PROJECTS BlackBox Biometrics The company was founded by RIT professor David Borkholder and recently graduated from the Venture Rochester Institute of Technology Creations incubator. http://b3inc.com Microelectronic business Engineering © January 23, 2017 Dr. Lynn Fuller Page 86 History of MEMS at RIT ENERGY HARVESTING Indirect Conversion of Radiation for 20 Year-Life Batteries Green Optimized Photocell Gaseous Tritium Light Source (GTLS) 1.6 cm Rochester Institute of Technology Microelectronic Engineering (GTLS) – Phosphor Coat Glass Vial with Tritium Inside Tritium: Radioactive Isotope of Hydrogen, 3H, 12year half life Emits Electrons Through Beta Decay Electrons Interact With Phosphor Material Green Light is Emitted (Radio luminescence) Photo Detector Captures Light and Converts to Energy Energy Management Electronics Stores Energy in a Super Capacitor © January 23, 2017 Dr. Lynn Fuller Page 87 History of MEMS at RIT VIBRATION ENERGY HARVESTER Dr. Denis Cormier 3-D Printer Brinkman Lab at RIT Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 88 History of MEMS at RIT WIRELESS MICROSYSTEMS Capacitor Sensor Bluetooth Transceiver 2.5” x 3” BT-Arduino Wireless Platform Breadboard 5” x 8” Breadboard Rochester Institute of Technology Microelectronic Engineering 1” x 1” PCB © January 23, 2017 Dr. Lynn Fuller 2mm x 3mm Custom CMOS & MEMS Page 89 History of MEMS at RIT COMPANIES WITH LINKS TO RIT Personal Sound Technologies Advanced Vision Technologies Integrated Nanotechnologies MicroGen BlackBox Biometerics Tenrehte Simpore Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 90 History of MEMS at RIT ACKNOWLEDGEMENTS Dr. Richard Lane Dr. Risa Robinson Dr. Robert Pearson Dr. KSV Santhanam Dr. Sergey Lyshevski Dr. David Borkholder Dr. Karl Hirschman Matt Matessa Jon Stephan Ed Sayer Jason Trost Kerstin Babbitt Stephanie Bennett Sheila Kawati An Pham Andrew Randles Kevin Munger Rob Manley Vee Chee Hwang Ivan Puchades Team Galt Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 91 History of MEMS at RIT TEAM GALT Tal, Lynn, Ellen Sedlack, Christian, Artur, Ivan, Renat B.S., M.S., Ph.D., students from EE, Rochester Institute of Technology ME, MicroE, CE, Materials Science Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Heidi, Murat Page 92 History of MEMS at RIT DR. FULLER’S STUDENTS IN EMCR 890 MEMS CLASS 2002 Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 93 History of MEMS at RIT CONFERENCE PUBLICATIONS 1. “Nanocomposite Material for Sensing of Halogenated Methanes: A Model Based on Charge Transfer Interaction for Selectivity,” R.Sangoi, L.Fuller, K.S.V. Santhanam, MRS Meeting, Boston, Massachusetts, October, 2003. 2. “Design and Analysis of a Shear Stress Sensor for Microcirculation Investigation,” ASME Fluid Engineering Division July 6-10, 2003, Honolulu, Hawaii, L.F.Fuller, Risa Robinson, et.el. 3. “Bulk Micromachined Pressure Sensor,” L.F.Fuller, Steve Sudirgo, Proceedings of the IEEE UGIM Conference, June 2003, Boise State University. 4. “An Inter-digitated Electrode Detector for the Identification of a Single Specific DNA Molecule Fragment,” L.F.Fuller, Renaldo Vega, Robert Manley, Vee Chee Hwang, Dan Jansen, An Pham, Nate Wescott, Mike Connolly, Proceedings of the IEEE UGIM Conference, June 2003, Boise State University. 5. “Fabrication of Polysilicon Surface Micromachined MEMs Structures”, Kevin Munger and Lynn F. Fuller, Microelectronic Engineering, Rochester Institute of Technology, Proceedings of the IEEE UGIM Conference, June 2001, Virginia Commonwealth University. 6. “MEMS Activity at Rochester Institute of Technology," L.F.Fuller, A.Pham, P. Merwah, Proceedings of the IEEE UGIM Conference, June 20-23, 1999, Minneapolis, MN 7. "A Surface Micromachined Capacitive Pressure Sensor for Biomedical Applications," K.E.Babbitt, L.F.Fuller, B.Keller, Proceedings of the IEEE UGIM Conference, July 20-23, 1997, Rochester, NY 8. "A Multi-project MEMs Leture and Laboratory Course," L.F.Fuller, Proceedings of the IEEE UGIM Conference, July 20-23, 1997, Rochester, NY 9. "Microelectronic Engineering at RIT - The First 10 Years", L.F.Fuller, R.E.Pearson, S.K.Kurinec, Rochester Institute of Technology I.R.Turkman, M.A.Jackson, R.L.Lane, Proceedings of the 10th Biennial University Industry MicroelectronicB.W.Smith, Engineering Government Microelectronics Symposium, May 1993, Durham NC. © January 23, 2017 Dr. Lynn Fuller Page 94 History of MEMS at RIT HOMEWORK – HISTORY OF MEMS 1. Read “A thermally Actuated Microelectromechanical (MEMS) Device for Measuring Viscoscity” I. Puchades and L.F. Fuller, IEEE Journal of MEMS, June 2011. Explain how the device works. 2. View the following link and read the article on “Blast Gauge” http://www.rit.edu/research/media/documents/11_SS_Research_at_ RIT.pdf What types of MEMS devices are inside the “Blast Gauge”. 3. Find the MEMS Fabrication Blog from the Fall of 2015. What types of devices were made? Look for pictures of devices. 4. Why is packaging important for MEMS devices? 5. List the MEMS devices you use have in your car or phone. Rochester Institute of Technology Microelectronic Engineering © January 23, 2017 Dr. Lynn Fuller Page 95
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