AY2015 NIT Ibaraki College
Takashi ISAGO
Email: [email protected]
Hidehito KOMATSUZAKI
ExperimentⅠ(C) (Inorganic Chemistry)
Email: [email protected]
Katsuyuki IWANAMI
Email: [email protected]
Yoshiharu MIYASHITA
Email: [email protected]
Basic Information
Course
Regular Course
Compulsory / Elective
Compulsory
Grade
3rd
Number of Credits
3
Semester
Full year
Credit Type
Normal
Class Type
Technical Subject
Course Objectives
Though the experiences in the experiment, you will acquire the knowledge that you have learned in
inorganic and organic chemistry, as well as the basic operation and technique of experiment. In addition,
you will identify and characterize the synthesized materials using several analytical instruments.
The course objectives are follows:
1. To understand how to achieve the objectives of each experiment by using the experimental equipment
and tools
2. To understand the basic technical knowledge of engineering through experiments and exercises
3. To discuss and explain the obtained data from experiments and exercises
4. To think logically about experiment outcomes and summarize them in a form of report
5. To communicate/ discuss his/her experiment with the teaching staff
Topic Outline / Schedule
Week
Topic
Outline
1
Safety Education, How to Write Report
3
Orientation for Inorganic
Chemistry Experiment
Copper (II) Sulfate（1）
Copper (II) Sulfate（2）
4
5
6
Lead(II,IV) Oxide (1)
Lead(II,IV) Oxide (2)
Lead(II,IV) Oxide (3)
Synthesis (1)
Synthesis (2)
Measurement of X-ray Diffraction Pattern
7
8
9
10
11
Cobalt (III) Complex (1)
Cobalt (III) Complex (2)
Cobalt (III) Complex (3)
Measurement of pKa
Sodium Carbonate (1)
Synthesis (1)
Synthesis (2)
Measurement of Visible-ultraviolet Absorption Spectrum
Acetic Acid, pH Titration Curve
Synthesis by Ammonia Soda Process (1)
2
Synthesis and Qualitative Experiment (1)
Synthesis and Qualitative Experiment (2)
1
AY2015 NIT Ibaraki College
12
13
14
Sodium Carbonate (2)
Nitric acid
Glass-work
Synthesis by Ammonia Soda Process (2)
Synthesis by Ostwald Process
Connection of Glass Tube
15
16
Check of Report and Review
Orientation for Organic Chemistry
Experiments
Esterification 1
Safety Education, How to Write Report,
Basic Experimental Procedure for Organic Synthesis
Synthesis of Ethyl Acetate 1
17
18
19
Esterification 2
21
Electrophilic
Substitution 1
Electrophilic Aromatic
Substitution 2
Discussion 1
22
23
Friedel-Crafts Reaction 1
Friedel-Crafts Reaction 2
Synthesis of 4-Methylacetophenone 1
Synthesis of 4-Methylacetophenone 2
24
25
Grignard Reaction 1
Grignard Reaction 2
Synthesis of 2-Phenylhexan-2-ol 1
Synthesis of 2-Phenylhexan-2-ol 2
26
Discussion 2
27
Reduction 1
Discussion for Synthesis of 4-Methylacetophenone and
2-Phenylhexan-2-ol
Synthesis of Hydrobenzoin 1
28
29
30
Reduction 2
Discussion 3
Check of Report and Review
20
Aromatic
Synthesis of Ethyl Acetate 2
Synthesis of o-Nitrophenol 1
Synthesis of o-Nitrophenol 2
Discussion for
o-Nitrophenol
Synthesis
of
Ethyl
Acetate
and
Synthesis of Hydrobenzoin 2
Discussion for Synthesis Hydrobenzoin
Textbooks and Other Readings
Material Engineering ExperimentⅠText (Inorganic Chemistry Experiment) , Department of Chemistry and
Material Engineering (ed.), 2015 (in Japanese )
Material Engineering ExperimentⅠText (Organic Chemistry Experiment) , Department of Chemistry and
Material Engineering (ed.), 2015 (in Japanese )
Kazuyuki HIRAO, Katsuhisa TANAKA, Atushi NAKAHIRA, Inorganic Chemistry -The Modern Approach
-(2rd Edition), Tokyo Kagaku Dojin (in Japanese)
J. McMurry, Organic Chemistry (8th Edition), Cengage Learning, 2012*
* available in our library
Relevant Online Resources
Adil Hosein: Crystal Field Theory-Part1 (University of the West Indies)
https://www.youtube.com/watch?v=MJz02yqXRw8&feature
Sacha Kop: Xray diffraction（The University of Texas at Austin）
https://www.youtube.com/watch?feature=player_detailpage&v=UfDW0-kghmI
Organic Chemistry Lab Experiments (YouTube)
https://www.youtube.com/playlist?list=PLJgMPwX2wmUwynBjAl06tI0k2lsiJMX7J
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AY2015 NIT Ibaraki College
Grading Policy
Grading will be based on experimental efforts, reports(R) and discussions (D). The weighting is as follows:
Efforts
50%
R&D
50%
total
100%
To get credits, you need to get 60 or more points in total.
Course Description
When making an experiment, you should sufficiently prepare by learning beforehand the purpose and
contents of each theme of experiment. To review each experiment, you need to check the books and
papers introduced in class.
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