AccuStandard
®
Table of Contents
Quality Control Standards
1-15
NotLot™ (Same Formulation but Independent Lot)
2
Column Testing
2
ASL (Alternate Source Line)
3-11
PT (Proficiency Testing) Self-Tests
12-13
ASTM QC Tests (see Petrochemical section)
271-272
Organic Single Analytes, Select Mixtures and Methods
Persistent Organic Pollutants (POP)
15-152
16-80
Polychlorinated biphenyls (PCBs) and Metabolites
16-35
Halogenated Aromatics (other than PCBs & PBDEs)
36-37
Dibenzo-p-dioxins (Dioxins)
38-39
Dibenzofurans
39-40
Polybrominated Diphenyl Ether (PBDE) Congeners, Metabolites & BFRs
41-54
PAHs and Derivatives
55-59
Nitrogen Containing Compounds
60
Pesticides and Herbicides 67 New
61-80
Volatiles (VOCs)
81-84
By Functional Group
85-92
Alcohols
85
Aldehydes and Derivatives
85-86
Ketones
86
Phenols
87-88
Amines, Anilines, Amino Compounds
88-90
Ethers
90
Halo Ethers
91
Haloacetic Acids
91
Fatty Acid Ethyl Esters
91-92
Phthalates
92
By Application
94-96
Fuels & Hydrocarbons (see Petrochemical section)
318-321
Plastic Additives 58 New
97-102
Food Analytes (Lipids, Vitamins and Preservatives)
103-107
Allergens (Personal Care Products)
108-113
Dyes
114-116
Perfluorinated Acids and Salts (PFOA, PFOS)
117
Odor Standards
117
Irritant Standards New
117
Refrigerants
118
Qualitative Kits
119-121
124-134
CLP (Contract Laboratory Program)
136-152
500 Series - For Drinking Water
153-180
600 Series - For Waste Water
181-192
1300 Series - TCLP (Toxicity Characteristic Leaching Procedure)
193-194
1600 Series - PBDEs, Pesticides, Pharmaceutical Waste Discharge & PCBs
195-206
8000 Series - For Solid Waste, Appendix IX and Explosives
207-249
■■Singles are listed by: POP category,
Functional group and Application
(highlighted in orange).
■■Individual analytes used in EPA
Methods are listed pages 124-134.
■■Indices: Catalog Number, CAS
Number and Organic Analytes are
on pages 412-440.
Mixtures:
■■Mixtures not associated with
specific methods can be found
in the single organic section with
their chemical group.
Custom Services
■ Custom Synthesis
■ Custom Formulations
■ Custom Packaging
■ Bulk Quantity Requirements
see page v for details
251-268
Regional Methods - Canada, Europe, Asia, USA States, Municipalities, etc.
252-266
ASTM 7065-6, 7485 Nonylphenols More
267
USP 467, Method 465-D, F-List
268
© AccuStandard, Inc. 2012
iii
iv
v
vi
vii
viii
Singles:
122-249
Individual Analytes from EPA Methods
Methods other than EPA
About AccuStandard
Quality Resources
Custom Services
Quality System
Certificate of Analysis
Technical Reference Books
93-121
Explosives
EPA Methods
Prefix
PRINTED ON
RECYCLED PAPER
Petrochemical
269-344
ASTM Listing and Cross References
269-270
Quality Control
271-272
Physical Properties
274-275
Sulfur Standards
276-279
PIANO
280-281
Detailed Hydrocarbon Analysis and SIM DIS
282-283
ASTM Reference Standards (other)
283-312
Diisocyanates
307
UOP Standards
313
Miscellaneous - Skinner List, Fire Debris
314
BioFuels
315-317
TPH & Fuels & Hydrocarbons
318-321
Brownfield Regulation and ISO/DIS 9337
321
LUFT/LUST (UST) Methods - State Specific, GRH, DRH - TPH
322-336
Oil, Grease & TPH - EPA Methods 1664, 413.2/418.1 and 8440
336
Wear Metals (Organometallics)
337-344
Lubricating Oils
342-344
Inorganic
New Products in
this Catalog
■■Pesticides 67 New
■■Plastic Additives 58 New
■■Irritant Standards
■■Mixed Bromo/Chloro Hydroxylated
Diphenyl Ethers
■■Organophosphate Flame
Retardants
■■Fluorinated PBDEs (ISTD) More
■■PBDE Congeners (205) More
■■PBDE Metabolites (60) More
■■PCB Metabolites More
■■Chlorodiphenyl Ethers
■■Brominated Benzo-p-Dioxins
■■Nonylphenols More
■■Instrument Specific ICP More
348-408
Single Element
348-364
ICP
348-351
ICP/MS
352-353
AA
354-356
Matrix Modifiers
357
Ion Chrom
358-361
Wet Chemicals
362-363
TPH, Oil and Grease
364
ICP Multi-Element
366-392
Merck Multi-Element
381-382
Alternate Source (Agilent/Varian, Perkin Elmer, Jobin Yvon, Teledyne)
383-391
Miscellaneous Applications
392
ICP/MS Multi-Element
393-396
Organometallics (Wear Metals)
397-404
Lubricating Oils
402-404
Inorganic ASTM Methods
405
Solid Matrix
406-408
Periodic Table of Elements, Unit Conversions, etc.
409-410
Art Gallery
411
Indices: Catalog Number, CAS Number, Organic Analyte
412-440
Custom Quotation Form, and Contact / Ordering Information
Back Pages
About the Cover
Alchemist in his Workshop
David Teniers II (Antwerp 1610-1690)
Courtesy of the Chemical Heritage Foundation Collections, and Roy Eddleman,
Oil on Canvas
Photograph by Will Brown
This painting is a depiction of an alchemist working at the bellows
in his cluttered laboratory. In this work, the mixture of the magical
aspects of alchemy (the hanging animal) mix with the more practical
aspects of chemistry (the many distillation units near the hearth).
Although alchemists were often looked upon as “crackpots” or
charlatans, many of their experiments and theories led to modern
chemistry.
Officers
Mike Bolgar
CEO
Amy Harvey
President
Susan Meronek
General Manager
Matt Bolgar
VP
Technical Service
ii
Eric D.
Manager, New Product
Development
Bob U.
Organic Technical
Quotation Specialist
Johanna G.
Organic Technical
Quotation Specialist
Lee M.
Organic Technical
Quotation Specialist
Tom A.
Inorganic
Product Manager
Danielle L.
Inorganic Technical
Quotation Specialist
Jack Hubball
Technical Director
Customer Service
Sheila M.
Organic Technical
Quotation Specialist
Carol W.
Office Manager
Susan C.
Customer Service Rep.
Viola P.
Customer Service Rep.
Accounts Receivable
Patty S.
Customer Service Rep.
Lisa Z.
Customer Service Rep.
Lisette P.
Customer Service Rep.
About Us
Founded in 1986, AccuStandard has grown from two to the current team of 65 people. The company started in a small business
incubator co-sponsored by Yale University, The City of New Haven and the State of Connecticut at the former site of Olin
Chemical Company in New Haven, Connecticut, USA. Outgrowing that facility, AccuStandard moved across town in 1998 into a
fully modernized facility of 37,000 square feet of laboratories, office and storage space. AccuStandard is now one of the leading
companies in the field of Chemical Reference Standards.
AccuStandard ships products to over 108 countries and maintains a distributor network in 65 of those countries. Since its beginning,
the product line has grown to include over 11,000 Reference Standard products and twice that number of special formulations
which have been developed for specific customer needs. Standards include those for analysis of the most important EPA Methods,
Pesticide Residue Screening, Flame Retardants, Biofuels, Plastic Additives, Dyes, Explosives, UOP and ASTM Methods and upgraded products for PIANO and Physical Property analyses.
The company is renowned for its recognition and speedy introduction of Standards to the market place. The company’s unparalleled
Synthesis Department gives us the opportunity to synthesize important and unique products and product lines. Featured, also in its
history of firsts, are all of the 209 congeners of polychlorinated biphenyls (PCBs), 205 out of the 209 congeners of Polybrominated
diphenyl ethers (PBDEs) as well as many halogenated dioxins and dibenzofurans, PAHs and pesticides.
Among the more recent introductions are the hydroxy and methoxy PBDE congeners as well as mixed bromo/chloro hydroxy and
methoxy diphenyl ethers, fluorinated PBDE congeners (used as internal standards), organophosphate flame retardants, biofuels,
plastic additives (AccuStandard authored a CRC Press Handbook), EPA Method 535 pesticide derivatives and previously unavailable
explosives.
AccuStandard’s quality system is accredited to ISO Guide 34, ISO/IEC 17025 and certified to ISO 9001.
AccuStandard owes its success in large part to the excellence, loyalty and dedication of its staff. We look forward to serving our
customers for many years to come.
AccuStandard, At Your Service
Synthesis
Organic and Inorganic Production
Assembly / Shipping
Organic and Inorganic Quality Control
AccuStandard.com
iii
AccuStandard’s Quality Resources
■ On-Going Stability Program for understanding of
chemical interactions
■ Complete range of instrumentation: Programable
pulse inert inlet high resolution GC/MS, GC/MS, GC/
ECD, GC/FID, GC/NPD, LC/MS/MS, HPLC, XOS
Sulfur analyzer, Antek 9000 sulfur analyzer, Physical
Standards instruments for Flash Point, Distillation,
Cloud Point, Freeze Point, Aniline Point, Pour Point,
Vapor Pressure. Plus ICP, ICP/MS, Karl Fischer,
IC with ion suppression conductivity detector, ion
selective electrodes, auto polarimeter and others.
■ Monthly internal meetings for formal failure analysis of
any non-conformances.
■ ISO Guide 34, ISO/IEC 17025 and ISO 9001
Agilent 1100/120 Series LC/MS/MS System
iv
Custom Services
Custom Synthesis
The AccuStandard Synthesis Department employs several PhD. Organic Chemists with many years of pertinent academic and industrial experience.
The experienced staff has developed hundreds of pure chemical compounds for companies and governmental agencies around the world. The
very well-equipped synthetic laboratory, with significant analytical support has made many notable synthesis projects possible. We specialize in
synthesizing chemicals of high purity to be used as reference standards, and also offer custom synthesis capability on milligram to kilogram scales.
Custom Synthesized Products
Analytical Capabilities
■■ GC-MS, GC-FID, GC-ECD, GC-NPD
■■ HPLC, LC-MS
■■ ICP, ICP-MS
■■ access to more anlytical instrumentation if
necessary
Synthesis and Purification
■■ Milligram to Kilogram Glassware
■■ Inert Conditions Equipment
■■ High Performance Flash Chromatography
■■ Distillation Equipment - High Vacuum,
Molecular (Kugelrohr), and Spinning Band
Columns Preparative TLC
■■ Parr Pressure and Hydrogenation Reactor
■■ PCBs (all 209 congeners), & hydroxy, methoxy, and
methylsulfonyl metabolites
■■ Halo-Dibenzodioxins and Furans
■■ PBDEs (205 out of 209 congeners) & hydroxy, methoxy,
and chloro metabolites
■■ Fluorinated PBDEs
■■ Other Brominated Flame Retardants
■■ PBBs
■■ PAHs, Nitro-PAHs, Methyl-PAHs
■■ Pesticides and metabolites
■■ Explosives and metabolites
■■ Nonyl- and Octylphenol Ethoxylates
■■ Mono- and Diester Phthalates
■■ Organophosphates
■■ Other Rare Chemicals
AccuStandard is renowned for its quick response to the needs for new compounds. The company’s especially strong Synthesis Department allows
the synthesis of important and unique products. Featured in its history of firsts, are all of the 209 congeners of polychlorinated biphenyls (PCBs), 205
out of the 209 congeners of polybrominated diphenyl ethers (PBDEs) as well as many halogenated dioxins and dibenzofurans, PAHs, pesticides and
fluorinated surrogates substituting the expensive isotopically labelled compounds.
Among the more recent introductions are the hydroxy and methoxy PBDE congeners, mixed bromo/chloro hydroxy and methoxy diphenyl ethers,
organophosphate flame retardants, biofuels, plastic additives (AccuStandard authored the Handbook for the Chemical Analysis of Plastic and Polymer
Additives published by CRC Press), EPA Method 535 pesticide derivatives and previously unavailable explosive standards.
Custom Formulations
With over 30,000+ custom and 10,000+ listed standards, there is a good chance that AccuStandard
will have a standard to meet your needs. However, if your laboratory requires something specific, our
Chemists will manufacture a Custom Standard to meet your unique requirements. Custom Standards are
an economical and time saving way to have a Standard prepared for your individual needs.
Custom QC options
1. Gravimetric/Volumetric Certification: Each purity is measured gravimetrically and QC verified
instrumentally (where available). Every component in the Standard is guaranteed to be within +/0.5% of the requested value unless otherwise stated on the Certificate of Analysis. The solutions
are diluted to volume using Class A glassware. A Certificate of Analysis accompanies each
Standard and documents the gravimetric values used.
2. Full Quantitative Certification: This QA/QC method includes extended GC analysis using both
internal calibration standards plus statistical analysis. A data package containing analytical and
gravimetric data can be provided if requested during the quotation phase (Organic Customs only).
Custom Packaging and Bulk Quantity Requirements
AccuStandard has the resources and equipment to meet your custom
packaging requirements.
■■ Automated ampule filling & sealing 0.2 mL up to 20 mL and
ampule sizes from 1 mL to 20 mL
■■ Quantities from 500 to over 500,000 ampules
■■ Homogeneity testing
■■ Amber ampules for added product stability
■■ Private labeling and packaging (OEM)
We can reduce your costs using the Cozzoli Auto
Filling/Sealing Machine to package just the right
size product for your application. OEM Standards Privately labeled standards manufactured and tested
to your specifications. Cold and under Nitrogen
sealing available.
AccuStandard.com
v
Quality System
ISO Guide 34 • ISO/IEC 17025 • ISO 9001
How AccuStandard Ensures the Best Quality in the Industry
Approved Vendors
Synthesis
AccuStandard has an established
network of qualified vendors that
supply raw materials that we do not
synthesize.
AccuStandard can custom synthesize
materials not available from other
commercial sources. Synthesis is
treated as an approved vendor.
Incoming Inspection
All materials are inspected
for appearance, integrity &
documentation upon receipt.
Production
All batches are quantitatively prepared
and documented to ensure traceability
of all analytes.
Quality Control
Inventory
1. QC certifies the incoming
material prior to release to
Production.
2. QC validates the product that
Production makes.
3. QC performs on-going stability
checks of existing inventory to
ensure product integrity.
4. Provides support to customers
experiencing difficulties.
Products in Inventory are properly
controlled to ensure long term
stability.
Shipping
Packaging Requirements Proper
Shipping Regulations
Customer
Customer Service
Provides service for all non-technical
questions a customer may have.
Technical Service
Provides technical support and custom
quotations for our customers.
Visit our website at for a copy of the latest Certificates.
vi
Certificate of Analysis
Sample: multi-component organic COA
Accreditation
Compounds assembled into a standard based on
method requirements and customer formulation
request - but all reviewed for solubilty and
coelution potential prior to manufacture.
CAS Number to
easily identify
compound
We use only high
purity starting
material.
Concentration calculated by using the
purity of the starting material
NIST Tracebility
Uncertainty Values
The uncertainty values as stated on our Certificate of Analysis have been determined using the
EURACHEM/CITAC Guide (Quantifying Uncertainty in Analytical Measurement). We have evaluated
both Type A (based on a series of observations) and Type B (manufacturers specifications and calibration
data) factors and report a combined expanded uncertainty.
Although uncertainty relates to the general concept of doubt, uncertainty of measurement does
not imply doubt about the validity of a measurement, but rather increased confidence in the validity
of a measurement result. Uncertainty takes the form of a range and cannot be used to correct a
measurement result. The uncertainty of the result should never be interpreted as representing the error
itself, or the error remaining after correction.
AccuStandard.com
QC management approval
vii
Technical Reference Books
Analytical Chemistry of
PCBs
Technical Reference Books
Physical, Spectra,
and Chromatographic
Properties of all
209 Individual PCB
Congeners
AccuStandard’s FT/IR, Mass
Spectral data, melting point and
chromatographic information along
with chromatographic data from
George Frame’s study is available in
this book.
Our own PCB Book
PCB Book
Physical, Spectral and Chromatographic Properties of all 209
Congeners.
BOOK-PCB-002
$ 25
Analytical Chemistry of PCBs
BOOK-PCB-001
$ 225
Handbook for the
Chemical Analysis of
Plastic and Polymer
Additives
Total Petroleum
Hydrocarbon Pattern
Recognition Standards
TPH Book
Total Petroleum Hydrocarbon
Pattern Recognition Standards
BOOK-TPH-001
$ 30
This book contains chromatography
for the various petroleum products
typically found during LUFT/LUST
site investigations. The chromatography shows each fuel pattern in
a 25 minute analytical run for early
eluting petroleum products like
gasoline to late eluting products like
motor oil. In addition, an n-alkane
standard analyzed under identical
conditions has been overlaid on
each petroleum product chromatogram. Use of the book will assist the
chemist’s identification of the fuel for
pattern recognition.
The n-alkane standard overlay
provides n-alkane reference points
between the standard and the
unknown sample. These beginning
and ending n-alkane reference
points can be used to establish
gross hydrocarbon concentrations.
By comparing the specific n-alkane
range of the closest identified
petroleum standard to that of the
unknown sample a reproducible
gross hydrocarbon number can be
achieved.
This book, published by CRC
Press, contains a host of analytical
reference data for each of the many
common plastics and polymer
additives. Each of the compounds
is also offered by AccuStandard as a
certified reference material, most in
both neat and solution form, making
comparison of the analytical results
easier.
Plastics Book
For the Chemical Analysis
of Plastic and Polymer Additives
BOOK-PLAS-001
$ 250
Second Edition
Coming soon!
Additional reference information, such as the full text of select
EPA Methods and EU Directives, can be found on our Website.
viii
Second Edition of Dr. Erickson’s
Analytical Chemistry of PCBs
appears a decade after the first
and is completely revised and
updated. The changes from the
First Edition reflect the significant
growth in the area and a growing
appreciation of the importance of
PCB analysis to our culture. This
book is a comprehensive review of
the analytical chemistry of PCBs.
It is part history, part annotated
bibliography, part comparison,
and part guidance. Featuring a
new chapter on analyst/customer
interactions and several new
appendices, the Second Edition is an
invaluable resource for both chemists
with no experience in PCB analysis
and seasoned PCB researchers.
Each compound has:(where
applicable)
■ Chemical Information
■ Structure
■ CAS Number
■ RTECS Number
■ Formula
■ Molecular Weight
■ IUPAC Name, other common
names and popular brand names
■ Physical Properties
■ Appearance
■ Melting and Boiling Points
■ Stability
■ Solubilities in several common
solvents
■ Application
■ Regulatory
■ Environmental Impact
■ Point of Release
■ Toxicological Data
■ Analytical Data
■ Mass Spectrum with key Ions
tabulated
■ Chromatogram with conditions
■ Other Important Information
AccuStandard is accredited to ISO Guide 34, ISO/IEC 17025 and certified to ISO 9001
Request our Periodic Table of Elements
(20 x 20 inch laminated poster)
With references, such as unit conversions, general constants,
element symbols, atomic weights and solvent miscibility table with
densities and boiling points.
Try our Inorganic Alternate Source Line and receive a FREE Periodic Table of Elements. *.
Buy over $ 250 of any standard and receive a FREE Periodic Table of Elements. *
* Please request when ordering.
AccuStandard
Periodic Table of Elements
1
IA
1.00794
®
LeaderinAnalyticalChemicalReferenceStandards
Tel.203-786-5290•www.AccuStandard.com
18VIIIA
ATOMICWEIGHT
1
H
4.002602
PHYSICALSTATE
SYMBOL
1s
bp: -252.9˚C
d: 0.089 g/l
Hydrogen
6.941
3
SOLID
LIQUID
NATURAL
RADIOACTIVE
ARTIFICIAL
RADIOACTIVE
IIA
9.012182
BOILINGORMELTINGPOINT
4
Li Be
13 IIIA 14 IVA 15
10.811
5
B
12.011
6
C
VA 16 VIA 17 VIIA
14.00674
7
N
15.9994
8
O
18.9984032
9
F
[He] 2s
mp: 180.5˚C
d: 0.53 g/cc
[He] 2s2
mp: 1287˚C
d: 1.848 g/cc
[He] 2s2 2p
mp: 2075˚C
d: 2.34 g/cc
[He] 2s22p2
mp: 3650˚C
d: 2.26 g/cc
[He] 2s22p3
bp: -195.8˚C
d: 1.25 g/l
[He] 2s22p4
bp: -183.0˚C
d: 1.404 g/l
[He] 2s22p5
bp: -188.1˚C
d: 1.696 g/l
Lithium
Beryllium
Boron
Carbon
Nitrogen
Oxygen
Fluorine
22.989768
11
24.3050
[Ne] 3s
mp: 97.72˚C
d: 0.968 g/cc
[Ne] 3s2
mp: 650˚C
d: 1.738 g/cc
Sodium
Magnesium
19
DENSITY
12
Na Mg
39.0983
40.078
20
26.981539
3IIIB 4
44.955910
21
IVB 5
47.88
22
VB 6
50.9415
V
23
VIB 7 VIIB 8
51.9961
24
13
Al
ELEMENTNAME
K Ca Sc Ti
54.93805
25
VIII 9
55.847
26
VIII 10 VIII 11
58.93320
27
58.6934
28
IB 12
63.546
29
IIB
65.38
30
28.0855
14
Si
30.973762
P
15
32.066
S
16
35.4527
17
[Ne] 3s2 3p
mp: 660.4˚C
d: 2.70 g/cc
[Ne] 3s2 3p2
mp: 1414˚C
d: 2.33 g/cc
[Ne] 3s2 3p3
mp: 44.2˚C
d: 1.82 g/cc
[Ne] 3s2 3p4
mp: 115.21˚C
d: 2.07 g/cc
[Ne] 3s2 3p5
bp: -34.0˚C
d: 2.95 g/l
Aluminum
Silicon
Phosphorus
Sulfur
Chlorine
69.723
31
72.61
32
74.92159
33
78.96
34
79.904
35
[Ar] 4s2
mp: 842˚C
d: 1.54 g/cc
[Ar] 3d 4s2
mp: 1541˚C
d: 2.989 g/cc
[Ar] 3d2 4s2
mp: 1668˚C
d: 4.506 g/cc
[Ar] 3d3 4s2
mp: 1910˚C
d: 6.11 g/cc
[Ar] 3d5 4s
mp: 1907˚C
d: 7.19 g/cc
[Ar] 3d5 4s2
mp: 1246˚C
d: 7.3 g/cc
[Ar] 3d6 4s2
mp: 1538˚C
d: 7.87 g/cc
[Ar] 3d7 4s2
mp: 1495˚C
d: 8.92 g/cc
[Ar] 3d8 4s2
mp: 1455˚C
d: 8.908 g/cc
[Ar] 3d10 4s
mp: 1083.0˚C
d: 8.84 g/cc
[Ar] 3d10 4s2
mp: 419.5˚C
d: 7.14 g/cc
[Ar] 3d10 4s2 4p
mp: 29.8˚C
d: 5.91 g/cc
[Ar] 3d10 4s2 4p2
mp: 937.2˚C
d: 5.32 g/cc
[Ar] 3d10 4s2 4p3
818˚C subl.
d: 5.778 g/cc
[Ar] 3d10 4s2 4p4
mp: 217˚C
d: 4.28 g/cc
[Ar] 3d10 4s2 4p5
bp: 59.47˚C
d: 3.10 g/cc
Calcium
Scandium
Titanium
Vanadium
Chromium
Manganese
Iron
Cobalt
Nickel
Copper
Zinc
Gallium
Germanium
Arsenic
Selenium
Bromine
87.62
38
Rb Sr
88.90585
Y
39
91.224
40
92.9064
41
95.94
42
98
43
101.07
44
102.9055
45
106.42
46
107.868
47
112.411
48
114.818
49
118.710
50
121.75
51
127.60
52
Zr Nb Mo Tc Ru Rh Pd Ag Cd In Sn Sb Te
126.9045
53
I
[Kr] 5s
mp: 39˚C
d: 1.532 g/cc
[Kr] 5s2
mp: 777˚C
d: 2.64 g/cc
[Kr] 4d 5s2
mp: 1522˚C
d: 4.47 g/cc
[Kr] 4d2 5s2
mp: 1855˚C
d: 6.52 g/cc
[Kr] 4d4 5s
mp: 2477˚C
d: 8.57 g/cc
[Kr] 4d5 5s
mp: 2623˚C
d: 10.22 g/cc
[Kr] 4d5 5s2
mp: 2157˚C
d: 11.0 g/cc
[Kr] 4d7 5s
mp: 2334˚C
d: 12.1 g/cc
[Kr] 4d8 5s
mp: 1964˚C
d: 12.41 g/cc
[Kr] 4d10
mp: 1554.9˚C
d: 12.02 g/cc
[Kr] 4d10 5s
mp: 961.8˚C
d: 10.5 g/cc
[Kr] 4d10 5s2
mp: 321.1˚C
d: 8.69 g/cc
[Kr] 4d10 5s2 5p
mp: 156.6˚C
d: 7.31 g/cc
[Kr] 4d10 5s2 5p2
mp: 232.0˚C
d: 7.265 g/cc
[Kr] 4d10 5s2 5p3
mp: 630.7˚C
d: 6.68 g/cc
[Kr] 4d10 5s2 5p4
mp: 449.5˚C
d: 6.24 g/cc
[Kr] 4d10 5s2 5p5
mp: 113.7˚C
d: 4.933 g/cc
Rubidium
Strontium
Yttrium
Zirconium
Niobium
Molybdenum
Technetium
Ruthenium
Rhodium
Palladium
Silver
Cadmium
Indium
Tin
Antimony
Tellurium
Iodine
132.9054
55
137.327
56
57-71
178.49
72
180.9479
10
Ne
[He] 2s22p6
bp: -246.1˚C
d: 0.8999 g/l
Neon
39.948
18
[Ne] 3s2 3p6
bp: -185.9˚C
d: 1.784 g/l
Argon
83.80
36
Cr Mn Fe Co Ni Cu Zn Ga Ge As Se Br Kr
[Ar] 4s
mp: 63.3˚C
d: 0.856 g/cc
37
Helium
20.1797
Cl Ar
Potassium
85.4678
1s2
bp: -268.9˚C
d: 0.179 g/l
GAS
ELECTRONCONFIGURATION
2
2
He
ATOMICNUMBER
73
183.84
74
186.207
75
190.23
76
192.22
77
195.08
78
196.96654
79
200.59
80
204.3833
81
207.2
82
208.98037
83
208.9824
84
209.9871
[Ar] 3d10 4s2 4p6
bp: -157.36˚C
d: 3.677 g/cL
Krypton
131.29
54
Xe
[Kr] 4d10 5s2 5p6
mp: -111.0˚C
d: 5.761 g/l
Xenon
85
222.0176
86
Cs Ba La- Hf Ta W Re Os Ir Pt Au Hg Tl Pb Bi Po At Rn
Lu
Fr Ra Ac- Rf Db Sg Bh Hs Mt Ds Rg Cn
Lr
[Xe] 6s
mp: 28.4˚C
d: 1.93 g/cc
[Xe] 6s2
mp: 727˚C
d: 3.62 g/cc
[Xe] 4f14 5d2 6s2
mp: 2227˚C
d: 13.31 g/cc
[Xe] 4f14 5d3 6s2
mp: 2996˚C
d: 16.4 g/cc
[Xe] 4f14 5d4 6s2
mp: 3410˚C
d: 19.3 g/cc
[Xe] 4f14 5d5 6s2
mp: 3180˚C
d: 20.8 g/cc
[Xe] 4f14 5d6 6s2
mp: 3045˚C
d: 22.61 g/cc
[Xe] 4f14 5d7 6s2
mp: 2410˚C
d: 22.5 g/cc
[Xe] 4f14 5d9 6s
mp: 1768.4˚C
d: 21.45 g/cc
[Xe] 4f14 5d10 6s
mp: 1064.2˚C
d: 19.32 g/cc
[Xe] 4f14 5d10 6s2
bp: 356.73˚C
d: 13.534 g/cc
[Xe] 4f14 5d10 6s2 6p
mp: 303.5˚C
d: 11.85 g/cc
[Xe] 4f14 5d10 6s2 6p2
mp: 327.5˚C
d: 11.34 g/cc
[Xe] 4f14 5d10 6s2 6p3
mp: 271.4˚C
d: 9.79 g/cc
[Xe] 4f14 5d10 6s2 6p4
mp: 254˚C
d: 9.20 g/cc
[Xe] 4f14 5d10 6s2 6p5
mp: 302˚C
d: none
[Xe] 4f14 5d10 6s2 6p6
mp: -61.8˚C
d: 9.72 g/cc
Cesium
Barium
Hafnium
Tantalum
Tungsten
Rhenium
Osmium
Iridium
Platinum
Gold
Mercury
Thallium
Lead
Bismuth
Polonium
Astatine
Radon
223.0197
87
226.0254
88
89-103
261.1087
104
262.1138
105
263.1182
106
262.1229
107
265
108
266
109
269
110
280
111
285
112
[Rn] 7s
mp: 27˚C
d: 2.29 g/cc
[Rn] 7s2
mp: 700˚C
d: 2.29 g/cc
[Rn] 5f14 6d2 7s2
mp: none
d: none
[Rn] 5f14 6d3 7s2
mp: none
d: none
[Rn] 5f14 6d4 7s2
mp: none
d: none
[Rn] 5f14 6d5 7s2
mp: none
d: none
[Rn] 5f14 6d6 7s2
mp/bp: none
d: none
[Rn] 5f14 6d7 7s2
mp/bp: none
d: none
mp/bp: none
d: none
mp/bp: none
d: none
mp/bp: none
d: none
Francium
Radium
Rutherfordium
Dubnium
Seaborgium
Bohrium
Hassium
Meitnerium
Darmstadtium
Roentgenium
Copernicium
138.9055
57
140.115
58
140.90765
59
144.24
60
146.9151
61
150.36
62
151.965
63
157.25
64
158.92534
65
162.50
66
164.93032
67
167.26
68
168.9342
69
173.04
70
174.967
71
La Ce Pr Nd Pm Sm Eu Gd Tb Dy Ho Er Tm Yb Lu
[Xe] 5d 6s2
mp: 920˚C
d: 6.17 g/cc
[Xe] 4f2 6s2
mp: 798˚C
d: 6.77 g/cc
[Xe] 4f3 6s2
mp: 935˚C
d: 6.77 g/cc
[Xe] 4f4 6s2
mp: 1021˚C
d: 7.00 g/cc
[Xe] 4f5 6s2
mp: 1080˚C
d: 7.22 g/cc
[Xe] 4f6 6s2
mp: 1072˚C
d: 7.54 g/cc
[Xe] 4f7 6s2
mp: 822˚C
d: 5.25 g/cc
[Xe] 4f7 5d 6s2
mp: 1311˚C
d: 7.89 g/cc
[Xe] 4f9 6s2
mp: 1356˚C
d: 8.27 g/cc
[Xe] 4f10 6s2
mp: 1409˚C
d: 8.56 g/cc
[Xe] 4f11 6s2
mp: 1474˚C
d: 8.78 g/cc
[Xe] 4f12 6s2
mp: 1529˚C
d: 9.05 g/cc
[Xe] 4f13 6s2
mp: 1545˚C
d: 9.32 g/cc
[Xe] 4f14 6s2
mp: 819˚C
d: 6.97 g/cc
Lanthanum
Cerium
Praseodymium
Neodymium
Promethium
Samarium
Europium
Gadolinium
Terbium
Dysprosium
Holmium
Erbium
Thulium
Ytterbium
227.0278
89
232.0381
90
231.0359
91
Ac Th Pa
238.0289
92
244.0642
94
243.0614
95
247.0703
96
247.0703
97
251.0796
98
252.0829
99
257.0951
100
258.0986
101
259.1009
102
Lutetium
262.11
103
[Rn] 6d 7s2
mp: 1050˚C
d: 10.07 g/cc
[Rn] 6d2 7s2
mp: 1750˚C
d: 11.72 g/cc
[Rn] 5f2 6d 7s2
mp: 1560˚C
d: 15.37 g/cc
[Rn] 5f3 6d 7s2
mp: 1132.3˚C
d: 19.07 g/cc
[Rn] 5f4 6d 7s2
mp: 637˚C
d: 20.45 g/cc
[Rn] 5f6 7s2
mp: 641˚C
d: 19.86 g/cc
[Rn] 5f7 7s2
mp: 1173˚C
d: 13.67 g/cc
[Rn] 5f7 6d 7s2
mp: 1345˚C
d: 13.51 g/cc
[Rn] 5f9 7s2
mp: 986˚C
d: 14.78 g/cc
[Rn] 5f10 7s2
mp: 900˚C
d: 15.1 g/cc
[Rn] 5f11 7s2
mp: 860˚C
d: 8.84 g/cc
[Rn] 5f12 7s2
mp: none
d: none
[Rn] 5f13 7s2
mp: none
d: none
[Rn] 5f14 7s2
mp: none
d: none
[Rn] 5f14 6d 7s2
mp: none
d: none
Actinium
Thorium
Protactinium
Uranium
Neptunium
Plutonium
Americium
Curium
Berkelium
Californium
Einsteinium
Fermium
Mendelevium
Nobelium
Lawrencium
R = 0.0821 (Atm)(L)/(K)(mole)
g = 32.17 ft/sec2, 9.8 m/sec2
N = 6.023 x 1023 molecules/mole
c = 186,282 miles/sec, 3 x 1010 cm/sec
ΔHfus = 79.7 cal/g
ΔHvap = 540 cal/g
22.4L/mol at 0˚C, 760 torr
F = 96485.31 C/mol
h = 6.626 x 10-27 erg/sec
2d nλ = 2d sin(λ)
-273.15˚C
-195.8˚C
Table of Element Symbol, Atomic Weights and ICP Catalog Numbers
Element
Actinium
Aluminum
Americium
Antimony
Argon
Arsenic
Astatine
Barium
Berkelium
Beryllium
Bismuth
Bohrium
Boron
Bromine
Cadmium
Calcium
Californium
Carbon
Cerium
Cesium
Chlorine
Chromium
Cobalt
Copper
Curium
Dubnium
Dysprosium
Einsteinium
Erbium
Symbol
Ac
Al
Am
Sb
Ar
As
At
Ba
Bk
Be
Bi
Bh
B
Br
Cd
Ca
Cf
C
Ce
Cs
Cl
Cr
Co
Cu
Cm
Db
Dy
Es
Er
Atomic
Weight
227.0278
26.981539
243.0614
121.757
39.948
74.92159
209.9871
137.327
247.0703
9.012182
208.98037
262.1229
10.811
79.904
112.411
40.078
251.0796
12.011
140.115
132.90543
35.4527
51.9961
58.93320
63.546
247.0703
262.1138
162.50
252.0829
167.26
Cat.No.
ICP
ICP-01N
ICP-02N
ICP-03N
ICP-04N
ICP-05N
ICP-06N
ICP-07W
ICP-08N
ICP-09N
ICP-11N
ICP-12N
ICP-13N
ICP-14N
ICP-15N
ICP-16N
ICP-17N
Element
Europium
Fermium
Fluorine
Francium
Gadolinium
Gallium
Germanium
Gold
Hafnium
Hassium
Helium
Holmium
Hydrogen
Indium
Iodine
Iridium
Iron
Krypton
Lanthanum
Lawrencium
Lead
Lithium
Lutetium
Magnesium
Manganese
Meitnerium
Mendelevium
Mercury
Molybdenum
Symbol
Eu
Fm
F
Fr
Gd
Ga
Ge
Au
Hf
Hs
He
Ho
H
In
I
Ir
Fe
Kr
La
Lr
Pb
Li
Lu
Mg
Mn
Mt
Md
Hg
Mo
Atomic
Cat.No.
Weight
ICP
151.96
ICP-18N
257.0951
18.9984032
223.0197
157.25
ICP-19N
69.723
ICP-20N
72.61
ICP-21W
196.96654 ICP-22H
178.49
ICP-23N
265
4.002602
164.93032 ICP-24N
1.00794
114.818
ICP-25N
126.9045
192.22
ICP-26H
55.847
ICP-27N
83.80
138.9055 ICP-28N
262.11
207.2
ICP-29N
6.941
ICP-30N
174.967
ICP-31N
24.3050
ICP-32N
54.93805 ICP-33N
266
258.0986
200.59
ICP-34N
95.94
ICP-35W
Element
Neodymium
Neon
Neptunium
Nickel
Niobium
Nitrogen
Nobelium
Osmium
Oxygen
Palladium
Phosphorus
Platinum
Plutonium
Polonium
Potassium
Praseodymium
Promethium
Protactinium
Radium
Radon
Rhenium
Rhodium
Rubidium
Ruthenium
Rutherfordium
Samarium
Scandium
Seaborgium
Selenium
Symbol
Nd
Ne
Np
Ni
Nb
N
No
Os
O
Pd
P
Pt
Pu
Po
K
Pr
Pm
Pa
Ra
Rn
Re
Rh
Rb
Ru
Rf
Sm
Sc
Sg
Se
Atomic
Weight
144.24
20.1797
237.0482
58.6934
92.9064
14.00674
259.1009
190.23
15.9994
106.42
30.973762
195.08
244.0642
208.9871
39.0983
140.9151
146.9151
231.0359
226.0254
222.0176
186.207
102.9055
85.4678
101.07
261.1087
150.36
44.95591
263.1182
78.96
Cat.No.
ICP
ICP-36N
ICP-37N
ICP-38W
ICP-40H
ICP-41W
ICP-42H
ICP-43N
ICP-44N
ICP-45W
ICP-46H
ICP-47N
ICP-48H
Solvent Miscibility Table, Density and Boiling Point
Element
Silicon
Silver
Sodium
Strontium
Sulfur
Tantalum
Technetium
Tellurium
Terbium
Thallium
Thorium
Thulium
Tin
Titanium
Tungsten
Uranium
Vanadium
Xenon
Ytterbium
Yttrium
Zinc
Zirconium
Symbol
Si
Ag
Na
Sr
S
Ta
Tc
Te
Tb
Tl
Th
Tm
Sn
Ti
W
U
V
Xe
Yb
Y
Zn
Zr
Atomic
Weight
28.0855
107.8682
22.989768
87.62
32.066
180.9479
98
127.6
158.92534
204.3833
232.0381
168.9342
118.710
47.88
183.84
238.0289
50.9415
131.29
173.04
88.90585
65.38
91.224
Cat.No.
ICP
ICP-52W
ICP-53N
ICP-54N
ICP-55N
ICP-56W
ICP-57W
ICP-58H
ICP-59N
ICP-60N
ICP-61N
ICP-62N
ICP-63N
ICP-64W
ICP-65W
ICP-66N
ICP-67N
ICP-68N
ICP-69N
ICP-70N
ICP-71N
ICP-49N
ICP-50N
ICPCatalogNumberKey
Matrix:
1000 µg/mL, 10,000 µg/mL (-10X)
Unit:
100 mL (-1), 500 mL (-5), -0.5 (50 mL)
ICP-51N
Example:
ICP-01N-1 (Al, in Nitric acid, 1000 µg/mL, 100 mL)
ICP-07W-10X-5 (B, in Water, 10,000 µg/mL, 500 mL)
Aceticacid(1.049g/mL)(117-118ºC)
Acetone(0.791g/mL)(56ºC)
Acetonitrile(AcCN)(0.786g/mL)(81-82ºC)
Benzene(0.874g/mL)(80ºC)
2-Butanol(0.808g/mL)(98ºC)
Butylalcohol(0.81g/mL)(116-118ºC)
tert-Butylmethylether(MtBE)(0.74g/mL)(55-56ºC)
Carbontetrachloride(1.594g/mL)(76-77ºC)
Chloroform(1.492g/mL)(60.5-61.5ºC)
Cyclohexane(0.779g/mL)(80.7ºC)
Cyclopentane(0.751g/mL)(50ºC)
Dichloroethane(1.256g/mL)(83ºC)
N,N-Dimethylformamide(DMF)(0.944g/mL)(153ºC)
1,4-Dioxane(1.034g/mL)(100-102ºC)
Dipropylether(0.736g/mL)(88-90ºC)
Ethylacetate(EtOAc)(0.902g/mL)(76.5-77.5ºC)
Ethylalcohol(EtOH)(0.789g/mL)(78ºC)
Ethylether(0.706g/mL)(34.6ºC)
n-Heptane(0.684g/mL)(98ºC)
n-Hexane(0.659g/mL)(69ºC)
Isooctane(0.692g/mL)(98-99ºC)
Isopropylalcohol(0.785g/mL)(82ºC)
Methanol(MeOH)(0.791g/mL)(64.7ºC)
Methylenechloride(CH2Cl2)(1.325g/mL)(39.8-40ºC)
Methylsulfoxide(DMSO)(1.10g/mL)(189ºC)
n-Pentane(0.626g/mL)(35-36ºC)
1,1,2,2-Tetrachloroethane(1.586g/mL)(147ºC)
Tetrahydrofuran(THF)(0.889g/mL)(65-67ºC)
Toluene(0.865g/mL)(110-111ºC)
Trichloroethane(1.336g/mL)(74-76ºC)
Water(1g/mL)(100ºC)
Xylene(0.868g/mL)(138-139ºC)
Technical Reference
1 ppm = 1 µg/mL (wt. /vol.) and
1 ppm = 1 µg/g (wt./wt.)
1% = 10,000 ppm (parts per million)
1 ppm = 1,000 ppb (parts per billion)
1 ppb = 1,000 ppt (parts per trillion)
1 g = 1,000 mg (milligram)
1 mg = 1,000 µg (microgram)
1 µg = 1,000 ng (nanogram)
1 L = 1,000 mL (milliLiter)
1 mL = 1,000 µL (microLiter)
1 µL = 1,000 nL (nanoLiter)
General Constants
Universal Gas Constant
Acceleration Due to Gravity
Avogadro’s Constant
Speed of Light
Heat of Fusion (water 1 atm, 0˚C)
Heat of Vaporization (water 1 atm, 100˚C)
Volume of Perfect Gas
Faraday’s Constant
Planck’s Constant
Bragg’s Law
Absolute Zero
Temp. of Liquid Nitrogen
93
U Np Pu Am Cm Bk Cf Es Fm Md No Lr
Unit Conversions
Temperature
˚Fahrenheit
˚Celsius
(˚F - 32) x 5/9
˚Celsius
˚Fahrenheit (˚C x 9/5) + 32
˚Celsius
˚Kelvin
˚C + 273
Mass
1 ounce
= 28.4 grams
0.03527 grams = 1 ounces
LiquidVolume
Multiplyby
Ounces (US) Milliliters
29.57
Pints (US)
Liters
0.47
Quarts (US)
Liters
0.95
Gallons (US) Liters
3.8
Milliliters
Ounces (US)
0.034
Liters
Pints (US)
2.1
Liters
Quarts (US)
1.06
Liters
Gallons (US)
0.26
237.0482
[Xe] 4f14 5d 6s2
mp: 1663˚C
d: 9.84 g/cc
Technical Reference
Solvent Miscibility Table, Density and Boiling Point
Acetic acid (1.049 g/mL) (117-118ºC)
Acetone (0.791 g/mL) (56ºC)
Acetonitrile (AcCN) (0.786 g/mL) (81-82ºC)
Benzene (0.874 g/mL) (80ºC)
2-Butanol (0.808 g/mL) (98ºC)
Butyl alcohol (0.81 g/mL) (116-118ºC)
tert-Butylmethyl ether (MtBE) (0.74 g/mL) (55-56ºC)
Carbon tetrachloride (1.594 g/mL) (76-77ºC)
Chloroform (1.492 g/mL) (60.5-61.5ºC)
Cyclohexane (0.779 g/mL) (80.7ºC)
Cyclopentane (0.751 g/mL) (50ºC)
Dichloroethane (1.256 g/mL) (83ºC)
N,N-Dimethylformamide (DMF) (0.944 g/mL) (153ºC)
1,4-Dioxane (1.034 g/mL) (100-102ºC)
Dipropyl ether (0.736 g/mL) (88-90ºC)
Ethyl acetate (EtOAc) (0.902 g/mL) (76.5-77.5ºC)
Ethyl alcohol (EtOH) (0.789 g/mL) (78ºC)
Ethyl ether (0.706 g/mL) (34.6ºC)
n-Heptane (0.684 g/mL) (98ºC)
n-Hexane (0.659 g/mL) (69ºC)
Isooctane (0.692 g/mL) (98-99ºC)
Isopropyl alcohol (0.785 g/mL) (82ºC)
Methanol (MeOH) (0.791 g/mL) (64.7ºC)
Methylene chloride (CH2Cl2) (1.325 g/mL) (39.8-40ºC)
Methyl sulfoxide (DMSO) (1.10 g/mL) (189ºC)
n-Pentane (0.626 g/mL) (35-36ºC)
1,1,2,2-Tetrachloroethane (1.586 g/mL) (147ºC)
Tetrahydrofuran (THF) (0.889 g/mL) (65-67ºC)
Toluene (0.865 g/mL) (110-111ºC)
Trichloroethane (1.336 g/mL) (74-76ºC)
Water (1 g/mL) (100ºC)
Xylene (0.868 g/mL) (138-139ºC)
Abbreviations
Technical Reference
410
Inductively Coupled Plasma
ICP
AA
Atomic Absorption
IR
Infrared
ACS
American Chemical Society
KF
Karl Fischer
ANSI American National Standards Institute
meq
Milliequivalent
AOAC Association of Official Analytical Chemists
NF
National Formulary
APHA American Public Health Association
NIST National Institute of Standards and Technology
ASTM American Society for Testing Materials
OSHA Occupational Safety and Health Administration
BSI
British Standards Institute
RFA
Renewable Fuel Association
CAS
Chemical Abstracts Service
SPE
Solid Phase Extraction
CI
Color Index
TLC
Thin Layer Chromatography
EPA
U.S. Environmental Protection Agency
USDA U.S. Department of Agriculture
GLC
Gas Liquid Chromatography
USP
U.S. Pharmacopoeia
GR
Guaranteed Reagent
Instrumentation for Analysis
GC
Gas Chromatography
GC/MS
Gas Chromatography/Mass Spectroscopy
GC/FID
Gas Chromatography/Flame Ionization Detector
GC/PID
Gas Chromatography/Photoionization Detector
GC/ECD
Gas Chromatography/Electron Capture Detector
GC/ELCD
Gas Chromatography/Electrolytic Conductivity Detector
GC/NPD
Gas Chromatography/Nitrogen phosphorus Detector
HPLC
High Performance Liquid Chromatography
NPD/TEA
Nitrogen-Phosphorus Detector/Thermal Energy Analyzer with the reductive Hall detector
TCD/FID
Thermal Conductivity Detector/Flame Ionization Detector
Nitrogen-Phosphorus Detector/Alkali-Flame Detector/Thermionic Specific Detector
NPD/AFD/TSD
NPA/ELCD/FPD Nitrogen-Phosphorus Detector/Electrolytic Conductivity Detector/Flame Photometric Detector
HRGC/LRMS
High Resolution Gas Chromatography/Low Resolution Mass Spectrometry
FTIR
Fourier Transform Infrared
General Constants
Universal Gas Constant
Acceleration Due to Gravity
Avogadro’s Constant
Speed of Light
Heat of Fusion (water 1 atm, 0ºC)
Heat of Vaporization (water 1 atm, 100ºC)
Volume of Perfect Gas
Faraday’s Constant
Planck’s Constant
Bragg’s Law
Absolute Zero
Temp. of Liquid Nitrogen
R = 0.0821(Atm)(L)/(K)(mole)
g = 32.17 ft/sec2, 9.8 m/sec2
N = 6.023 x 1023 molecules/mole
c = 186,282 miles/sec, 3 x 1010 cm/sec
ΔHfus = 79.7 cal/g
ΔHvap = 540 cal/g
22.4L/mol at 0ºC, 760 torr
F = 96485.31 C/mol
h = 6.626 x 10-27 erg/sec
2d nλ = 2d sin(θ)
-273.15 ºC
-195.8 ºC
Miscible
Immiscible
Read down column
and across for solvent
miscibility
Density@25°C
Boiling Point
Unit Conversions
Temperature
°Fahrenheit
°Celsius
(°F - 32) x 5/9
°Celsius
°Fahrenheit (°C x 9/5) + 32
°Celsius
°Kelvin
°C + 273
Mass
1 ounce
= 28.4 grams
0.03527 grams = 1 ounces
Liquid Volume
Multiply by
Ounces (US) Milliliters
29.57
Pints (US)
Liters
0.47
Quarts (US) Liters
0.95
Gallons (US) Liters
3.8
Milliliters
Ounces (US)
0.034
Liters
Pints (US)
2.1
1.06
Liters
Quarts (US)
Liters
Gallons (US)
0.26
Cubic Feet
Cubic meters
0.03
Cubic Yards Cubic meters
0.76
1 ppm = 1 µg/mL (wt. /vol.) and
1 ppm = 1 µg/g (wt./wt.)
1% = 10,000 ppm (parts per million)
1 ppm = 1,000 ppb (parts per billion)
1 ppb = 1,000 ppt (parts per trillion)
1 g = 1,000 mg (milligram)
1 mg = 1,000 µg (microgram)
1 µg = 1,000 ng (nanogram)
1 L = 1,000 mL (milliLiter)
1 mL = 1,000 µL (microLiter)
1 µL = 1,000 nL (nanoLiter)