Elenco alunni iscritti a.s. 2015_16 Scuola Inf Papa Giov XXIII.pdf

Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry.
This journal is © The Royal Society of Chemistry 2014
Electronic Supplementary Information
3-NO2-5,10,15-triarylcorrolato-Cu as a versatile
platform for synthesis of novel 3-functionalized corrole
derivatives
Manuela Stefanelli,a Marco Mancini,a Michele Raggio,a Sara Nardis, *a Frank R. Fronczeck,b Gregory
McCandless,b,c Kevin M. Smith,b and Roberto Paolessea
[email protected];
a
Dipartimento di Scienze e Tecnologie Chimiche, Università di Roma Tor Vergata, via della Ricerca
Scientifica 1, 00133 Rome, Italy
b
Department of Chemistry, Louisiana State University, Baton Rouge, LA 70803, USA
c
Department of Chemistry, The University of Texas at Dallas, Richardson, TX 75080, USA
Copies of 1H NMR and IR spectra
Figure S1: 1H NMR spectrum of 3-NHC(O)CH3-TtBuCorrCu(2)
Figure S2: 1H NMR spectrum of 3-[NHC(O)(CH2)4CH3]-TtBuCorrCu(3)
Figure S3: 1H NMR spectrum of 3-NHC(O)CH2Cl-TtBuCorrCu(4)
Figure S4: 1H NMR spectrum of 3-NHC(O)CH2N3-TtBuCorrCu(5)
100,2
98
96
2321,86
1921,58
2202,62
1853,14
1798,021765,83
94
92
90
1604,99
1436,43 1402,95
1476,35
88
1422,62
86
1462,67
84
82
80
%T
1685,25
78
76
74
2116,23
72
70
68
66
64
62
1535,00
60,0
2400,0
2200
2000
1900
1800
cm-1
1700
1600
1500
Figure S5: IR spectrum of 3-NHC(O)CH2N3-TtBuCorrCu(5)
1400,0
Figure S6: 1H NMR spectrum of 3-NHC(O)CH2(4-tolyl-triazole)TtBuCorrCu(6)
Figure S6: 1H NMR spectrum of 3-NHC(O)H-TtBuCorrCu(7)

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